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41. 发明授权

US06313210B1 Silica-reinforced rubber compounds containing moisture stabilized polymers 有权
标题翻译：含有水分稳定的聚合物的二氧化硅增强橡胶化合物
公开(公告)号：US06313210B1
公开(公告)日：2001-11-06
申请号：US09630343
申请日：2000-07-31
申请人： Chen-Chy Lin , Terrence E. Hogan , William L. Hergenrother
发明人： Chen-Chy Lin , Terrence E. Hogan , William L. Hergenrother
IPC分类号： C08K334
CPC分类号： C08K3/04 , C08C19/25 , C08K3/36 , C08L83/04
摘要： A vulcanizable elastomeric composition comprises a moisture stabilized polymer, a reinforcing filler comprising silica, a processing aid, and a cure agent comprising an effective amount of sulfur to achieve a satisfactory cure of the composition. The moisture stabilized polymer comprises the hydrolysis reaction product of a hydrolyzable substituent of an alkoxysilane terminated polymer reacted with a viscosity stabilizing effective amount of a viscosity stabilizing agent comprising a first long chain alcohol, prior to contacting the polymer with water. The processing aid is a second long chain alcohol, an alkyl alkoxysilane, or a mixture thereof.
摘要翻译：可硫化的弹性体组合物包含水分稳定的聚合物，包含二氧化硅的增强填料，加工助剂和包含有效量的硫的固化剂以实现组合物的令人满意的固化。水分稳定的聚合物包括在与聚合物接触之前，烷氧基硅烷封端聚合物的可水解取代基与粘度稳定有效量的包含第一长链醇的粘度稳定剂反应的水解反应产物。加工助剂是第二长链醇，烷基烷氧基硅烷或其混合物。

42. 发明授权

US06255404B1 Method to control increase in viscosity during aging of siloxane modified polymers 有权
标题翻译：控制硅氧烷改性聚合物老化过程中粘度增加的方法
公开(公告)号：US06255404B1
公开(公告)日：2001-07-03
申请号：US09360551
申请日：1999-07-26
申请人： Terrence E. Hogan , Chen-Chy Lin , William L. Hergenrother
发明人： Terrence E. Hogan , Chen-Chy Lin , William L. Hergenrother
IPC分类号： C08F800
CPC分类号： C08K5/5419 , C08C19/44 , C08K5/13 , C08L9/06 , C08L43/04
摘要： A method for controlling any increase in Mooney viscosity during aging of siloxane-functionalized polymers includes the step of adding a viscosity stabilizing effective amount of a viscosity stabilizing agent selected from the group consisting of alkyl alkoxysilanes of the structural formula R1nSi(OR2)4-n wherein R1 is selected from the group consisting of C1 to C20 alkyl, C4 to C10 cycloalkyl, or C5 to C20 aromatic groups, wherein R2 may be the same as or different from R1 and is selected from the group consisting of C1 to C20 alkyl, C4 to C10 cycloalkyl, or C5 to C20 aromatic groups, and wherein n is an integer from 1 to 3. The method provides for the stabilization of Mooney viscosity of siloxane-functionalized polymers at any given level upon aging. The viscosity stabilizing agents react with the siloxane-functionalized polymers during hydrolysis of the siloxane end groups to form moisture stabilized polymers.
摘要翻译：用于控制硅氧烷官能化聚合物老化期间门尼粘度的任何增加的方法包括添加粘度稳定有效量的粘度稳定剂的步骤，所述粘度稳定剂选自由结构化学式R的烷基烷氧基硅烷组成的组，其选自 C 1至C 20烷基，C 4至C 10环烷基或C 5至C 20芳族基团，其中R 2可以与R 1相同或不同，并且选自C 1至C 20烷基，C 4至C 10环烷基或C 5至 C20芳族基团，并且其中n是1至3的整数。该方法提供了在老化时以任何给定水平稳定硅氧烷官能化聚合物的门尼粘度。在硅氧烷端基的水解期间，粘度稳定剂与硅氧烷官能化的聚合物反应以形成水分稳定的聚合物。

