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41. 发明授权

US4329148A Dye mixtures, and their use in dyeing polyesters 失效
标题翻译：染料混合物及其在染色聚酯中的应用
公开(公告)号：US4329148A
公开(公告)日：1982-05-11
申请号：US222926
申请日：1981-01-06
申请人： Guenter Hansen , Wolf-Dieter Kermer , Jochen-Wilfried Stuck
发明人： Guenter Hansen , Wolf-Dieter Kermer , Jochen-Wilfried Stuck
IPC分类号： C09B29/08 , C09B67/22 , C09B27/00 , C09B45/48 , D06P1/18
CPC分类号： C09B67/0051 , C09B29/081 , C09B29/0823 , C09B29/0828
摘要： Dye mixtures, containing dyes of the formula I ##STR1## where X is hydrogen, chlorine or bromine,R.sup.1 is hydrogen, methoxy, ethoxy or phenoxy,R.sup.2 is hydrogen, methyl, ethyl, n-propyl or iso-propyl andR is ##STR2## where R.sup.3 is allyl, methallyl, crotonyl, prenyl or benzyl,R.sup.4 is C.sub.1 -C.sub.5 -alkyl, allyl, methallyl, crotonyl, prenyl or benzyl andR.sup.4 is C.sub.1 -C.sub.5 -alkyl,the mixtures containing not less than 60% of dyes wherein R is ##STR3## or NHC.sub.2 H.sub.4 CN, from 0 to 40% of one or more dyes wherein R is ##STR4## and from 0 to 40% of one or more dyes wherein R is ##STR5## the two last-mentioned components accounting for not less than 5% of the mixture.The mixtures are exceptionally useful for dyeing polyesters.
摘要翻译：含有式I的染料的染料混合物，其中X是氢，氯或溴，R1是氢，甲氧基，乙氧基或苯氧基，R2是氢，甲基，乙基，正丙基或异丙基，R是其中R 3是烯丙基，甲代烯丙基，巴豆基，异戊烯基或苄基，R 4是C 1 -C 5 - 烷基，烯丙基，甲代烯丙基，巴豆基，异戊烯基或苄基，R 4是C 1 -C 5烷基，所述混合物含有不少于60％的染料，其中R是或NHC 2 H 4 CN，0至40％的一种或多种染料，其中R是一种或多种染料，其中R是两个最后提到的组分占不少于5％的混合物。该混合物特别适用于染色聚酯。

42. 发明授权

US4321055A Navy dye mixtures and their use in dyeing polyesters 失效
标题翻译：海军染料混合物及其在染色聚酯中的应用
公开(公告)号：US4321055A
公开(公告)日：1982-03-23
申请号：US222923
申请日：1981-01-06
申请人： Guenter Hansen , Wolf-Dieter Kermer , Hans J. Kolbinger
发明人： Guenter Hansen , Wolf-Dieter Kermer , Hans J. Kolbinger
IPC分类号： C09B29/08 , C09B67/22 , C09B29/00
CPC分类号： C09B67/0051 , C09B29/0813 , C09B29/0823 , Y10S534/01
摘要： Dye mixtures containing dyes of the formula I ##STR1## where X is hydrogen, chlorine or bromine,R.sup.1 is hydrogen, methoxy, ethoxy or phenoxy,R.sup.2 is hydrogen, methyl, ethyl, n-propyl or i-propyl andR is ##STR2## where R.sup.3 is C.sub.1 -C.sub.5 -alkyl, allyl, methallyl, crotonyl, prenyl or benzyl,R.sup.4 is unsubstituted or phenyl- or phenoxy-substituted straight-chain or branched C.sub.1 -C.sub.8 -alkyl which may be interrupted by 1, 2 or 3 0 atoms, or is C.sub.3 -C.sub.5 -alkenyl, unsubstituted or chlorine-, bromine-, C.sub.1 -C.sub.4 -alkyl- or C.sub.1 -C.sub.4 -alkoxy-substituted phenyl or benzyl,the mixtures containing not less than 40% of dyeswherein R is ##STR3## or NHC.sub.2 H.sub.4 CN, from 0 to 20% of one or more dyes wherein R is ##STR4## and from 10 to 60% of one or more dyes wherein R is ##STR5##
摘要翻译：含有式I的染料的染料混合物，其中X是氢，氯或溴，R1是氢，甲氧基，乙氧基或苯氧基，R2是氢，甲基，乙基，正丙基或异丙基，R是< 其中R 3是C 1 -C 5 - 烷基，烯丙基，甲代烯丙基，巴豆基，异戊烯基或苄基，R 4是未取代的或苯基或苯氧基取代的直链或支链C 1 -C 8 - 烷基，其可被1,2或或者是C3-C5-烯基，未取代的或氯 - ，溴 - ，C1-C4-烷基 - 或C1-C4-烷氧基取代的苯基或苄基，所述混合物含有不少于40％的染料，其中R 是一种或多种染料的0至20％，其中R是“IMAGE”，或10至60％的一种或多种染料，其中R是或NHC2H4CN，

