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1. 发明授权

US09079777B2 Method for producing inorganic oxide particles 有权
标题翻译：无机氧化物粒子的制造方法
公开(公告)号：US09079777B2
公开(公告)日：2015-07-14
申请号：US14533560
申请日：2014-11-05
申请人： TOKUYAMA CORPORATION
发明人： Takayuki Maehara , Tadaharu Komatsubara , Yuya Yamano , Kenichi Ishizu , Makoto Sato , Hiroaki Taira , Hiroshi Kato
IPC分类号： C07F7/02 , C01B33/146 , C01B13/36 , C01B33/18 , C01B33/148 , C01G23/04 , C01G25/02 , C07F7/08 , C07F7/10
CPC分类号： C01B33/146 , C01B13/36 , C01B13/363 , C01B33/141 , C01B33/148 , C01B33/154 , C01B33/18 , C01G23/04 , C01G25/02 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C07F7/08 , C07F7/10 , C09C1/3081
摘要： The present invention relates to a method for producing inorganic oxide particles, comprising at least the following steps of: coagulating a dispersion obtained by carrying out the hydrolysis reaction and the polycondensation reaction of a metal alkoxide in the presence of a basic catalyst; filtering the dispersion to obtain particles; and drying the particles, wherein the step of coagulating the dispersion is carried out by adding a coagulant comprising at least one compound selected from the group consisting of carbon dioxide, ammonium carbonate, ammonium hydrogen carbonate and ammonium carbamate to the dispersion. The inorganic oxide particles obtained by the method of the present invention have high purity and are excellent in flowability.
摘要翻译：本发明涉及无机氧化物粒子的制造方法，至少包括以下步骤：在碱性催化剂的存在下使通过进行水解反应和金属醇盐的缩聚反应得到的分散体凝结; 过滤分散体以获得颗粒; 并干燥所述颗粒，其中通过将至少一种选自二氧化碳，碳酸铵，碳酸氢铵和氨基甲酸铵的化合物的凝结剂加入到分散体中来进行凝固分散体的步骤。通过本发明的方法获得的无机氧化物颗粒具有高纯度并且流动性优异。

2. 发明申请

US20130145964A1 PROCESS FOR PRODUCING A SILICA SOL MATERIAL 有权
标题翻译：生产二氧化硅溶胶材料的方法
公开(公告)号：US20130145964A1
公开(公告)日：2013-06-13
申请号：US13702676
申请日：2010-06-02
申请人： Ekkehard Barth , Rolf Bachmann , Arne Braun , Maren Heinemann , Sebastian Schmidt
发明人： Ekkehard Barth , Rolf Bachmann , Arne Braun , Maren Heinemann , Sebastian Schmidt
IPC分类号： C01B33/141 , C01B33/14
CPC分类号： C01B33/141 , C01B33/14 , C01B33/145 , C01B33/148 , C04B35/6224 , C04B35/624 , C04B35/6263 , C04B35/62635 , C04B35/62685 , C04B2235/3418 , C04B2235/441 , C08L83/02
摘要： The present invention relates to an improved process for producing a biodegradable and/or absorbable silica sol material which is advantageous especially with regard to the reproducibility of the material, the rapidity of the synthesis and the possibility of being able to produce the silica sol material on an industrial scale. A further subject matter of the invention relates to a biodegradable and/or absorbable silica sol material which can be produced by the synthesis process according to the invention.
摘要翻译：本发明涉及一种用于生产可生物降解和/或可吸收的硅溶胶材料的改进方法，其特别是关于材料的再现性，合成的快速性以及能够生产二氧化硅溶胶材料的可能性是有利的工业规模。本发明的另一个主题涉及可通过根据本发明的合成方法制备的可生物降解和/或可吸收的硅溶胶材料。

3. 发明申请

US20130068139A1 Silica gel comprising guanidine carbonate 审中-公开
标题翻译：含有碳酸胍的硅胶
公开(公告)号：US20130068139A1
公开(公告)日：2013-03-21
申请号：US13617807
申请日：2012-09-14
申请人： Lothar Puppe , Dietrich Pantke
发明人： Lothar Puppe , Dietrich Pantke
IPC分类号： C08K3/28
CPC分类号： C08K3/28 , C01B33/148 , D21H17/68 , D21H21/10
摘要： A process of preparing a silica sol is described. The process involves reacting a fresh sol with guanidine carbonate. The reaction may be conducted in the presence of a base (e.g., sodium water glass), and at a pH of from 8 to 12. The process of the present invention may also include concentrating steps. The silica sol prepared by the method of the present invention has a BET surface area of greater than or equal to 100 m2/g, and contains from 0.05 to 15% by weight of gaunidinium ions, based on the total weight of the silica gel.
摘要翻译：描述了制备二氧化硅溶胶的方法。该方法包括使新鲜的溶胶与碳酸胍反应。反应可以在碱（例如钠水玻璃）存在下进行，pH为8〜12。本发明的方法还可以包括浓缩步骤。通过本发明的方法制备的二氧化硅溶胶具有大于或等于100m 2 / g的BET表面积，并且基于硅胶的总重量含有0.05至15重量％的高锰酸根离子。

