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51. 发明申请

US20110262339A1 PRODUCTION OF SOLAR-GRADE SILICON FROM SILICON DIOXIDE 审中-公开
标题翻译：从二氧化硅生产太阳能级硅
公开(公告)号：US20110262339A1
公开(公告)日：2011-10-27
申请号：US13121759
申请日：2009-09-28
申请人： Hartwig Rauleder , Ekkehard Müh , Mustafa Siray , Peter Nagler , Bodo Frings , Ingrid Lunt-Rieg , Alfons Karl , Christian Panz , Thomas Groth , Guido Stochniol , Matthias Rochnia , Jürgen Erwin Lang , Oliver Wolf , Rudolf Schmitz , Bernd Nowitzki , Dietmar Wewers
发明人： Hartwig Rauleder , Ekkehard Müh , Mustafa Siray , Peter Nagler , Bodo Frings , Ingrid Lunt-Rieg , Alfons Karl , Christian Panz , Thomas Groth , Guido Stochniol , Matthias Rochnia , Jürgen Erwin Lang , Oliver Wolf , Rudolf Schmitz , Bernd Nowitzki , Dietmar Wewers
IPC分类号： C01B33/025
CPC分类号： C01B33/025 , C01B32/05 , C01B33/148
摘要： The invention relates to a complete method for producing pure silicon that is suitable for use as solar-grade silicon, comprising the reduction of a purified silicon oxide using one or more pure carbon sources, the purified silicon oxide, which was purified as silicon oxide dissolved in an aqueous phase, having a content of other polyvalent metals or metal oxides, in relation to the silicon oxide, of less than or equal to 300 ppm, preferably less than 100 ppm, especially preferably less than 50 ppm and according to the invention less than 10 ppm of the other metals and being obtained advantageously by gel formation in alkaline conditions. The invention also relates to a formulation containing an activator and to the use of purified silicon oxide together with an activator for producing silicon.
摘要翻译：本发明涉及一种适用于太阳能级硅的纯硅生产的完整方法，其中包括使用一种或多种纯碳源还原纯化的氧化硅，纯化的氧化硅被溶解为氧化硅在水相中，具有相对于氧化硅的其它多价金属或金属氧化物的含量小于或等于300ppm，优选小于100ppm，特别优选小于50ppm，并且根据本发明，较少超过10ppm的其他金属，并且有利地通过在碱性条件下的凝胶形成获得。本发明还涉及含有活化剂的配方和使用纯化的氧化硅以及用于生产硅的活化剂。

52. 发明申请

US20110236288A1 METHOD FOR PRODUCING HIGH-PURITY SIO2 FROM SILICATE SOLUTIONS 审中-公开
标题翻译：从硅酸盐溶液中生产高纯度SIO2的方法
公开(公告)号：US20110236288A1
公开(公告)日：2011-09-29
申请号：US13121754
申请日：2009-09-28
申请人： Christian Panz , Markus Ruf , Guido Titz , Florian Paulat , Hartwig Rauleder , Sven Müller , Jürgen Behnish , Jens Peltzer
发明人： Christian Panz , Markus Ruf , Guido Titz , Florian Paulat , Hartwig Rauleder , Sven Müller , Jürgen Behnish , Jens Peltzer
IPC分类号： C01B33/187 , G02B6/10 , C01B33/12
CPC分类号： C01B33/193
摘要： The invention relates to a novel method for producing high-purity SiO2 from silicate solutions, a novel high-purity SiO2 having a specific impurity spectrum and use thereof.
摘要翻译：本发明涉及一种从硅酸盐溶液中生产高纯度SiO2的新方法，一种具有特定杂质光谱的新型高纯SiO2及其用途。

53. 发明申请

US20110163462A1 Universal Infrastructure for Chemical Processes 审中-公开
标题翻译：化学工艺通用基础设施
公开(公告)号：US20110163462A1
公开(公告)日：2011-07-07
申请号：US13063171
申请日：2009-05-14
申请人： Jürgen Erwin Lang , Carl-Friedrich Hoppe , Hartwig Rauleder , Ekkehard Müh
发明人： Jürgen Erwin Lang , Carl-Friedrich Hoppe , Hartwig Rauleder , Ekkehard Müh
IPC分类号： C07G99/00 , G05B1/00
CPC分类号： B01J19/00 , B01J2219/00015 , B01J2219/00022 , B01J2219/00225
摘要： The invention relates to a plant for carrying out chemical processes comprising at least means for directly carrying out the conversion in the form of means for developing products and/or in the form of at least one reactor for the continuous industrial manufacture of products, devices for receiving and/or providing starting materials and/or products and devices for controlling the conversion, which are combined to a single integrated and transportable functional unit serving as infrastructure, preferably in the form of a standardised transport container.
摘要翻译：本发明涉及一种用于执行化学过程的设备，该设备至少包括用于以用于开发产品和/或以至少一个反应器的形式直接进行转化的装置，用于产品的连续工业化生产的装置，用于接收和/或提供用于控制转换的起始材料和/或产品和装置，其被组合到用作基础设施的单个集成和可运输的功能单元，优选地以标准化运输容器的形式。

