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21. 发明授权

US5886187A Benzene derivatives having a heterocyclic radical 失效
标题翻译：具有杂环基团的苯衍生物
公开(公告)号：US5886187A
公开(公告)日：1999-03-23
申请号：US983325
申请日：1998-01-26
申请人： Helmut Hagen , Manfred Patsch , Bernd-Peter Walther , Andrea Zamponi
发明人： Helmut Hagen , Manfred Patsch , Bernd-Peter Walther , Andrea Zamponi
IPC分类号： C07D271/06 , C09B62/503 , C07D271/107 , C07D285/08 , C07D285/12
CPC分类号： C07D271/06 , C09B62/503
摘要： Benzene derivatives of the formula ##STR1## wheren is 0, 1 or 2,x is nitro or amino,Z is a direct bond or unsubstituted or substituted C.sub.1 -C.sub.6 -alkylene,Y is vinyl or a radical of the formula C.sub.2 H.sub.4 --Q, where Q is hydroxyl or a group which can be removed under alkaline reaction conditions,R.sup.1 and R.sup.2 are hydrogen, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, halogen, nitro, amino, hydroxysulfonyl or a radical of the formula Z--S(O).sub.n --Y, where n, Z and Y have the abovementioned meanings, andHet is the radical of a heterocyclic ring, are described.
摘要翻译： PCT No.PCT / EP96 / 03224 371日期1998年1月26日 102（e）1998年1月26日PCT PCT 1996年7月22日PCT公布。公开号WO97 / 05124 日期：1997年2月13日具有式（I）的式（I）的苯衍生物，其中n是0,1或2，x是硝基或氨基，Z是直接键或未取代或取代的C 1 -C 6亚烷基，Y是乙烯基或式C2H4-Q的基团，其中Q是羟基或可在碱性反应条件下除去的基团，R 1和R 2是氢，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，卤素，硝基，氨基，羟基磺酰基或描述了式ZS（O）nY的基团，其中n，Z和Y具有上述含义，Het是杂环的基团。

22. 发明授权

US5625089A Aniline derivatives 失效
标题翻译：苯胺衍生物
公开(公告)号：US5625089A
公开(公告)日：1997-04-29
申请号：US608198
申请日：1996-02-28
申请人： Manfred Patsch
发明人： Manfred Patsch
IPC分类号： C07C317/36 , C07C317/40 , C07C317/48 , C07C305/24 , C07C317/14
CPC分类号： C07C317/36 , C07C317/40
摘要： Anilines of the formula ##STR1## where rings A and B may each be benzofused,X is a bridge member,R.sup.1 and R.sup.2 are each hydrogen, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, halogen, hydroxysulfonyl, carboxyl, C.sub.1 -C.sub.4 -alkoxycarbonyl or C.sub.1 -C.sub.4 -alkylsulfonyl,R.sup.3 is hydrogen, amino, C.sub.1 -C.sub.4 -alkanoylamino or nitro, andY is vinyl or a radical of the formula C.sub.2 H.sub.4 --Q, where Q is a group detachable under alkaline reaction conditions.
摘要翻译：其中环A和B可以各自为苯并稠合的式“IMAGE”的苯胺，X为桥基，R1和R2各自为氢，C1-C4烷基，C1-C4-烷氧基，卤素，羟基磺酰基，羧基，C1- C 4 - 烷氧基羰基或C 1 -C 4 - 烷基磺酰基，R 3是氢，氨基，C 1 -C 4 - 烷酰基氨基或硝基，Y是乙烯基或式C 2 H 4 -Q基团，其中Q是在碱性反应条件下可分离的基团。

23. 发明授权

US5488127A Aminophenols useful as intermediates for formazan reactive dyes 失效
标题翻译：氨基酚可用作甲an活性染料的中间体
公开(公告)号：US5488127A
公开(公告)日：1996-01-30
申请号：US407956
申请日：1995-03-22
申请人： Claus Marschner , Manfred Patsch
发明人： Claus Marschner , Manfred Patsch
IPC分类号： C07C323/44 , C07C317/28 , C07D295/20 , C09B62/018 , C09B62/44 , C09B62/503
CPC分类号： C09B62/4401 , C07C317/28 , C09B62/018 , C09B62/5036
摘要： There are described formazan dyes of the formula ##STR1## where m and n are each 1 or 2,Kat.sup..sym. is the equivalent of a cation,Me is copper or nickel,X is oxygen or a radical of the formula CO--O or SO.sub.2 --0,Y is vinyl or a radical of the formula C.sub.2 H.sub.4 --Q, wherein Q is a group that is detachable under alkaline reaction conditions,E is a fiber-reactive radical,the rings A and B may be substituted and benzofused, andthe ring C may be substituted,the use thereof for dyeing or printing hydroxyl- or nitrogen-containing organic substrates, novel aminophenols and a process for preparing same.
摘要翻译：描述了式IMAMA的甲an染料，其中m和n各自为1或2，Kat（+）为阳离子的当量，Me为铜或镍，X为氧或式CO-O基团或SO 2 -O，Y为乙烯基或式C 2 H 4 -Q基团，其中Q为在碱性反应条件下可分离的基团，E为纤维反应性基团，环A和B可以被取代和苯并，并且环C可以被取代，其用于染色或印刷羟基或含氮有机底物，新型氨基苯酚及其制备方法的用途。

