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31. 发明申请

US20050095203A1 Photoactive lanthanide complexes with phosphine oxides, phosphine oxide-sulfides, pyridine N-oxides, and phosphine oxide-pyridine N-oxides, and devices made with such complexes 审中-公开
公开(公告)号：US20050095203A1
公开(公告)日：2005-05-05
申请号：US11011699
申请日：2004-12-14
申请人： Vladimir Grushin , Norman Herron , Viacheslav Petrov , Nora Radu , Ying Wang
发明人： Vladimir Grushin , Norman Herron , Viacheslav Petrov , Nora Radu , Ying Wang
IPC分类号： H01L51/50 , C07C49/92 , C07D213/26 , C07D213/89 , C07D217/08 , C07F5/00 , C07F9/53 , C07F19/00 , C09K11/06 , A61K49/00 , A61K31/555
CPC分类号： C09K11/06 , C07F9/5345 , C09K2211/10 , C09K2211/1003 , C09K2211/1007 , C09K2211/1011 , C09K2211/1014 , C09K2211/1018 , C09K2211/1029 , C09K2211/1044 , C09K2211/182 , Y10S428/917
摘要： The present invention is generally directed to luminescent lanthanide compounds with phosphine oxide, phosphine oxide-sulfide, pyridine N-oxide, and phosphine oxide-pyridine N-oxide ligands. It also relates to electronic devices in which the active layer includes a lanthanide complex.

32. 发明授权

US09676795B2 Process to obtain a trifluoromethylating composition 有权
公开(公告)号：US09676795B2
公开(公告)日：2017-06-13
申请号：US14000116
申请日：2012-02-17
申请人： Vladimir Grushin , Alessandro Zanardi
发明人： Vladimir Grushin , Alessandro Zanardi
IPC分类号： C07F1/08 , C07B39/00 , C07C17/32 , C07C201/12 , C07F1/00 , C07C41/30 , C07C45/45 , C07C45/68
CPC分类号： C07F1/08 , C07B39/00 , C07C17/32 , C07C41/30 , C07C45/455 , C07C45/68 , C07C201/12 , C07F1/005 , C07C22/08 , C07C205/11 , C07C43/225 , C07C49/80
摘要： Process to obtain a trifluoromethylating composition which comprises the reaction between a copper (I) source and a base in the presence of a solvent and between the resulting cuprating reagent with fluoroform.

33. 发明授权

US08212075B2 Process for preparing 2-amino-5-cyanobenzoic acid derivatives 有权
标题翻译：制备2-氨基-5-氰基苯甲酸衍生物的方法
公开(公告)号：US08212075B2
公开(公告)日：2012-07-03
申请号：US12741635
申请日：2008-11-07
申请人： Vladimir Grushin , Albert Loren Casalnuovo
发明人： Vladimir Grushin , Albert Loren Casalnuovo
IPC分类号： C07C231/12
CPC分类号： C07C253/14 , C07D231/14 , C07D401/04 , C07F17/02 , C07C255/58
摘要： Disclosed is a method for preparing a compound of Formula 1 comprising contacting a compound of Formula 2 with at least one alkali metal cyanide of Formula 3 and a compound of Formula 4. wherein R1 is NHR3 or OR4; R2 is CH3 or Cl; R3 is H, C1-C4 alkyl, cyclopropyl, cyclopropylcyclopropyl, cyclopropylmethyl or methylcyclopropyl; R4 is H or C1-C4 alkyl; X is Br, Cl or I; and R5, R6, R7, R8, R9 and R10 are as defined in the disclosure.Also disclosed is a method for preparing a compound of Formula 4 wherein R9 and R10 together are a cycloalkadiene bidentate ligand, comprising contacting a compound of Formula 5 wherein Y is Cl, Br or I, with a cycloalkadiene bidentate ligand, at least one metal reducing agent and a nitrile solvent.Also disclosed is a method for preparing a compound of Formula 1 comprising preparing a compound of Formula 4 by contacting a compound of Formula 5 with a cycloalkadiene bidentate ligand and at least one metal reducing agent, and then contacting the reaction mixture comprising the compound of Formula 4 with a compound of Formula 2 and at least one alkali metal cyanide of Formula 3; and further disclosed is a method for preparing a compound of Formula 6 wherein R15, R16, R17 and Z are as defined in the disclosure using a compound of Formula 1, characterized by preparing the compound of Formula 1 by a method disclosed above.
摘要翻译：公开了制备式1化合物的方法，包括使式2的化合物与至少一种式3的碱金属氰化物和式4的化合物接触，其中R 1是NHR 3或OR 4; R2是CH3或Cl; R3是H，C1-C4烷基，环丙基，环丙基环丙基，环丙基甲基或甲基环丙基; R4是H或C1-C4烷基; X是Br，Cl或I; 并且R5，R6，R7，R8，R9和R10如本公开所定义。还公开了制备式4化合物的方法，其中R 9和R 10一起是环二烯二齿配体，包括使式5的化合物，其中Y是Cl，Br或I与环二烯二齿配体，至少一种金属还原助剂和腈溶剂。还公开了制备式1化合物的方法，包括通过使式5的化合物与环二烯二齿配体和至少一种金属还原剂接触来制备式4的化合物，然后使包含式 4与式2的化合物和至少一种式3的碱金属氰化物反应; 并且进一步公开了制备式6化合物的方法，其中R 15，R 16，R 17和Z如本公开中所定义，使用式1化合物，其特征在于通过上述方法制备式1化合物。

