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21. 发明授权

US4975323A Ferrophosphorus particles treated with hypophosphorous acid 失效
标题翻译：用次磷酸处理的铁磷颗粒
公开(公告)号：US4975323A
公开(公告)日：1990-12-04
申请号：US399130
申请日：1989-08-28
申请人： Donald H. Campbell
发明人： Donald H. Campbell
IPC分类号： C09C1/22 , C09C3/06 , C09D5/24 , H01B1/02 , H01B1/22
CPC分类号： H01B1/02 , C09C1/22 , C09C3/06 , C09D5/24 , H01B1/22 , C01P2004/61 , C01P2004/62 , C01P2006/40 , Y10T428/256 , Y10T428/2991
摘要： The conductivity of ground ferrophosphorus particles is increased by contacting the particles with an aqueous solution of hypophosphorus acid, preferably at a temperature between room temperature and about 50.degree.C. The particles are then washed and dried and can be mixed with resinous binders to formulate coating compositions. The coating compositions are particularly useful for coating galvanized steel that is to be welded.
摘要翻译：通过使颗粒与次磷酸的水溶液接触，优选在室温至约50℃之间的温度下，研磨的磷酸铁颗粒的电导率增加。然后将颗粒洗涤并干燥，并与树脂粘合剂混合以配制涂层组合物。涂料组合物特别适用于涂覆待焊接的镀锌钢板。

22. 发明授权

US4889773A Resistance welding of galvanized steel 失效
标题翻译：镀锌钢板电阻焊
公开(公告)号：US4889773A
公开(公告)日：1989-12-26
申请号：US245483
申请日：1988-11-07
申请人： Donald H. Campbell , Gerald L. Evarts
发明人： Donald H. Campbell , Gerald L. Evarts
IPC分类号： B23K11/16 , B23K11/34 , B23K35/22
CPC分类号： B23K11/34 , B23K35/226 , Y10T428/12049 , Y10T428/12056 , Y10T428/12063 , Y10T428/12139
摘要： A coating for improved resistance welding of galvanized steel parts or sheets comprises a binder, and a metal phosphide pigment, preferably a ferrophosphorus pigment, having a particle size of from about 0.1 to about 30 microns. The pigment can also include up to about 40% by weight of an additional metal such as tin, aluminum or lead, which can be combined with the metal phosphide in pigment form or deposited onto the surface of the particles. The coating can be applied to either the faying or non-faying surfaces of the galvanized steel, or to the resistance welding electrode, and may be removed, if desired, after the welding operation.The advantages of the present invention include a significant reduction in welding current and an increase in the weldability lobe width, a restoration of the dynamic resistance beta peak, and an increase in electrode life.
摘要翻译：用于改进镀锌钢部件或片材的电阻焊接的涂层包括粘合剂和具有约0.1至约30微米的粒度的金属磷化物颜料，优选磷酸铁颜料。颜料还可以包括至多约40重量％的另外的金属如锡，铝或铅，其可以与颜料形式的金属磷化物结合或沉积在颗粒表面上。涂层可以应用于镀锌钢板或电镀焊接电极的焊接表面或非焊接表面，如果需要，可以在焊接操作之后去除涂层。本发明的优点包括焊接电流的显着降低和可焊接凸角宽度的增加，动态电阻β峰的恢复以及电极寿命的增加。