24. 发明授权

US5449762A Phenylazo- or naphthylazobenzenes having thioether groups 失效
标题翻译：具有硫醚基团的苯基或萘基偶氮苯
公开(公告)号：US5449762A
公开(公告)日：1995-09-12
申请号：US382180
申请日：1995-02-01
申请人： Matthias Wiesenfeldt , Bernd Siegel , Manfred Patsch
发明人： Matthias Wiesenfeldt , Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/513 , C07D251/50 , C09B62/09 , C09B62/44 , D06P1/38
CPC分类号： C09B62/09 , C07D251/50 , C09B62/4411 , C09B62/4415
摘要： Reactive dyes of the formula I ##STR1## where n is 0 or 1R.sup.1, R.sup.2 and R.sup.3 are in each case hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,R.sup.4 is fluorine, chlorine, bromine, C.sub.1 -C.sub.4 -alkylsulfonyl, phenylsulfonyl or a radical of the formula ##STR2## L is a bridge member, A is unsubstituted or substituted C.sub.2 -C.sub.8 -alkylene,Y is vinyl or a radical of the formula --CH.sub.2 --CH.sub.2 --Q, Q being a group which can be removed under alkaline reaction conditions, andD is phenyl or naphthyl, it being possible for these radicals to be substituted, and a process for preparing reactive dyes by oxidation of the abovementioned compounds are described.
摘要翻译：式I的反应性染料，其中n为0或1，R 1，R 2和R 3各自为氢，C 1 -C 4 - 烷基或苯基，R 4为氟，氯，溴，C 1 -C 4 - 烷基磺酰基，苯基磺酰基或下式的基团是桥连基团，A是未取代的或取代的C 2 -C 8 - 亚烷基，Y是乙烯基或式-CH 2 -CH 2 -Q基，Q是可以在碱性反应条件下除去，D是苯基或萘基，这些基团可以被取代，并描述了通过氧化上述化合物制备活性染料的方法。

25. 发明授权

US5410027A Method of preparing fiber-reactive formazan dyes involving hydrolysis of a formyl amino moiety 失效
标题翻译：制备涉及甲酰氨基部分水解的纤维反应性甲an染料的方法
公开(公告)号：US5410027A
公开(公告)日：1995-04-25
申请号：US74608
申请日：1993-06-11
申请人： Claus Marschner , Manfred Patsch
发明人： Claus Marschner , Manfred Patsch
IPC分类号： C07C233/43 , C09B62/04 , C09B62/44 , D06P1/382 , C09B62/018 , C09B43/16 , C09B50/00 , C09B62/038
CPC分类号： C09B62/4407 , C07C233/43 , C09B62/046 , Y02P20/55
摘要： Fiber-reactive formazan dyes are prepared by diazotizing a protectively formylated hydroxyphenylenediamine, coupling with a hydrazone compound, metallizing, eliminating the protective group, and reacting with a halotriazine and optionally thereafter with an amine or a hydroxy compound via novel aminophenol intermediates.
摘要翻译：通过将保护性甲酰化羟基苯二胺重氮化，与腙化合物偶合，金属化，除去保护基，并与卤代三嗪反应，然后任选地通过新的氨基苯酚中间体与胺或羟基化合物反应制备纤维反应性甲an染料。

26. 发明授权

US5391719A Preparation of aminoformazans 失效
标题翻译：氨基甲苯胺的制备
公开(公告)号：US5391719A
公开(公告)日：1995-02-21
申请号：US79926
申请日：1993-06-23
申请人： Matthias Wiesenfeldt , Klaus Pandl , Manfred Patsch
发明人： Matthias Wiesenfeldt , Klaus Pandl , Manfred Patsch
IPC分类号： C09B50/00 , C09B62/04 , C09B50/10 , C09B62/018 , C09B62/038
CPC分类号： C09B50/00 , C09B62/046
摘要： A process for preparing metal aminoformazans by alkaline hydrolysis of the corresponding acylated amino derivates in aqueous medium, is described, the hydrolysis being carried out at from 120.degree. to 170.degree. C. and from 3 to 5 bar in the presence of from 1.5 to 3 mol of an alkali metal hyroxide, based on 1 mol of acylated aminoformazan.
摘要翻译：描述了通过在水性介质中碱性水解相应的酰化氨基衍生物制备金属氨基甲缩醛的方法，水解在120-170℃和3至5巴下在1.5至3的存在下进行基于1摩尔酰化氨基甲的碱金属氢氧化物。