4. 发明授权

US08299131B2 Silica gel comprising guanidine carbonate 失效
标题翻译：含有碳酸胍的硅胶
公开(公告)号：US08299131B2
公开(公告)日：2012-10-30
申请号：US10520574
申请日：2003-07-07
申请人： Lothar Puppe , Dietrich Pantke
发明人： Lothar Puppe , Dietrich Pantke
IPC分类号： C01B33/12 , C01B33/141
CPC分类号： C08K3/28 , C01B33/148 , D21H17/68 , D21H21/10
摘要： A process of preparing a silica sol is described. The process involves reacting a fresh sol with guanidine carbonate. The reaction may be conducted in the presence of a base (e. g. , sodium water glass), and at a pH of from 8 to 12. The process of the present invention may also include concentrating steps. The silica sol prepared by the method of the present invention has a BET surface area of greater than or equal to 100 m2/g, and contains from 0.05 to 15% by weight of gaunidinium ions, based on the total weight of the silica gel.
摘要翻译：描述了制备二氧化硅溶胶的方法。该方法包括使新鲜的溶胶与碳酸胍反应。反应可以在碱（例如钠水玻璃）存在下进行，pH为8〜12。本发明的方法还可以包括浓缩步骤。通过本发明的方法制备的二氧化硅溶胶具有大于或等于100m 2 / g的BET表面积，并且基于硅胶的总重量含有0.05至15重量％的高锰酸根离子。

5. 发明申请

US20100003204A1 Nanoparticle hybrid sunscreens 审中-公开
标题翻译：纳米粒子混合防晒剂
公开(公告)号：US20100003204A1
公开(公告)日：2010-01-07
申请号：US12459541
申请日：2009-07-02
申请人： Douglas Anson Loy , Kenneth J. Shea , Dylan J. Boday , Jason T. Wertz
发明人： Douglas Anson Loy , Kenneth J. Shea , Dylan J. Boday , Jason T. Wertz
IPC分类号： A61K8/02 , C01B33/12
CPC分类号： C01B33/145 , A61K8/025 , A61K8/585 , A61K8/891 , A61K2800/412 , A61K2800/434 , A61K2800/612 , A61K2800/651 , A61Q17/04 , C01B33/146 , C01B33/148
摘要： The invention discloses and claims a new class of chemical compositions with ideal sunscreen properties. The chemical composition comprises spherical particles between 200 nm and 10 microns in diameter prepared by an emulsion polymerization of tetraalkoxysilanes or organotrialkoxysilanes or organobridged trialkoxysilanes with a dye monomer bearing two or more alkoxysilyl groups attached to the bridging chromophore. The resulting spheres absorb ultraviolet light. The dye can be any organic chromophore capable of receiving multiple trialkoxysilyl groups resulting in multipoint covalent attachment that precludes leaching of the dye from the spheres. The formic acid-toluene-monomer emulsion polymerization allows for large-scale (>100 gram) synthesis of monodisperse particles under acidic, non-aqueous conditions without surfactants. The particles less than 1 micron in diameter are smooth as talc to the touch and will provide a smooth formulation for sunscreen creams or lotions.
摘要翻译：本发明公开并要求具有理想的防晒性能的新一类化学组合物。化学组成包括通过四烷氧基硅烷或有机三烷氧基硅烷或有机桥连三烷氧基硅烷与带有两个或多个连接到桥接发色团上的烷氧基甲硅烷基的染料单体的乳液聚合制备的直径在200nm和10微米之间的球形颗粒。所得球体吸收紫外线。染料可以是能够接受多个三烷氧基甲硅烷基的任何有机发色团，导致多点共价连接，其排除了染料从球体中浸出。甲酸 - 甲苯 - 单体乳液聚合允许在无表面活性剂的酸性，非水性条件下大规模（> 100克）合成单分散颗粒。直径小于1微米的颗粒作为滑石使其光滑滑动，并提供防晒霜或乳液的光滑配方。