23. 发明授权

US08906507B2 Coating system for achieving excellent MVSS adhesion 有权
标题翻译：涂层系统可实现优异的MVSS粘附力
公开(公告)号：US08906507B2
公开(公告)日：2014-12-09
申请号：US12516836
申请日：2008-02-13
申请人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
发明人： Donald H. Campbell , Gregory G. Menovcik , David J. Santure , Walter H. Ohrbom , Donald St. Aubin , Paul J. Harris
IPC分类号： B32B27/08 , B32B27/40 , C08G18/00 , B05D7/00 , C09D201/02
CPC分类号： B05D7/576 , B05D2202/15 , C09D201/025 , Y10T428/31551 , C08L2666/16
摘要： A coating system includes a clear coat layer and a sealant. The clear coat layer is formed from a clear coat composition that comprises a crosslinkable carbamate-functional resin and an aminoplast. Optionally, the coating system further includes a sub-clear coat layer. The sealant is bonded to the clear coat layer opposite the sub-clear coat layer. Optionally, the coating system further includes a tie coat layer and that is disposed between the sealant and the clear coat layer. An adhesion promoter is present in the clear coat composition in an amount of less than or equal to about 3% by weight based on the total weight of resin solids of the clear coat composition. Further, the adhesion promoter is present in at least one of the sub-clear coat composition and the tie coat composition in an amount sufficient to increase adhesion between the clear coat layer and the sealant.
摘要翻译：涂层系统包括透明涂层和密封剂。透明涂层由透明涂层组合物形成，该组合物包含可交联的氨基甲酸酯官能树脂和氨基塑料。任选地，涂层系统还包括副透明涂层。密封剂粘合到与透明涂层相对的透明涂层。任选地，涂层系统还包括粘结涂层，并且设置在密封剂和透明涂层之间。基于透明涂料组合物的树脂固体的总重量，粘合促进剂以小于或等于约3重量％的量存在于透明涂料组合物中。此外，粘合促进剂以足以增加透明涂层和密封剂之间的粘合力的量存在于至少一种亚透明涂料组合物和粘合涂层组合物中。

24. 发明授权

US07989070B2 Coating composition for achieving excellent MVSS adhesion 有权
标题翻译：用于实现优异的MVSS粘附的涂料组合物
公开(公告)号：US07989070B2
公开(公告)日：2011-08-02
申请号：US11960815
申请日：2007-12-20
申请人： Donald H. Campbell , Gregory G. Menovcik , Timothy S. December
发明人： Donald H. Campbell , Gregory G. Menovcik , Timothy S. December
IPC分类号： C08G18/32
CPC分类号： C09D161/28 , C08G2190/00 , C08L61/28 , C08L75/04 , C09D175/04 , Y10T428/265 , Y10T428/31511 , Y10T428/31551 , Y10T428/31601 , Y10T428/31928 , C08L2666/20 , C08L2666/16
摘要： A coating composition comprises a crosslinkable carbamate-functional resin and an aminoplast. The aminoplast comprises the reaction product of an aldehyde and a melamine. The aminoplast has a content of imino groups of less than or equal to about 10%, a content of alkylol groups of at least about 7%, and a remainder of groups being alkoxyalkyl groups, all based on a total number of reactive sites present in the melamine prior to reaction. A coating system includes a clear coat layer that comprises the reaction product of the crosslinkable carbamate-functional resin and the aminoplast. Threshold adhesion strength, in accordance with MVSS standards, can be achieved between glass and the coating system when the crosslinkable carbamate-functional resin and the specific aminoplast set forth above are reacted to form the clear coat layer, while minimizing problems associated with high viscosity of aminoplasts having a high content of imino groups of greater than 10%.
摘要翻译：涂料组合物包含可交联的氨基甲酸酯官能树脂和氨基塑料。氨基塑料包括醛和三聚氰胺的反应产物。氨基塑料具有小于或等于约10％的亚氨基的含量，至少约7％的羟烷基的含量，剩余的基团是烷氧基烷基，全部基于存在于反应前的三聚氰胺。涂层系统包括透明涂层，其包含可交联的氨基甲酸酯官能树脂与氨基塑料的反应产物。当可交联的氨基甲酸酯官能树脂和上述特定的氨基塑料反应形成透明涂层时，玻璃和涂层体系之间可以实现根据MVSS标准的阈值粘附强度，同时最小化与高粘度具有大于10％的亚氨基的高含量的氨基塑料。