43. 发明申请

US20080308204A1 FUNCTIONAL POLYMERS PREPARED WITH SULFUR-CONTAINING INITIATORS 有权
标题翻译：功能性聚合物与含硫装置的制备
公开(公告)号：US20080308204A1
公开(公告)日：2008-12-18
申请号：US12139567
申请日：2008-06-16
申请人： Terrence E. Hogan , William L. Hergenrother
发明人： Terrence E. Hogan , William L. Hergenrother
IPC分类号： B60C1/00 , C07C321/14
CPC分类号： B60C1/0016 , B60C1/00 , B60C1/0025 , C08F36/04 , C08L19/006 , C08F4/48
摘要： A method for forming a polymer including a sulfur-containing functional group, the method comprising introducing a sulfur-containing initiator defined by the formula with conjugated diene monomer and optionally copolymerizable monomer within a polymerization medium and allowing the sulfur-containing initiator to initiate the polymerization of the conjugated diene monomer and the optional copolymerizable monomer, where R1 is a monovalent organic group, R2 is a divalent organic group, R3 is a divalent organic group or a bond, and a is an integer from 1 to about 5.
摘要翻译：一种形成含有含硫官能团的聚合物的方法，所述方法包括将由式表示的含硫起始物与共轭二烯单体和任选的可共聚单体引入聚合介质中，并允许含硫引发剂引发聚合的共轭二烯单体和任选的可共聚单体，其中R 1为一价有机基团，R 2为二价有机基团，R 3为二价有机基团或键，a为1至约5的整数。

44. 发明授权

US06303694B1 Compounding process for achieving uniform, fine particle size dispersion of curing agents in the substantial absence of solvents and a sealant produced thereby 失效
标题翻译：在基本上不存在溶剂的情况下实现固化剂的均匀，细粒度分散的复合方法和由此产生的密封剂
公开(公告)号：US06303694B1
公开(公告)日：2001-10-16
申请号：US09507381
申请日：2000-02-18
申请人： Terrence E. Hogan , William L. Hergenrother , Christine Morehart
发明人： Terrence E. Hogan , William L. Hergenrother , Christine Morehart
IPC分类号： C08F800
CPC分类号： C08J3/226 , C08J2321/00 , C08K5/33 , C08L21/00
摘要： A process for the preparation of a sealant composition by mixing an elastomer in the substantial absence of an organic solvent and separately dispersing a quinoid curing agent in a polymer having a molecular weight below about 5,000 to form a curing agent concentrate. Thereafter, combining the curing agent concentrate with the elastomer to form the sealant composition. The composition is a rubber masterbatch having many applications and is advantageously, substantially free from organic solvents.
摘要翻译：通过在基本上不存在有机溶剂的情况下混合弹性体并且将醌型固化剂单独分散在分子量低于约5,000的聚合物中以形成固化剂浓缩物来制备密封剂组合物的方法。此后，将固化剂浓缩物与弹性体组合以形成密封剂组合物。该组合物是具有许多应用的橡胶母料，并且有利地基本上不含有机溶剂。

45. 发明申请

US20150126675A1 Polydienes And Diene Copolymers Having Organophosphine Functionality 有权
标题翻译：具有有机膦功能的聚二烯和二烯共聚物
公开(公告)号：US20150126675A1
公开(公告)日：2015-05-07
申请号：US14398644
申请日：2013-05-01
申请人： Terrence E. Hogan , William l. Hergenrother , David M. Roggeman , Bridgestone Corporation
发明人： Terrence E. Hogan , William L. Hergenrother , David M. Roggeman
IPC分类号： C08F236/06 , C08K3/36 , C08K3/04
CPC分类号： C08F236/06 , C08F230/02 , C08F236/04 , C08K3/04 , C08K3/36 , C08L43/02
摘要： Embodiments provide polydienes and diene copolymers having organophosphines functionality. Specific embodiments employ phosphorus-containing organometal initiators and copolymers prepared by anionically polymerizing conjugated diene monomer and vinyl organophosphine.
摘要翻译：实施方案提供具有有机膦功能性的聚二烯和二烯共聚物。具体实施方案使用含磷有机金属引发剂和通过阴离子聚合共轭二烯单体和乙烯基有机膦制备的共聚物。