43. 发明授权

US5270456A Azo dyes with A2-aminothiophene dye azo component and a coupling component and coupling component of the diphenylamine series 失效
标题翻译：偶氮染料与A 2-氨基噻吩染料偶氮组分和偶联组分和二苯胺系列的偶联组分
公开(公告)号：US5270456A
公开(公告)日：1993-12-14
申请号：US727881
申请日：1991-07-10
申请人： Erwin Hahn , Guenter Hansen , Karl-Heinz Etzbach , Helmut Reichelt , Ernst Schefczik , Sabine Greuttner , Helmut Degen
发明人： Erwin Hahn , Guenter Hansen , Karl-Heinz Etzbach , Helmut Reichelt , Ernst Schefczik , Sabine Greuttner , Helmut Degen
IPC分类号： C09B29/09 , C09B29/00 , C09B29/08 , C09B43/32 , C09B43/40 , C09B29/033 , D06P1/18 , D06P3/54
CPC分类号： C09B29/081 , C09B29/0059 , C09B29/0811 , C09B43/325 , C09B43/40 , Y10S8/922
摘要： Thiopheneazo dye I which are chiefly useful as disperse dyes for dyeing textile material, in particular polyesters, have the formula ##STR1## where the substituents are as defined in the description.
摘要翻译：主要用作染色纺织材料，特别是聚酯的分散染料的噻吩偶氮染料I具有式（I），其中取代基如说明书中所定义。

44. 发明授权

US5112362A Navy dye mixtures of azo disperse dyes for polyester 失效
标题翻译：用于聚酯的AZO分散染料的NAVY DYE混合物
公开(公告)号：US5112362A
公开(公告)日：1992-05-12
申请号：US679100
申请日：1991-04-02
申请人： Erwin Hahn , Guenter Hansen , Gunther Lamm , Helmut Reichelt , Gerhard Wagenblast
发明人： Erwin Hahn , Guenter Hansen , Gunther Lamm , Helmut Reichelt , Gerhard Wagenblast
IPC分类号： C09B67/22 , D06P3/54
CPC分类号： C09B67/0051 , Y10S8/922
摘要： Dye mixtures useful for dyeing or printing synthetic fabrics contain at least one azo dye whose diazo component is 2-amino-3,5-dicyano-4-methylthiophene and whose coupling component comes from the 2-amino-4-thienylthiazole series and also at least one azo dye whose diazo component is 2-amino-3,5-dicyano-4-methylthiophene, 2-amino-3-alkoxycarbonyl-5-cyano-4-methylthiophene or 2-amino-5-alkoxycarbonyl-3-cyano-4-methylthiophene and whose coupling component comes from the 3-cyano-4-methyl-2,6-diaminopyridine series, and/or at least one azo dye whose diazo component is a 2,6-dicyano-4-alkylaniline and whose coupling component comes from the m-phenylenediamine series.
摘要翻译：用于染色或印刷合成织物的染料混合物含有至少一种重氮组分为2-氨基-3,5-二氰基-4-甲基噻吩并且其偶联组分来自2-氨基-4-噻吩噻唑系列的偶氮染料，二偶氮组分为2-氨基-3,5-二氰基-4-甲基噻吩，2-氨基-3-烷氧基羰基-5-氰基-4-甲基噻吩或2-氨基-5-烷氧基羰基-3-氰基-4-甲基噻吩的至少一种偶氮染料， 4-甲基噻吩，其偶联成分来自3-氰基-4-甲基-2,6-二氨基吡啶系列，和/或至少一种重氮组分为2,6-二氰基-4-烷基苯胺的偶氮染料，其偶合组分来自间苯二胺系列。