34. 发明授权

US07887779B2 Process for making anatase titanium (IV) oxide 有权
标题翻译：锐钛型氧化钛（IV）的制备方法
公开(公告)号：US07887779B2
公开(公告)日：2011-02-15
申请号：US12515762
申请日：2007-12-20
申请人： David M. Scott , Carmine Torardi , Vladimir Grushin
发明人： David M. Scott , Carmine Torardi , Vladimir Grushin
IPC分类号： B01J23/00
CPC分类号： C01G23/047 , B82Y30/00 , C01G23/053 , C01P2002/70 , C01P2002/84 , C01P2004/51 , C01P2004/64 , C01P2006/22 , C09C1/3661
摘要： The disclosure pertains to a process for making anatase titanium dioxide particles, comprising: vigorously mixing (a) a volume of a first component comprising a major proportion of an alcohol, a minor proportion of a titanium alkoxide and a minor proportion of a titanium alkoxide activator selected from the group consisting of water and a first aqueous base, and (b) a second component selected from the group consisting of water and a second aqueous base, at least one of the first component or the second component having, a base therein, the second component being substantially free of alcohol, to form a mixture comprising a suspension of finely divided titanium (IV) oxide particles, the mixture having a water to titanium molar ratio ranging from about 40 to about 1 to about 5000 to about 1, wherein the proportion of the titanium alkoxide, the proportion of the activator, the mixing vigor, and a ratio of the volume of the first component to the second component are effective for the suspension of the finely divided titanium (IV) oxide particles to form in the mixture; and heating the suspension to convert the titanium (IV) oxide particles of the suspension to anatase titanium dioxide.
摘要翻译：本公开涉及制备锐钛型二氧化钛颗粒的方法，其包括：剧烈混合（a）一定体积的第一组分，其包含主要部分的醇，少部分的钛醇盐和少部分的钛醇盐活化剂选自水和第一含水碱，和（b）选自水和第二水性碱的第二组分，所述第一组分或第二组分中的至少一种具有其中的碱，所述第二组分基本上不含醇，以形成包含细碎的氧化钛（IV）颗粒的悬浮液的混合物，所述混合物的水与钛的摩尔比为约40至约1至约5000至约1，其中钛醇盐的比例，活化剂的比例，混合活度以及第一组分与第二组分的体积比对于sus是有效的在混合物中形成细碎的氧化钛（IV）颗粒的养护金; 并加热悬浮液以将悬浮液中的钛（IV）氧化物颗粒转化成锐钛矿二氧化钛。