54. 发明申请

US20080071119A1 Process for preparing alkoxy-pure alkaline-earth alkoxides 审中-公开
公开(公告)号：US20080071119A1
公开(公告)日：2008-03-20
申请号：US11980380
申请日：2007-10-31
申请人： Burkhard Standke , Hartwig Rauleder
发明人： Burkhard Standke , Hartwig Rauleder
IPC分类号： C07C29/68
CPC分类号： C07C29/705 , C07C31/30
摘要： The present invention relates to a process for preparing a metal-free, alkoxide-pure alkaline-earth alkoxide of the general formula I M(OR1)2 (I) in which M stands for an element pertaining to the second Main Group of the Periodic Table of the Elements and R1 represents a linear, branched or cyclic alkyl group with 2 to 20 C atoms, by alcoholysis of a compound of the general formula II M(OR2)x(OR3)y(OR4)z (II) in which M stands for an element pertaining to the second Main Group of the Periodic Table of the Elements, groups R2, R3 and R4 are the same or different and represent a linear alkyl group with 1 to 4 C atoms, with the proviso 0≦x≦2, 0≦y≦2, 0≦z≦2 with (x+y+z)=2, with an alcohol, which is employed in excess, of the general formula III HOR1 (III) in which R1 has the same significance as in formula I, is different from groups R2, R3 and R4 according to formula II, and in the alkyl chain possesses at least one C atom more than the longest alkyl group from the series R2, R3 and R4, the compounds of the formula I and/or of the formula II being kept dissolved, at least in a proportion, during the conversion.

55. 发明申请

US20070166456A1 Process for producing low-k dielectric films 失效
标题翻译：低k电介质薄膜的制造方法
公开(公告)号：US20070166456A1
公开(公告)日：2007-07-19
申请号：US10563450
申请日：2004-06-02
申请人： Adolf Kuehnle , Carsten Jost , Hartwig Rauleder , Come Rentrop , Roelant Van Dam , Klaas Timmer , Hartmut Fischer
发明人： Adolf Kuehnle , Carsten Jost , Hartwig Rauleder , Come Rentrop , Roelant Van Dam , Klaas Timmer , Hartmut Fischer
IPC分类号： B05D3/12 , B05D3/02
CPC分类号： H01L21/02126 , C09D183/04 , H01L21/02203 , H01L21/02216 , H01L21/02282 , H01L21/31695
摘要： The invention relates to processes for producing low-k dielectric films on semiconductors or electrical circuits, which comprises using incompletely condensed polyhedral oligomeric silsesquioxanes of the formula [(RaXbSiO1.5)m(RcYdSiO)n] with: a, b=0-1; c, d=1; m+n≧3; a+b=1; n, m≧1, R=hydrogen atom or alkyl, cycloalkyl, alkenyl, cycloalkenyl, alkynyl, cycloalkynyl, aryl or heteroaryl group, in each case substituted or unsubstituted, X=an oxy, hydroxyl, alkoxy, carboxyl, silyl, silyloxy, halogen, epoxy, ester, fluoroalkyl, isocyanate, acrylate, methacrylate, nitrile, amino or phosphine group or substituents of type R containing at least one such group of type X, Y=hydroxyl, alkoxy or a substituent of type O—SiZ1Z2Z3, where Z1, Z2 and Z3 are fluoroalkyl, alkoxy, silyloxy, epoxy, ester, acrylate, methacrylate or a nitrile group or substituents of type R and are identical or different, not only the substituents of type R being identical or different but also the substituents of type X and Y in each case being identical or different, and comprising at least one hydroxyl group as substituent of type Y, for producing the film, and to low-k dielectric films produced by this process.
摘要翻译：本发明涉及用于在半导体或电路上生产低k电介质膜的方法，其包括使用下式的不完全缩合的多面体低聚倍半硅氧烷：[（R a）a＆lt; b＆gt; 其中：a（a）和（c），m ，b = 0-1; c，d = 1; m + n> = 3; a + b = 1; n，m = 1，R =氢原子或烷基，环烷基，烯基，环烯基，炔基，环炔基，芳基或杂芳基，各自为取代或未取代的，X =氧基，羟基，烷氧基，羧基，甲硅烷基，卤素，环氧基，酯，氟代烷基，异氰酸酯，丙烯酸酯，甲基丙烯酸酯，腈，氨基或膦基或含有至少一个X，Y =羟基，烷氧基或O-SiZ型取代基的至少一种的R型取代基，其中Z 1，Z 2和Z _{3是氟代烷基，烷氧基，甲硅烷氧基，环氧基，酯，丙烯酸酯，甲基丙烯酸酯或腈基或R的取代基相同或不同，不仅R的取代基相同或不同，而且取代基 X和Y各自相同或不同，并且包含至少一个作为Y型取代基的羟基，用于制备该膜，以及通过该方法制备的低k电介质膜。}