25. 发明授权

US07179861B2 Carbamate functional addition polymers and a method for their preparation 失效
标题翻译：氨基甲酸酯官能加成聚合物及其制备方法
公开(公告)号：US07179861B2
公开(公告)日：2007-02-20
申请号：US10815327
申请日：2004-04-01
申请人： Donald H. Campbell , Donald L. St. Aubin , Walter H. Ohrbom
发明人： Donald H. Campbell , Donald L. St. Aubin , Walter H. Ohrbom
IPC分类号： C08F8/30
CPC分类号： C09D201/025 , C08F222/20 , C08F222/22
摘要： A carbamate or terminal urea functional vinyl polymer is prepared by reacting a compound having an hydroxyl group and a carbamate group, terminal urea group, or a group that can be converted to a carbamate or terminal urea group, with a cyclic carboxylic acid anhydride group to form an ester bond and a free acid group from the anhydride; and reacting the free acid group with a compound having an epoxide group. The cyclic carboxylic acid anhydride group may be pendant to a vinyl polymer, or one of the compound having an hydroxyl group, a compound having the cyclic carboxylic acid anhydride group, and the compound having an epoxide group may have polymerizable ethylenic unsaturation that is polymerized, optionally with one or more copolymerizable monomers to form a vinyl polymer. When the compound having an hydroxyl group has a group that can be converted to a carbamate or terminal urea group, the group is converted to the carbamate or terminal urea group after step (a). The carbamate or terminal urea functional vinyl polymer may be included in a coating composition. The coating composition may be applied to a substrate and cured to form a cured coating on the substrate.
摘要翻译：通过将具有羟基和氨基甲酸酯基的化合物，末端脲基团或可转化为氨基甲酸酯或末端脲基团的化合物与环状羧酸酐基团反应制备氨基甲酸酯或末端脲官能乙烯基聚合物，从酸酐形成酯键和游离酸基团; 并使游离酸基与具有环氧基的化合物反应。环状羧酸酐基可以侧链至乙烯基聚合物，或具有羟基的化合物，具有环状羧酸酐基的化合物和具有环氧基的化合物之间可具有可聚合的烯属不饱和基团，任选地与一种或多种可共聚单体形成乙烯基聚合物。当具有羟基的化合物具有可以转化为氨基甲酸酯或末端脲基团的基团时，在步骤（a）之后将该基团转化为氨基甲酸酯或末端脲基团。氨基甲酸酯或末端脲官能的乙烯基聚合物可以包括在涂料组合物中。涂料组合物可以施加到基底上并固化以在基底上形成固化的涂层。

26. 发明授权

US06858693B2 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
标题翻译：具有改进粘合性的氨基甲酸酯官能树脂，其制备方法以及改进层间粘附性的方法
公开(公告)号：US06858693B2
公开(公告)日：2005-02-22
申请号：US10602852
申请日：2003-06-24
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
IPC分类号： C09D5/00 , C08F8/00 , C08F8/30 , C08F220/00 , C08G18/38 , C08G18/81 , C09D133/00 , C09D157/06 , C09D183/04 , C09D201/02 , C09J5/00 , C08F126/02
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.
摘要翻译：本发明提供氨基甲酸酯官能树脂和包含所述树脂的涂料组合物，其相对于随后施加的膜或涂层具有改善的粘合性。更具体地说，本发明涉及具有每个氨基甲酸酯基团至少250克聚合物的氨基甲酸酯官能加成聚合物，它们以小于35重量％的非官能单体，优选小于20重量％，最优选0至小于10重量％，基于聚合物的总重量。本发明还提供一种制备通过所要求保护的方法制备的氨基甲酸酯官能聚合物和氨基甲酸酯官能聚合物的方法。最后，本发明提供了一种用于改善第一涂料组合物与随后施加的材料的粘附性的方法，以及制备包含涂覆的基材，粘合剂组合物和具有至少一个表面的玻璃的复合材料的方法。

27. 发明授权

US06855789B2 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
公开(公告)号：US06855789B2
公开(公告)日：2005-02-15
申请号：US10348484
申请日：2003-03-25
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce E. Oermann
IPC分类号： C09D5/00 , C08F8/00 , C08F8/30 , C08F220/00 , C08G18/38 , C08G18/81 , C09D133/00 , C09D157/06 , C09D183/04 , C09D201/02 , C09J5/00 , C08F126/02
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.