6. 发明授权

US3969266A Microporous membrane process for making concentrated silica sols 失效
标题翻译：用于制备浓缩硅溶胶的微孔膜方法
公开(公告)号：US3969266A
公开(公告)日：1976-07-13
申请号：US375943
申请日：1973-07-02
申请人： Ralph K. Iler
发明人： Ralph K. Iler
IPC分类号： C01B33/143 , C01B33/148 , B01J13/00
CPC分类号： C01B33/148 , C01B33/143
摘要： Aqueous silica sols having a pH from 8 to 11 containing 1 to 40% by weight of colloidal silica and soluble salts can be purified and concentrated by filtering the soluble salt from the sol using a microporous membrane filter while maintaining the salt concentration within a range determined by the concentration of silica in the sol. In one embodiment, colloidal silica particles are grown to a larger size by starting with a sol of nuclei, and adding sodium silicate solution and acid.
摘要翻译：含有1〜40重量％胶体二氧化硅和可溶性盐的pH为8〜11的二氧化硅水溶液可以通过使用微孔膜过滤器从溶胶中过滤可溶性盐进行纯化和浓缩，同时将盐浓度保持在确定的范围内通过二氧化硅在溶胶中的浓度。在一个实施方案中，胶体二氧化硅颗粒通过从核溶胶开始并加入硅酸钠溶液和酸而生长至更大的尺寸。

7. 发明授权

US3654105A Production of silica sols by electrolysis 失效
标题翻译：通过电解制备二氧化硅溶胶
公开(公告)号：US3654105A
公开(公告)日：1972-04-04
申请号：US3654105D
申请日：1969-07-15
申请人： MONSANTO CHEMICALS
发明人： CHILTON HENRY THOMAS JOSEPH
IPC分类号： C01B33/148 , C25B1/00 , B01J13/00 , B01K1/00 , C01B33/14
CPC分类号： C01B33/148 , C25B1/00 , Y10S264/19
摘要： THE PRESENT INVENTION RELATED TO THE PRODUCTION OF A SILICA SOL WHICH COMPRISES THE STEPS OF PASSING AN ELECTRIC CURRENT BETWEEN THE PAIR OF ELECTRODES, THE ANODE OF WHICH PAIR IS FABRICATED OF A SILICON-CONTAINING MATERIAL SUCH AS A FERROSILICON, POSITIONED IN AN ELECTROLYTIC CELL CONTAINING A LIQUID MEDIUM COMPRISING WATER, AN ALCOHOL SUCH AS ETHANOL AND AN ELECTROLYTE SUCH AS SULPHURIC ACID FOR A SUFFICIENT PERIOD OF TIME TO FORM THE ABOVE-DESCRIBED SILICA SOL. ADDITIONAL EMBODIMENTS (OF THE PRESENT INVENTION) COVER THE AQUEOUS MEDIUM COMPOSITION PER SE AND THE CONTINUOUS PROCESS FOR PREPARING THE SILICA SOL.

8. 发明授权

US3502593A Method for preparing a small particle size silica sol 失效
标题翻译：制备小颗粒硅胶的方法
公开(公告)号：US3502593A
公开(公告)日：1970-03-24
申请号：US3502593D
申请日：1966-10-18
申请人： NALCO CHEMICAL CO
发明人： MINDICK MORRIS
IPC分类号： C01B33/148 , C01B33/14 , B01J13/00 , C09J1/00
CPC分类号： C01B33/148

9. 发明授权

US2833724A Concentrating silica sols without particle growth 失效
标题翻译：浓缩硅胶无颗粒生长
公开(公告)号：US2833724A
公开(公告)日：1958-05-06
申请号：US45896354
申请日：1954-09-28
申请人： DU PONT
发明人： ALEXANDER GUY B , MCWHORTER JOHN R
IPC分类号： C01B33/148
CPC分类号： C01B33/148

10. 发明授权

US10865113B2 Method for producing purified aqueous solution of silicic acid 有权
公开(公告)号：US10865113B2
公开(公告)日：2020-12-15
申请号：US15768846
申请日：2016-10-14
申请人： NISSAN CHEMICAL INDUSTRIES, LTD.
发明人： Hiroaki Sakaida , Eiichiro Ishimizu
IPC分类号： C01B33/12 , C01B33/141 , C01B33/148 , C01B33/143 , B01D15/38 , B01J39/07 , B01D15/36 , B01J39/04 , B01J39/18 , B01J45/00 , B01J47/026 , C09K3/14
CPC分类号： C01B33/122 , B01D15/362 , B01D15/3828 , B01J39/04 , B01J39/07 , B01J39/18 , B01J45/00 , B01J47/026 , C01B33/141 , C01B33/148 , C01B33/1435 , C01P2006/60 , C09K3/1409
摘要： There is provided a method for obtaining a purified aqueous solution of silicic acid containing less metal impurities such as Cu and Ni using water glass as a raw material with less number of purification steps than that in conventional methods without using any unnecessary additives. The method for producing a purified aqueous solution of silicic acid, the method comprising the steps of:

(a) passing an aqueous solution of alkaline silicate having a silica concentration of 0.5% by mass or more and 10% by mass or less through a column filled with a polyamine-, iminodiacetic acid-, or aminophosphoric acid-type chelating resin, and
(b) passing the aqueous solution passed in the step (a) through a column filled with a hydrogen-type cation exchange resin.

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