35. 发明申请

US20110034695A1 PROCESS FOR PREPARING 2-AMINO-5-CYANOBENZOIC ACID DERIVATIVES 有权
标题翻译：制备2-氨基-5-氰基苯甲酸衍生物的方法
公开(公告)号：US20110034695A1
公开(公告)日：2011-02-10
申请号：US12741635
申请日：2008-11-07
申请人： Vladimir Grushin , Albert Loren Casalnuovo
发明人： Vladimir Grushin , Albert Loren Casalnuovo
IPC分类号： C07D401/04 , C07C231/12 , C07F15/04
CPC分类号： C07C253/14 , C07D231/14 , C07D401/04 , C07F17/02 , C07C255/58
摘要： Disclosed is a method for preparing a compound of Formula 1 comprising contacting a compound of Formula 2 with at least one alkali metal cyanide of Formula 3 and a compound of Formula 4. wherein R1 is NHR3 or OR4; R2 is CH3 or Cl; R3 is H, C1-C4 alkyl, cyclopropyl, cyclopropylcyclopropyl, cyclopropylmethyl or methylcyclopropyl; R4 is H or C1-C4 alkyl; X is Br, Cl or I; and R5, R6, R7, R8, R9 and R10 are as defined in the disclosure. Also disclosed is a method for preparing a compound of Formula 4 wherein R9 and R10 together are a cycloalkadiene bidentate ligand, comprising contacting a compound of Formula 5 wherein Y is Cl, Br or I, with a cycloalkadiene bidentate ligand, at least one metal reducing agent and a nitrile solvent.Also disclosed is a method for preparing a compound of Formula 1 comprising preparing a compound of Formula 4 by contacting a compound of Formula 5 with a cycloalkadiene bidentate ligand and at least one metal reducing agent, and then contacting the reaction mixture comprising the compound of Formula 4 with a compound of Formula 2 and at least one alkali metal cyanide of Formula 3; and further disclosed is a method for preparing a compound of Formula 6 wherein R15, R16, R17 and Z are as defined in the disclosure using a compound of Formula 1, characterized by preparing the compound of Formula 1 by a method disclosed above.
摘要翻译：公开了制备式1化合物的方法，包括使式2的化合物与至少一种式3的碱金属氰化物和式4的化合物接触，其中R 1是NHR 3或OR 4; R2是CH3或Cl; R3是H，C1-C4烷基，环丙基，环丙基环丙基，环丙基甲基或甲基环丙基; R4是H或C1-C4烷基; X是Br，Cl或I; 并且R5，R6，R7，R8，R9和R10如本公开所定义。还公开了制备式4化合物的方法，其中R 9和R 10一起是环二烯二齿配体，包括使式5的化合物，其中Y是Cl，Br或I与环二烯二齿配体，至少一种金属还原助剂和腈溶剂。还公开了制备式1化合物的方法，包括通过使式5的化合物与环二烯二齿配体和至少一种金属还原剂接触来制备式4的化合物，然后使包含式 4与式2的化合物和至少一种式3的碱金属氰化物反应; 并且进一步公开了制备式6化合物的方法，其中R 15，R 16，R 17和Z如本公开中所定义，使用式1化合物，其特征在于通过上述方法制备式1化合物。

36. 发明申请

US20100243954A1 PERFLUOROALKYLATED BENZOATE SURFACTANTS 失效
标题翻译：全氟烷基苯甲酸酯表面活性剂
公开(公告)号：US20100243954A1
公开(公告)日：2010-09-30
申请号：US12412408
申请日：2009-03-27
申请人： Vladimir Grushin
发明人： Vladimir Grushin
IPC分类号： C09K3/00 , C07C63/06
CPC分类号： C11D1/004 , C07C63/04 , C07C63/64 , C07C65/21
摘要： Provided are new compounds based on salts of aromatic acids containing perfluoroalkyl substituents. The compounds can be used as surfactants.
摘要翻译：提供了基于含有全氟烷基取代基的芳族酸盐的新化合物。该化合物可用作表面活性剂。

37. 发明申请

US20120123085A1 PROCESSES FOR PREPARING DIACIDS, DIALDEHYDES AND POLYMERS 有权
标题翻译：制备DIACIDS，DIALDEHYDES和聚合物的方法
公开(公告)号：US20120123085A1
公开(公告)日：2012-05-17
申请号：US13357985
申请日：2012-01-25
申请人： Vladimir Grushin , Walter Partenheimer , Leo E. Manzer
发明人： Vladimir Grushin , Walter Partenheimer , Leo E. Manzer
IPC分类号： C08G12/26 , C07D307/02
CPC分类号： C08G65/002 , C07C45/298 , C07D307/36 , C07D307/46 , C07D307/48 , C07D307/68 , C08G6/00
摘要： Alcohols are catalytically oxidized to aldehydes, in particular to benzaldehyde and diformylfuran, which are useful as intermediates for a multiplicity of purposes. The invention also relates to the polymerization of the dialdehyde and to the decarbonylation of the dialdehyde to furan.
摘要翻译：醇被催化氧化成醛，特别是苯甲醛和二甲基呋喃，其可用作多种目的的中间体。本发明还涉及二醛的聚合和二醛对呋喃的脱羰作用。