46. 发明申请

US20130281588A1 RUBBER COMPOSITIONS WITH FILLER AND KETOXIME OR KETIXMO SILANE 有权
标题翻译：橡胶组合物与填充剂和KETOXIME或KETIXMO硅烷
公开(公告)号：US20130281588A1
公开(公告)日：2013-10-24
申请号：US13819815
申请日：2011-08-31
申请人： Chenchy J. Lin , Yaohong Chen , Atsushi Fukushima , William L. Hergenrother , Terrence E. Hogan
发明人： Chenchy J. Lin , Yaohong Chen , Atsushi Fukushima , William L. Hergenrother , Terrence E. Hogan
IPC分类号： C08K5/5465
CPC分类号： C08K5/5465 , C08K3/04 , C08K5/548 , C08L91/00 , C08L21/00
摘要： A composition includes an elastomer and a ketoximo silane or a ketoxime additive. The ketoximo silane corresponds to Formula I: where D is selected from a C1 to C60 hydrocarbyl group, or when A is 0 or 1 a hydrogen, or the structure in Formula III; and wherein n and j are independently 1, 2, or 3, m and q are independently 0 or 1, z and t are independently 0 or 1 and (n+m+z) is equal to 3 and (j+q+t) is equal to 3; A is 0 or greater than or equal to 1; R1 and R2 are independently Ci to C60 divalent organic groups and may optionally include O, N S, Si, and/or P heteroatoms with the proviso that when A is 0 either of R1 and R2 may be a chemical bond; R3, R4, R8 and R9 are independently a hydrogen, or a C1 to C60 hydrocarbyl or alkoxy group optionally including O, N, S, Si and/or P; R5 and R6 are independently hydrogen or C1 to C60 hydrocarbyl groups and may optionally include O, N S, Si, and/or P heteroatoms, and may optionally be bonded together to form a cyclic ring; R10 and R11 are independently hydrogen or C1 to C60 hydrocarbyl groups and may optionally include O, N S, Si, and/or P heteroatoms, and may optionally be bonded together to form a cyclic ring.
摘要翻译：组合物包括弹性体和酮肟基硅烷或酮肟添加剂。酮肟基硅烷对应于式I：其中D选自C1至C60烃基，或当A为0或1时为氢或式III中的结构; 并且其中n和j独立地为1,2或3，m和q独立地为0或1，z和t独立地为0或1，并且（n + m + z）等于3，并且（j + q + t ）等于3; A为0或大于或等于1; R 1和R 2独立地为C 1至C 60二价有机基团，并且可任选地包括O，N S，Si和/或P杂原子，条件是当A为0时，R 1和R 2可以是化学键; R 3，R 4，R 8和R 9独立地为氢或任选包括O，N，S，Si和/或P的C 1至C 60烃基或烷氧基; R 5和R 6独立地是氢或C 1至C 60烃基，并且可任选地包括O，N S，Si和/或P杂原子，并且可以任选地结合在一起形成环状环; R 10和R 11独立地为氢或C 1至C 60烃基，并且可以任选地包括O，N S，Si和/或P杂原子，并且可以任选地结合在一起形成环状环。

47. 发明授权

US08362181B2 Functional polymers prepared with sulfur-containing initiators 有权
标题翻译：用含硫引发剂制备的官能聚合物
公开(公告)号：US08362181B2
公开(公告)日：2013-01-29
申请号：US13247245
申请日：2011-09-28
申请人： Terrence E. Hogan , William L. Hergenrother
发明人： Terrence E. Hogan , William L. Hergenrother
IPC分类号： C08F36/04 , C08F4/48
CPC分类号： B60C1/0016 , B60C1/00 , B60C1/0025 , C08F36/04 , C08L19/006 , C08F4/48
摘要： A sulfur-containing anionic polymerization initiator defined by the formula: R1S—R2aR3⊖Li⊕ where R1 is a monovalent organic group, R2 is a divalent organic group, R3 is a divalent organic group or a bond, and a is an integer from 1 to about 5.
摘要翻译：一种由下式定义的含硫阴离子聚合引发剂：R1S-R2aR3⊖Li⊕其中R1为一价有机基团，R2为二价有机基团，R3为二价有机基团或键，a为1 至约5。