45. 发明授权

US4994564A Azo dyes with a diazo component of the 3-amino thiophene series and a coupling component of the pyridine, pyridone or pyrazole series 失效
标题翻译：具有3-氨基噻吩系列的重氮组分的偶氮染料和吡啶，吡啶酮或吡唑系的偶联组分
公开(公告)号：US4994564A
公开(公告)日：1991-02-19
申请号：US269646
申请日：1988-11-10
申请人： Karl-Heinz Etzbach , Helmut Reichelt , Guenter Hansen , Ernst Schefczik , Helmut Hagen , Gunther Lamm
发明人： Karl-Heinz Etzbach , Helmut Reichelt , Guenter Hansen , Ernst Schefczik , Helmut Hagen , Gunther Lamm
IPC分类号： C09B29/09 , C09B29/00 , C09B29/42 , C09B29/48
CPC分类号： C09B29/0059 , C09B29/3621 , C09B29/3634 , C09B29/3656
摘要： Thien-3-ylazo dyes of the formula: ##STR1## where X is cyano, nitro, C.sub.1 -C.sub.6 -alkanoyl, substituted or unsubstituted benzoyl, substituted or unsubstituted phenyl or the radical COOR.sup.1 or CONR.sup.1 R.sup.2 where R.sup.1 and R.sup.2 are identical or different and each is independently of each other substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl, C.sub.5 -C.sub.7 -cycloalkyl, C.sub.3 -C.sub.4 -alkenyl, substituted or unsubstituted phenyl or together with the nitrogen atom linking them a 5- or 6-membered saturated heterocyclic radical, and R.sup.2 may additionally be hydrogen, Y is hydrogen, cyano, C.sub.1 -C.sub.6 -alkanoyl, substituted or unsubstituted benzoyl, C.sub.1 -C.sub.4 -alkylsulfonyl, substituted or unsubstituted phenylsulfonyl, substituted or unsubstituted phenyl or the radical COOR.sup.1 or CONR.sup.1 R.sup.2 where R.sup.1 and R.sup.2 are each as defined above, Z is hydrogen, substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl, substituted or unsubstituted phenyl, substituted or unsubstituted C.sub.1 -C.sub.6 -alkylthio, substituted or unsubstituted phenylthio, substituted or unsubstituted C.sub.1 -C.sub.6 -alkylsulfonyl or phenylsulfonyl or together with the radical Y a fused benzo ring which may be substituted, and K is the radical of a coupling component of the 2,6-diaminopyridine, 6-hydroxypyrid-2-one or 5-aminopyrazole series, are used for dyeing synthetic fiber materials, in particular synthetic polyesters, in yellow to red shades and are notable for good light fastness, fastness to dry heat setting and pleating and for good affinity.
摘要翻译：噻吩-3-基偶氮染料，其结构式如下：其中X为氰基，硝基，C 1 -C 6烷酰基，取代或未取代的苯甲酰基，取代或未取代的苯基或基团COOR1或CONR1R2，其中R 1和R 2相同或不同，各自独立地为取代或未取代的C 1 -C 8 - 烷基，C 5 -C 7 - 环烷基，C 3 -C 4 - 烯基，取代或未取代的苯基或与连接它们的氮原子一起形成5-或6-元饱和杂环基， R 2可另外为氢，Y为氢，氰基，C 1 -C 6烷酰基，取代或未取代的苯甲酰基，C 1 -C 4 - 烷基磺酰基，取代或未取代的苯基磺酰基，取代或未取代的苯基或基团COOR1或CONR1R2，其中R1和R2为 Z是氢，取代或未取代的C 1 -C 8 - 烷基，取代或未取代的苯基，取代或未取代的C 1 -C 6 - 烷硫基，取代或未取代的苯硫基，取代或未取代的C 1 -C 6 - 烷基磺酰基或与苯基磺酰基或与基团Y一起可以被取代的稠合苯并环，K是2,6-二氨基吡啶，6-羟基吡啶-2-酮或5-氨基吡唑系列的偶联组分的基团用于将合成纤维材料，特别是合成聚酯染色为黄色至红色，并且具有良好的耐光性，耐干燥定型和打褶的牢度以及良好的亲和力。