38. 发明授权

US07858553B2 Suspensions of surface treated titanium (IV) oxides and processes for making them 有权
标题翻译：表面处理的钛（IV）氧化物的悬浮液及其制备方法
公开(公告)号：US07858553B2
公开(公告)日：2010-12-28
申请号：US12515765
申请日：2007-12-20
申请人： David M Scott , Carmine Torardi , Vladimir Grushin
发明人： David M Scott , Carmine Torardi , Vladimir Grushin
IPC分类号： B01J23/00
CPC分类号： C01G23/053 , B82Y30/00 , C01G23/047 , C01P2004/52 , C01P2004/64 , C01P2006/22 , C02F2305/08 , C02F2305/10 , C09C1/3661
摘要： The disclosure relates to a process for making a surface treated suspension of finely divided titanium (IV) oxide particles, typically, finely divided titanium (IV) oxide nanoparticles, comprising: vigorously mixing (a) a volume of a first component comprising a major proportion of alcohol, a minor proportion of titanium alkoxide and a minor proportion of a titanium alkoxide activator selected from the group consisting of water and a first aqueous base, and b) a volume of a second component selected from the group consisting of water and a second aqueous base, at least one of the first component or the second component having a base therein, the second component being substantially free of alcohol, to form a mixture comprising a suspension of finely divided titanium (IV) oxide particle, the mixture having a water to titanium molar ratio ranging from about 40 to about 1 to about 5000 to about 1, wherein the proportion of the titanium alkoxide, the proportion of the activator, the mixing vigor, and the ratio of the volume of the first component to the volume of the second component are effective for the suspension of the finely divided particles to form in the mixture; and treating the suspension with a compound comprising a source of silicon, aluminum or zinc, and products made by the foregoing process. The suspension can be dried to recover a powder.
摘要翻译：本公开涉及一种用于制备精细分离的氧化钛（IV）颗粒（通常为细碎的氧化钛（IV））纳米颗粒的经表面处理的悬浮液的方法，其包括：剧烈混合（a）一定体积的包含主要比例的第一组分的醇，少量的烷氧基钛和少部分选自水和第一含水碱的钛醇盐活化剂，和b）一定体积的第二组分，其选自水和第二组分水性碱，第一组分或第二组分中的至少一种在其中具有碱，第二组分基本上不含醇，以形成包含细碎的氧化钛（IV）颗粒的悬浮液的混合物，该混合物具有水钛摩尔比为约40至约1至约5000至约1，其中钛醇盐的比例，活化剂的比例，混合活性，并且第一组分的体积与第二组分的体积的比率对于在混合物中形成的细碎颗粒的悬浮是有效的; 并用包含硅，铝或锌的源的化合物和通过前述方法制备的产物处理悬浮液。可以将悬浮液干燥以回收粉末。

39. 发明申请

US20060074261A1 Processes for preparing fluoroarenes from haloarenes 失效
标题翻译：从卤代芳烃制备氟代烯烃的方法
公开(公告)号：US20060074261A1
公开(公告)日：2006-04-06
申请号：US11244980
申请日：2005-10-05
申请人： Vladimir Grushin
发明人： Vladimir Grushin
IPC分类号： C07C19/08 , C07C43/18 , C07C209/74
CPC分类号： C07C17/208 , C07B39/00 , C07C25/22 , C07C25/13
摘要： Processes for preparing fluoroarenes are provided. The processes include contacting a compound having an unactivated aryl group with a source of fluoride or bifluoride in the presence of a transition metal a ligand.
摘要翻译：提供制备氟代烯烃的方法。该方法包括在过渡金属配体的存在下使具有未活化芳基的化合物与氟化物或二氟化物源接触。

40. 发明申请

US20050240028A1 Pyrrolyl complexes of copper for copper metal deposition 审中-公开
标题翻译：用于铜金属沉积的铜的吡咯基络合物
公开(公告)号：US20050240028A1
公开(公告)日：2005-10-27
申请号：US10523493
申请日：2003-07-31
申请人： Vladimir Grushin
发明人： Vladimir Grushin
IPC分类号： C07D207/30 , C07D207/32 , C07D207/333 , C07D207/335 , C07F1/08 , C23C16/18 , C23C16/44 , C23C16/455
CPC分类号： C23C16/45553 , C07D207/333 , C07D207/335 , C23C16/18 , C23C16/45525
摘要： The present invention relates to a process for the preparation of ligands and copper complexes useful in the deposition of copper via Atomic Layer Deposition (ALD) and Chemical Vapor Deposition (CVD)), and the use of the copper complexes in ALD and CVD processes.
摘要翻译：本发明涉及一种制备可用于通过原子层沉积（ALD）和化学气相沉积（CVD）沉积铜的配体和铜络合物的方法，以及铜配合物在ALD和CVD工艺中的应用。

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