48. 发明授权

US07799870B2 Compounding silica-reinforced rubber with low volatile organic compound (VOC) emission 有权
标题翻译：具有低挥发性有机化合物（VOC）排放的复合二氧化硅增强橡胶
公开(公告)号：US07799870B2
公开(公告)日：2010-09-21
申请号：US11387569
申请日：2006-03-23
申请人： William L. Hergenrother , Chenchy Jeffrey Lin , Terrence E. Hogan , Ashley S. Hilton
发明人： William L. Hergenrother , Chenchy Jeffrey Lin , Terrence E. Hogan , Ashley S. Hilton
IPC分类号： B60C1/00
CPC分类号： C07F7/21 , B60C1/00 , B60C1/0016 , C08G77/28 , C08K3/04 , C08K3/36 , C08K5/5406 , C08K5/5419 , C08K5/548 , C08K5/549 , C08K13/02 , C08L7/00 , C08L9/00 , C08L9/06 , C08L21/00 , C08L83/04 , C08L2205/02 , Y10T152/10 , Y10T152/10846 , Y10T428/2991 , Y10T428/2995 , C08L2666/02 , C08L83/00
摘要： Alkoxy-modified silsesquioxane compounds are described. The alkoxy-modified silsesquioxane compounds contain an alkoxysilane group that participates in an alkoxysilane-silica reaction as a silica dispersing agent in rubber, with the release of zero to about 0.1% by weight of the rubber of volatile organic compounds (VOC), especially alcohol, during compounding and further processing. Further described are methods for making alkoxy-modified silsesquioxanes, methods for making vulcanizable rubber compounds containing alkoxy-modified silsesquioxanes, vulcanizable rubber compounds containing alkoxy-modified silsesquioxanes, and pneumatic tires comprising a component that contains alkoxy-modified silsesquioxanes.
摘要翻译：描述了烷氧基改性的倍半硅氧烷化合物。烷氧基改性的倍半硅氧烷化合物含有作为二氧化硅分散剂参与烷氧基硅烷 - 二氧化硅反应的橡胶中的烷氧基硅烷基，释放出约0.1重量％的挥发性有机化合物（VOC）的橡胶，特别是醇，在复合和进一步加工过程中。还描述了制备烷氧基改性倍半硅氧烷的方法，制备含有烷氧基改性倍半硅氧烷的可硫化橡胶化合物的方法，含有烷氧基改性倍半硅氧烷的可硫化橡胶化合物，以及含有烷氧基改性倍半硅氧烷的组分的充气轮胎。

49. 发明申请

US20080171827A1 AMINE-CONTAINING ALKOXYSILYL-FUNCTIONALIZED POLYMERS 有权
标题翻译：含胺的烷基官能化聚合物
公开(公告)号：US20080171827A1
公开(公告)日：2008-07-17
申请号：US11962221
申请日：2007-12-21
申请人： Terrence E. Hogan , William L. Hergenrother , Maria Tallman
发明人： Terrence E. Hogan , William L. Hergenrother , Maria Tallman
IPC分类号： C08F136/14 , C08F8/30
CPC分类号： C08C19/22 , B60C1/00 , B60C1/0016 , B60C1/0025 , C08C19/25 , C08C19/44 , C08F8/32 , C08F8/42 , C08L15/00
摘要： An amine-containing alkoxysilyl-functionalized polymer, a method of preparing a reactive polymer functionalized with an alkoxysilane functionalizing agent and further reacted with an amino alcohol, the resulting polymer, and vulcanizates thereof.
摘要翻译：含胺的烷氧基甲硅烷基官能化聚合物，制备用烷氧基硅烷官能化剂官能化的反应性聚合物的方法，并进一步与氨基醇反应，得到的聚合物和硫化产物。

50. 发明授权

US06630535B1 Rubber compositions & vulcanizates including comb polymers 失效
标题翻译：橡胶组合物和硫化胶，包括梳形聚合物
公开(公告)号：US06630535B1
公开(公告)日：2003-10-07
申请号：US09642497
申请日：2000-08-18
申请人： Terrence E. Hogan , James A. Krom , James E. Hall , Xiaorong Wang , Peyman Pakdel , William L. Hergenrother
发明人： Terrence E. Hogan , James A. Krom , James E. Hall , Xiaorong Wang , Peyman Pakdel , William L. Hergenrother
IPC分类号： C08L5100
CPC分类号： C08L51/003 , C08L51/04 , C08L2666/02 , C08L2666/04
摘要： A composition comprising an elastomer, a filler, and a comb-like polymer, the comb-like polymer comprising a backbone and a plurality of side chains, the backbone having a length greater than or equal to the entanglement length, the side chains having a length greater than about 33% of the entanglement length, the backbone including at least one side chain per entanglement length, and the comb-like polymer having a Tg of less than −5° C.
摘要翻译：包含弹性体，填料和梳状聚合物的组合物，所述梳状聚合物包含骨架和多个侧链，主链具有大于或等于缠结长度的长度，侧链具有长度大于缠结长度的约33％，骨架包括每个缠结长度的至少一个侧链，并且梳状聚合物的Tg小于-5℃。

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