27. 发明授权

US5245020A Reactive dyes with two or three nitrogen-containing haloheterocycles as reactive system 失效
标题翻译：具有两个或三个含氮卤素杂环的活性染料作为反应体系
公开(公告)号：US5245020A
公开(公告)日：1993-09-14
申请号：US853518
申请日：1992-03-18
申请人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
发明人： Joerg L. Jessen , Klaus Pandl , Hermann Loeffler , Bernd Siegel , Manfred Patsch
IPC分类号： C09B62/04
CPC分类号： C09B62/043
摘要： Reactive dyes of the formula ##STR1## where l is 0 or 1,n is 0 or 1,E is nitrogen or C--ClA is the radical of an azo dye attached to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimido group,B--if E is nitrogen--is the radical of an azo dye or of a formazan dye which in either case is bonded to the triazine ring via an imino of C.sub.1 -C.sub.4 -alkylimino group or else--if n is 0--is fluorine, chlorine or unsubstituted or substituted amino, or--if E is C--Cl--is fluorine, chlorine or methyl,X.sup.1 and X.sup.2 are independently of the other fluorine or chlorine,X.sup.3 is fluorine or chlorine or else--if E is C--Cl--methylsulfonyl andZ.sup.1 and Z.sup.2 are independently of the the other a radical of the formula ##STR2## where L.sup.3 and L.sup.4 are independently of the other hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 -alkyl,with the proviso that l and n are not simultaneously 0 and that, if E is C--Cl or if n is 0 and Z.sup.1 is the radical of the formula ##STR3## where L.sup.3 and L.sup.4 are each as defined above, A may also be the radical of a formazan dye which is bonded to the triazine ring via an imino or C.sub.1 -C.sub.4 -alkylimino group, are useful for dyeing or printing hydroxyl- or nitrogen-containing substrates.
摘要翻译：其中l为0或1的反应性染料，其中l为0或1，n为0或1，E为氮或C-Cl为经由亚氨基或C 1 -C 4烷基亚氨基连接到三嗪环上的偶氮染料的基团基团，B-如果E是氮，则是偶氮染料或甲an染料的基团，在任一情况下，通过C 1 -C 4 - 烷基亚氨基的亚氨基键合到三嗪环，或者 - 如果n是0- 氟，氯或未取代或取代的氨基，或 - 如果E是C-Cl-是氟，氯或甲基，则X1和X2独立于其它氟或氯，X3是氟或氯，或者 - 如果E是C- Cl-甲基磺酰基，Z 1和Z 2独立地为下式的基团：其中L 3和L 4独立于另一个氢或未取代或取代的C 1 -C 4 - 烷基，条件是 l和n不同时为0，并且如果E是C-Cl，或者如果n是0，并且Z1是式“IMAGE”的基团，其中L3和L4各自如上定义，则A也可以是通过亚氨基或C 1 -C 4烷基亚胺基与三嗪环结合的甲an染料的基团可用于染色或印刷含羟基或含氮基底。

28. 发明授权

US5225595A Arylsulfonyl compounds with unsaturated radicals 失效
标题翻译：具有不饱和基团的芳基磺酰基化合物
公开(公告)号：US5225595A
公开(公告)日：1993-07-06
申请号：US971270
申请日：1992-11-04
申请人： Bernd Siegel , Claus Marschner , Manfred Patsch
发明人： Bernd Siegel , Claus Marschner , Manfred Patsch
IPC分类号： C07C317/14 , C07C317/32 , C07C317/36 , C07C317/40 , C09B62/447 , C09B62/82
CPC分类号： C07C317/14 , C07C317/32 , C07C317/36 , C07C317/40 , C09B62/447 , C09B62/82
摘要： Sulfonyl compounds of the formula ##STR1## where Ar is the radical of a benzene or naphthalene ring,R.sup.1 and R.sup.2 are each hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl, substituted or unsubstituted phenyl, C.sub.1 -C.sub.4 -alkoxy, carboxyl, C.sub.1 -C.sub.4 -alkoxycarbonyl, cyano, halogen or hydroxysulfonyl,R.sup.3 is nitro, amino, C.sub.1 -C.sub.4 -alkanoylamino or benzoylamino, andR.sup.4 is a radical of the formula ##STR2## where X.sup.1, X.sup.2 and X.sup.3 are each hydrogen, substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl or substituted or unsubstituted phenyl, andX.sup.4 is a group which is detachable under alkaline conditions,either in the free form or in the form of their salts, are useful for synthesizing reactive dyes.
摘要翻译：式（I）的磺酰化合物其中Ar是苯或萘环的基团，R 1和R 2各自为氢，取代或未取代的C 1 -C 4 - 烷基，取代或未取代的苯基，C 1 -C 4 - 烷氧基，羧基，C 1 -C 4 - 烷氧基羰基，氰基，卤素或羟基磺酰基，R 3是硝基，氨基，C 1 -C 4 - 烷酰基氨基或苯甲酰基氨基，R 4是下式的基团：其中X 1，X 2和X 3各自为氢，取代或未取代的C1-C4烷基或取代或未取代的苯基，X4是在碱性条件下以游离形式或其盐形式可分离的基团，可用于合成活性染料。