46. 发明授权

US4952681A Dyes containing 3,4-disubstituted-2-diaza-thiophene radicals 失效
标题翻译：含有3,4-取代-2-二氮杂-苯并呋喃的染料
公开(公告)号：US4952681A
公开(公告)日：1990-08-28
申请号：US205359
申请日：1988-07-27
申请人： Guenter Hansen , Ernst Schefczik , Karl-Heinz Etzbach , Helmut Reichelt , Hermann Loeffler
发明人： Guenter Hansen , Ernst Schefczik , Karl-Heinz Etzbach , Helmut Reichelt , Hermann Loeffler
IPC分类号： C09B29/00 , C09B62/35 , C09B29/033 , C09B29/33 , C09B29/36
CPC分类号： C09B29/0059
摘要： Compounds of the formula I ##STR1## where X is fluorine, chlorine, bromine, SO.sub.2 E or unsubstituted or substituted hydroxyl or mercapto, E is alkyl, alkenyl, cycloalkyl, aralkyl, aryl, chlorine or unsubstituted or substituted hydroxyl or amino, Y is cyano, nitro, alkanoyl, aroyl, alkylsulfonyl, arylsulfonyl, carboxyl, a carboxylic ester group or unsubstituted or substituted carbamyl, T is hydrogen, C.sub.1 -C.sub.4 -alkyl, a radical which can be introduced by electrophilic substitution or a radical of the formula --CH.dbd.B, in which B is a radical of a methylene-active compound or of an amine, and K is a radical of a coupling component, are disclosed. They are useful for dyeing synthetic fibers or plastics.
摘要翻译： 1.式I的化合物参见图示：EP0201896，P71，F3，其中X是氟，氯，溴，SO2E，OH，OCH3，OC2H5，OC3H7，OC4H9，OCH2 C6H5，OC6H11，OC6H5 ，OC 6 H 4 CH 3，OC 6 H 4 Cl，SH，SCH 3，SC 2 H 5，SC 3 H 7，SC 4 H 9，SCH 2 C 6 H 5，SC 2 H 4 OH，SCH 2 COOCH 3，SCH 2 COOC 2 H 5，SC 6 H 11，SC 6 H 5或SC 6 H 4 CH 2，E是烷基，链烯基，环烷基，芳烷基，芳基，氯，OH，CH3O，C2H5O，C3H7O，C4H9O，C6H5 -CH2O，C6H5 -CH2 -CH2O，C6H5O，CIC6H4O， CH 3 C 4 H 4 O，NH 2，NHCH 3，N（CH 3）2，NHC 2 H 5，N（C 2 H 5）2，NCH 4 H 9，N（C 4 H 9）2，NHC 6 H 5，NHC 6 H 4 -CH 3，NHC 6 H 4 Cl或NCH 3 C 6 H 5 ，Y是氰基，硝基，烷酰基，芳酰基，烷基磺酰基，芳基磺酰基，羧基，羧酸酯基或未取代或取代的氨基甲酰基，T是氢，C 1 -C 4烷基，NO，NO 2，SO 3 H，CHO，CN，，C 2 H 5 CO，C 6 H 5 CO，CH 3 SO 2，C 2 H 5 SO 2，C 6 H 5 SO 2或式-CH = B的基团，其中B是亚甲基活性化合物或胺的基团，K是激进或耦合部件。