28. 发明授权

US06696159B2 Carbamate-functional resins having improved adhesion, method of making the same, and method of improving intercoat adhesion 有权
公开(公告)号：US06696159B2
公开(公告)日：2004-02-24
申请号：US10348491
申请日：2003-01-21
申请人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce Oermann
发明人： Donald H. Campbell , Walter H. Ohrbom , Joseph Borst , Michael A. Gessner , Donald L. St. Aubin , Marvin L. Green , Bruce Oermann
IPC分类号： B32B2700
CPC分类号： C08G18/8116 , C08F8/00 , C08F2800/20 , C08F2810/50 , C08G18/3823 , C09D201/025 , Y10T428/31551 , Y10T428/31573 , Y10T428/31645 , C08F2220/325 , C08F220/34 , C08F220/20 , C08F212/08
摘要： The invention provides carbamate-functional resins and coating compositions incorporating said resins that have improved adhesion with respect to subsequently applied films or coatings. More particularly, the invention relates to carbamate-functional addition polymers having at least 250 grams of polymer per carbamate group which are made with less than 35 percent by weight of nonfunctional monomers, preferably with less than 20 percent by weight and most preferably from 0 to less than 10 percent by weight, based on the total weight of the polymer. The invention further provides a method of making a carbamate-functional polymer and carbamate-functional polymers made by the claimed method. Finally, the invention provides a method for improving the adhesion of a first coating composition to a subsequently applied material as well as a method of making a composite comprising a coated substrate, an adhesive composition, and a glass having at least one surface.

29. 发明授权

US06652919B1 Highly scratch-resistant multilayer coat, method for producing and use of the same 失效
标题翻译：高耐刮擦多层涂层，其制造和使用方法
公开(公告)号：US06652919B1
公开(公告)日：2003-11-25
申请号：US09890760
申请日：2001-08-02
申请人： Donald H. Campbell , Hubert Baumgart , Thomas Farwick , Ulrike Röckrath
发明人： Donald H. Campbell , Hubert Baumgart , Thomas Farwick , Ulrike Röckrath
IPC分类号： C08G1810
CPC分类号： B05D7/574 , B05D7/577 , C09D175/04 , Y10T428/31551
摘要： A highly scratch-resistant multicoat paint system on a primed or unprimed substrate, comprising above one another in this order (A) a basecoat, (B) a first clearcoat as intermediate coat, and (C) a second clearcoat as the topmost coat, wherein the second clearcoat (C) is producible from a coating coating material (C) comprising (C1) at least one oligomer and/or polymer containing at least one pendant carbamate and/or allophanate group (c11), especially carbamate group (c11), of the formula: —O—(CO)—NH2—O—(CO)—NH—(CO)—NH2 and (C2) at least one crosslinking agent containing at least two functional groups (c21) which undergo crosslinking reactions with the carbamate group and/or allophanate group (c11); and also a process for producing highly scratch-resistant multicoat systems.
摘要翻译：在底漆或未底漆基材上的高度耐刮擦的多色漆系统，其顺序包括（A）底漆，（B）第一透明涂层作为中间涂层，和（C）作为最上层涂层的第二透明涂层，其中所述第二透明涂层（C）可由包含（C1）至少一种含有至少一个氨基甲酸酯和/或脲基甲酸酯基（c11），特别是氨基甲酸酯基（c11）的至少一种低聚物和/或聚合物的涂层涂料（C），和（C2）至少一种含有至少两个与氨基甲酸酯基和/或脲基甲酸酯基团（c11）发生交联反应的官能团（c21）的交联剂;以及用于生产高耐划伤性的方法多点系统

30. 发明授权

US5726244A Aqueous coating compositions for environmental etch resistant coatings 失效
公开(公告)号：US5726244A
公开(公告)日：1998-03-10
申请号：US513587
申请日：1995-08-10
申请人： John D. McGee , Donald H. Campbell , John W. Rehfuss
发明人： John D. McGee , Donald H. Campbell , John W. Rehfuss
IPC分类号： C08L51/00 , C08G18/80 , C08G81/02 , C08L51/06 , C09D151/00 , C09D151/06 , C09D161/20 , C09D201/02 , C08L33/08
CPC分类号： C09D201/025 , C08G18/8077 , C08G81/021 , C09D161/20 , Y10S525/902 , Y10T428/31855
摘要： Environmental etch resistant coatings are described. The coatings are derived from aqueous, curable coating compositions comprising: (a) a carbamate-functional grafted acrylic polymer that comprises the reaction product of a first acrylic polymer and a second acrylic polymer, with at least one of the first and second acrylic polymers having groups that impart water dispersibility to the grafted acrylic polymer, and at least one of the first and second acrylic polymers having carbamate functionality; and (b) a second component comprising a compound having a plurality of functional groups that are reactive with the carbamate functionality.

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