29. 发明授权

US5216137A Doubled phenyl azo naphthalene reactive dyes having four halotriazine reactive groups and a phenylene diamine series bridge member 失效
标题翻译：具有四种抗坏血酸组合物的苯偶氮苯并噻唑类反应性染料和苯乙烯二胺系列桥构件
公开(公告)号：US5216137A
公开(公告)日：1993-06-01
申请号：US726242
申请日：1991-07-05
申请人： Hermann Loeffler , Manfred Patsch , Reinhold Krallmann
发明人： Hermann Loeffler , Manfred Patsch , Reinhold Krallmann
IPC分类号： C09B62/04
CPC分类号： C09B62/043
摘要： Azo reactive dyes useful for dyeing or printing hydroxyl- or nitrogen-containing substrates have the formula ##STR1## where m is 0, 1 or 2,n is 0 or 1,p is 0 or 1,R.sup.1 and R.sup.2 are each independently of the other hydrogen or substituted or unsubstituted C.sub.1 -C.sub.4 -alkyl,R.sup.3 is hydrogen, methyl or ethyl,T is carboxyl or hydroxysulfonyl,Hal is fluorine or chlorine, andthe ring A may be benzofused or substituted.
摘要翻译：可用于染色或印刷含羟基或含氮底物的偶氮活性染料具有式（1）其中m为0,1或2，n为0或1，p为0或1， R 1和R 2各自独立地为另一个氢或取代或未取代的C 1 -C 4 - 烷基，R 3是氢，甲基或乙基，T是羧基或羟基磺酰基，Hal是氟或氯，并且环A可以是苯并稠合或取代的。

30. 发明授权

US5175259A Mono- and bis-azo compounds containing 6-hydroxy-3-heterocyclic onium-pyridone-2-groupings coupled to diazo components containing diazine or triazine rings 失效
标题翻译：含有6-羟基-3-杂环基的β-吡咯烷酮-2-基团的单 - 和双 - 异氰酸酯化合物与含有二氮杂环或三嗪环的DIAZO组分相连
公开(公告)号：US5175259A
公开(公告)日：1992-12-29
申请号：US843193
申请日：1992-02-28
申请人： Joerg L. Jessen , Manfred Ruske , Knut Kessel , Manfred Patsch
发明人： Joerg L. Jessen , Manfred Ruske , Knut Kessel , Manfred Patsch
IPC分类号： C09B62/085 , C09B62/04 , C09B62/245 , C09B62/44 , C09B62/51 , D06P1/38
CPC分类号： C09B62/245 , C09B62/04 , C09B62/4411
摘要： Reactive dyes of the formula ##STR1## where n is 1 or 2,X is a six-membered halogen-containing nitrogen heterocycle,L.sup.1, depending on n, is fluorine, chlorine, C.sub.1 -C.sub.4 -alkoxy, phenoxy, C.sub.1 -C.sub.4 -alkyl, substituted or unsubstituted phenyl or a bridge member which has one or two hydroxysulfonyl groups,D is the radical of a diazo component of the aniline or naphthalene series which has at least one hydroxysulfonyl group,L.sup.2 is hydrogen or substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl,L.sup.3 is the cationic radical of an aromatic heterocycle which is linked to the pyridone ring via a nitrogen atom, andL.sup.4 is hydrogen or C.sub.1 -C.sub.4 -alkyl,with the proviso that the number of hydroxysulfonyl groups in the molecule exceeds that of the cationic groups by at least one, are useful for dyeing and printing hydroxyl- or nitrogen-containing substrates.
摘要翻译：式中，n为1或2的反应性染料，X为6元含卤素的氮杂环，L1取决于n，为氟，氯，C 1 -C 4 - 烷氧基，苯氧基，C 1 -C 4 - 烷基，取代或未取代的苯基或具有一个或两个羟基磺酰基的桥连构件，D是具有至少一个羟基磺酰基的苯胺或萘系的重氮组分的基团，L2是氢或取代或未取代的C1-C8 - 烷基，L3是通过氮原子与吡啶酮环连接的芳族杂环的阳离子基团，L4是氢或C1-C4-烷基，条件是分子中羟基磺酰基的数目超过通过至少一个的阳离子基团可用于染色和印刷含羟基或含氮底物。

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