47. 发明授权

US4908041A Navy and black dye mixtures: thiophene azo disperse dye and red, yellow or orange disperse dye 失效
标题翻译：海军和黑色染料混合物：噻吩偶氮分散染料和红色，黄色或橙色分散染料
公开(公告)号：US4908041A
公开(公告)日：1990-03-13
申请号：US256997
申请日：1988-10-13
申请人： Erwin Hahn , Guenter Hansen , Karl-Heinz Etzbach , Helmut Reichelt , Ernst Schefczik , Helmut Degen , Reinhold Krallmann , Gerhard Wagenblast
发明人： Erwin Hahn , Guenter Hansen , Karl-Heinz Etzbach , Helmut Reichelt , Ernst Schefczik , Helmut Degen , Reinhold Krallmann , Gerhard Wagenblast
IPC分类号： C09B29/00 , C09B67/22
CPC分类号： C09B67/0041 , C09B29/0059 , Y10S8/922
摘要： Navy and black dye mixtures contain one or more thiophene-azo dyes of the formula ##STR1## where R.sup.1, R.sup.2, R.sup.3, R.sup.4, R.sup.5, X and Y each have defined meanings, and one or more dyes F whose absorption maximum is at a wavelength of from 390 to 520 nm, the proportion of thiophene-azo dyes being from 60 to 99% by weight, based on the total weight of thiophene-azo dyes and dyes F in the mixture.
摘要翻译：海军和黑色染料混合物含有一种或多种式（IMAGE）的噻吩 - 偶氮染料，其中R1，R2，R3，R4，R5，X和Y各自具有定义的含义，以及一种或多种吸收最大值为波长为390-520nm，噻吩 - 偶氮染料的比例为60-99重量％，基于噻吩 - 偶氮染料和染料F在混合物中的总重量。

48. 发明授权

US4751288A Azo dyes containing 2-amino-3-cyano-5-formylthiophene derivatives as diazo components and substituted aniline compounds as coupling components 失效
标题翻译：含有2-氨基-3-氰基-5-甲酰基噻吩衍生物作为重氮组分的偶氮染料和取代的苯胺化合物作为偶联组分
公开(公告)号：US4751288A
公开(公告)日：1988-06-14
申请号：US843397
申请日：1986-03-24
申请人： Udo Bergmann , Erwin Hahn , Guenter Hansen , Helmut Reichelt
发明人： Udo Bergmann , Erwin Hahn , Guenter Hansen , Helmut Reichelt
IPC分类号： C09B29/09 , C09B29/00 , C09B29/033 , C09B29/08 , D06P1/18 , D06P3/54
CPC分类号： C09B29/0809 , C09B29/0059 , C09B29/0808 , Y10S534/02
摘要： The compounds of the formula I ##STR1## where R is unsubstituted or substituted phenyl or naphthyl, R.sup.1 and R.sup.2 are each unsubstituted or substituted alkyl, alkenyl or cycloalkyl, and one of the radicals may furthermore be hydrogen, R.sup.3 is hydrogen, methyl, methoxy, ethoxy or chlorine, and R.sup.4 is acylamino, are particularly useful for dyeing polyesters.
摘要翻译：其中R是未取代或取代的苯基或萘基，R 1和R 2各自为未取代或取代的烷基，链烯基或环烷基，并且其中一个基团可以是氢，R 3是氢，甲基，甲氧基，乙氧基或氯，R4为酰氨基，特别适用于染色聚酯。