56. 发明申请

US20050131257A1 Process for preparing alkoxy-pure alkaline earth alkoxides 失效
标题翻译：制备烷氧基 - 纯碱土金属醇盐的方法
公开(公告)号：US20050131257A1
公开(公告)日：2005-06-16
申请号：US11010831
申请日：2004-12-13
申请人： Burkhard Standke , Hartwig Rauleder
发明人： Burkhard Standke , Hartwig Rauleder
IPC分类号： C07C29/128 , C07C29/70 , C07C31/30 , C07C29/10
CPC分类号： C07C29/705 , C07C31/28
摘要： The present invention provides a process for preparing a metal-free alkaline earth methanolate by alcoholysis of an alkaline earth ethanolate with methanol.
摘要翻译：本发明提供了一种通过碱土金属醇化物与甲醇的醇解制备无金属碱土金属甲醇的方法。

57. 发明授权

US5068382A Process for the production of organosilicon compounds 失效
标题翻译：生产有机硅化合物的方法
公开(公告)号：US5068382A
公开(公告)日：1991-11-26
申请号：US491775
申请日：1990-03-12
申请人： Hartwig Rauleder , Hans-Joachim Kotzch
发明人： Hartwig Rauleder , Hans-Joachim Kotzch
IPC分类号： C07F7/18
CPC分类号： C07F7/188 , C07F7/182
摘要： Organosilicon compounds of the formula ##STR1## wherein R.sup.1 and R.sup.2 are each independently straight or branched alkyl of 1 to 4 carbon atoms or --OR.sup.3,R.sup.3 is R.sup.4 --(OR.sup.5).sub.m --,R.sup.6 is straight or branched alkyl of 1 to 4 carbon atoms,m is an integer from 0 to 6, inclusive,R.sup.5 is straight or branched alkylene of 2 to 4 carbon atoms, which may be identical or different when m is an integer from 2 to 6, andR.sup.6 is straight or branched alkylene of 2 to 6 carbon atoms,are prepared by reacting hydrogensilanes of the formula ##STR2## wherein R.sup.7 are identical or different groups R.sup.4 or the group OR.sup.4, and R.sup.4 has the previously indicated meaning,with terminally unsaturated ethers of the formulaR.sup.4 --(OR.sup.5).sub.m --OR.sup.8whereinm, R.sup.4 and R.sup.5 have the previously indicated meanings, andR.sup.8 is terminally unsaturated straight or branched alkenyl or 2 to 6 carbon atoms,in the presence of a catalyst at controlled temperatures to form addition products of the formula ##STR3## wherein m and R.sup.4, R.sup.5, R.sup.6 and R.sup.7 have the previously indicated meanings, and the R.sup.4 's are identical or differentwhich are converted into the desired end products by thermal and/or catalytic transesterification with monofunctional hydroxy compounds of the formulaR.sup.4 --(OR.sup.5).sub.m OHwhereinm, R.sup.4 and R.sup.5 have the previously indicated meanings.
摘要翻译：其中R 1和R 2各自独立地为具有1至4个碳原子的直链或支链烷基或-OR 3，R 3为R 4 - （OR 5）m - ，R 6为具有1至4个碳原子的直链或支链烷基的有机硅化合物原子，m为0〜6的整数，包括0和6的整数，R 5为2〜4个碳原子的直链或支链亚烷基，当m为2〜6的整数时，可以相同或不同，R6为直链或支链的亚烷基 2至6个碳原子的化合物通过使下式的化合物：其中R 7为相同或不同的基团R 4或基团OR 4，且R 4具有前述含义的氢化山西与式R4-（OR5）的末端不饱和醚反应制备， m-OR 8，其中m，R 4和R 5具有前述含义，并且R 8是在受控温度下在催化剂存在下的末端不饱和的直链或支链烯基或2-6个碳原子，以形成下式的加成产物：其中m和R4，R5，R6和R7具有之前的并且R4相同或不同，其通过用式R 4 - （OR 5）m OH的单官能羟基化合物的热和/或催化酯交换转化为所需的最终产物，其中m，R 4和R 5具有前面所述的含义。

58. 发明授权

US09446954B2 Process for the coupled preparation of trisilylamine and polysilazanes having a molar mass of up to 500 g/mol 有权
标题翻译：具有摩尔质量高达500g / mol的三甲胺和聚硅氮烷的偶联制备方法
公开(公告)号：US09446954B2
公开(公告)日：2016-09-20
申请号：US14345587
申请日：2013-06-05
申请人： Carl-Friedrich Hoppe , Christian Goetz , Goswin Uehlenbruck , Hartwig Rauleder
发明人： Carl-Friedrich Hoppe , Christian Goetz , Goswin Uehlenbruck , Hartwig Rauleder
IPC分类号： C01B21/087 , B01D3/14 , C08G77/62 , B01J19/24
CPC分类号： C01B21/087 , B01D3/143 , B01J19/24 , B01J2219/24 , C08G77/62
摘要： The invention relates to a process for preparing trisilylamine and polysilazanes in the liquid phase, in which ammonia is introduced in a superstoichiometric amount relative to 5 monochlorosilane which is present in an inert solvent. Here, a reaction in which trisilylamine and polysilazanes are formed proceeds. TSA is subsequently separated off in gaseous form from the product mixture. The TSA obtained is purified by filtration and distillation and obtained in high or very high purity. The bottom product mixture is conveyed from the reactor through a filter unit in which solid ammonium chloride is separated off to give a liquid mixture of polysilazanes and solvent. This is fed to a further distillation to recover solvent. As a result of the NH3 being introduced in a superstoichiometric amount relative to monochlorosilane, monochlorosilane is completely reacted in the reactor. This completely prevents the reaction of monochlorosilane with additional disilylamine formed in small amounts to form solid ammonium chloride in the downstream plant parts for purification of the TSA. The solutions filtered downstream of the reactor are accordingly completely free of solids.
摘要翻译：本发明涉及一种在液相中制备三甲胺和聚硅氮烷的方法，其中相对于存在于惰性溶剂中的5个一氯硅烷，以超化学计量的量引入氨。这里，形成三甲基胺和聚硅氮烷的反应。 TSA随后从产物混合物中分离出气态。通过过滤和蒸馏纯化获得的TSA，得到高纯度或非常高的纯度。底部产物混合物从反应器通过过滤器单元输送，其中分离固体氯化铵以得到聚硅氮烷和溶剂的液体混合物。将其进料进一步蒸馏以回收溶剂。作为相对于一氯硅烷以超化学计量量引入NH 3的结果，一氯硅烷在反应器中完全反应。这完全防止一氯甲硅烷与少量形成的另外的二甲硅烷的反应在下游的植物部分中形成固体氯化铵，用于纯化TSA。因此，在反应器下游过滤的溶液完全不含固体。

59. 发明授权

US09359205B2 Production of trisilylamine from monochlorosilane and ammonia by use of inert solvent 有权
公开(公告)号：US09359205B2
公开(公告)日：2016-06-07
申请号：US14724114
申请日：2015-05-28
申请人： Carl-Friedrich Hoppe , Hartwig Rauleder , Christian Goetz
发明人： Carl-Friedrich Hoppe , Hartwig Rauleder , Christian Goetz
IPC分类号： C01B33/00 , C07F7/02 , C01B21/087 , B01D3/14 , B01D3/00 , B01J19/24
CPC分类号： C01B21/087 , B01D3/009 , B01D3/143 , B01J19/24 , B01J2219/00002 , B01J2219/24 , C01B33/00 , C07F7/025
摘要： The present invention relates to a specific process for producing trisilylamine from monochlorosilane and ammonia in the liquid phase. The invention further relates to a plant wherein such a process can be carried out with advantage.

60. 发明授权

US08246925B2 Processing of chlorosilane flows containing boron 有权
标题翻译：加工含硼的氯硅烷流程
公开(公告)号：US08246925B2
公开(公告)日：2012-08-21
申请号：US12528087
申请日：2008-01-22
申请人： Christoph Schwarz , Dorothea Schwarz , Hartwig Rauleder , Ingo Pauli , Andreas Nelte , Harald Seiler
发明人： Christoph Schwarz , Dorothea Schwarz , Hartwig Rauleder , Ingo Pauli , Andreas Nelte , Harald Seiler
IPC分类号： C01B33/08
CPC分类号： B01D3/143 , C01B33/10778
摘要： The invention relates to a method for yielding boron-depleted chlorosilanes from a chlorosilane mixture containing boron by means of separation by distillation of a boron-enriched distillation flow. The invention further relate to a device for yielding boron-depleted chlorosilanes from a chlorosilane mixture containing boron.
摘要翻译：本发明涉及通过蒸馏富硼蒸馏流分离从含有硼的氯硅烷混合物中产生贫硼的氯硅烷的方法。本发明还涉及从含有硼的氯硅烷混合物中产生贫硼的氯硅烷的装置。

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