49. 发明授权

US4464181A Mixtures of benzisothiazole mono-azo dyes for cellulose acetate 失效
标题翻译：乙酸纤维素的苯并异噻唑单偶氮染料的混合物
公开(公告)号：US4464181A
公开(公告)日：1984-08-07
申请号：US457223
申请日：1983-01-11
申请人： Helmut Degen , Johannes P. Dix , Norbert Grund , Guenter Hansen , Reinhold Krallmann
发明人： Helmut Degen , Johannes P. Dix , Norbert Grund , Guenter Hansen , Reinhold Krallmann
IPC分类号： C09B29/00 , C09B29/08 , C09B67/22
CPC分类号： C09B67/0051 , C09B29/0081 , C09B29/0813 , C09B29/0819 , Y10S534/01 , Y10S8/921
摘要： Dye mixtures which comprise two or more dyes of the formula ##STR1## ps where X is hydrogen, methyl or chlorine, and R is a radical of the formula OR.sup.1, OCOCH.sub.3, OCOC.sub.2 H.sub.5, R.sup.1 being hydrogen or C.sub.1 -C.sub.4 -alkyl, are very useful for dyeing cellulose esters.
摘要翻译：包含两种或更多种式的化合物的染料混合物，其中X是氢，甲基或氯，R是式OR1，OCOCH 3，OCOC 2 H 5，R 1是氢或C 1 -C 4 - 烷基，对染色纤维素酯非常有用。

50. 发明授权

US4405330A Navy disperse dye mixtures 失效
标题翻译：海军分散染料混合物
公开(公告)号：US4405330A
公开(公告)日：1983-09-20
申请号：US433393
申请日：1982-10-08
申请人： Udo Bergmann , Helmut Degen , Guenter Hansen , Reinhold Krallmann , Wolf-Dieter Kermer
发明人： Udo Bergmann , Helmut Degen , Guenter Hansen , Reinhold Krallmann , Wolf-Dieter Kermer
IPC分类号： C09B29/08 , C09B67/22 , D06P3/54 , D06P1/04
CPC分类号： C09B67/0051 , C09B29/081 , C09B29/0813 , Y10S534/01 , Y10S8/922
摘要： Navy mixtures which contain dyes of the formula I ##STR1## where X is chlorine or bromine,Y is hydrogen, methoxy or ethoxy andR is N(C.sub.2 H.sub.5).sub.2, N(CH.sub.2 CH.dbd.CH.sub.2).sub.2 or N(C.sub.2 H.sub.4 OCOCH.sub.3).sub.2,the mixtures being composed of 10-70% of dyes with Y.dbd.H and R=N(C.sub.2 H.sub.5).sub.2, 5-40% of dyes with Y=OCH.sub.3 or OC.sub.2 H.sub.5 and R.dbd.N(CH.sub.2 --CH.dbd.CH.sub.2).sub.2 and 5-80% of dyes with Y=OCH.sub.3 or OC.sub.2 H.sub.5 and R=N(C.sub.2 H.sub.4 OCOCH.sub.3).sub.2.The novel mixtures have excellent tinctorial properties and give very fast dyeings on synthetic polyesters.
摘要翻译：含有式I的染料的海军混合物，其中X是氯或溴，Y是氢，甲氧基或乙氧基，R是N（C2H5）2，N（CH2CH = CH2）2或N（C2H4OCOCH3）2，该混合物由10-70％的具有Y = H和R = N（C 2 H 5）2的染料组成，5-40％的具有Y = OCH 3或OC 2 H 5和R = N（CH 2 -CH 2 CH 2）2和5 -80％的具有Y = OCH 3或OC 2 H 5和R = N（C 2 H 4 OCOCH 3）的染料。新型混合物具有优异的着色性能，并在合成聚酯上产生非常快的染色。

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