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21. 发明授权

US4293727A Process for the oligomerization of ethylene 失效
标题翻译：乙烯低聚方法
公开(公告)号：US4293727A
公开(公告)日：1981-10-06
申请号：US179076
申请日：1980-08-18
申请人： David L. Beach , James J. Harrison
发明人： David L. Beach , James J. Harrison
IPC分类号： C07C2/32 , B01J31/00 , B01J31/18 , B01J31/22 , B01J31/24 , C07B61/00 , C07C1/00 , C07C2/36 , C07C11/02 , C07C67/00 , C07F15/04 , C08F110/02 , C07C2/02
CPC分类号： B01J31/2404 , B01J31/1895 , B01J31/2247 , C07C2/36 , C07F15/04 , C08F110/02 , B01J2231/20 , B01J2531/847 , B01J2540/32 , C07C2531/24
摘要： Ethylene is oligomerized by contacting ethylene under oligomerization conditions with a nickel ylide defined by the following Formula I: ##STR1## wherein R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.6, R.sub.7 and R.sub.8 are either alike or different members selected from the group consisting of hydrogen, alkyl radicals having from about one to about 24 carbon atoms, preferably from about one to about 10 carbon atoms; aryl radicals having from about six to about 20 carbon atoms, preferably from about six to about 10 carbon atoms; alkenyl radicals having from about two to about 30 carbons atoms, preferably from about two to about 20 carbon atoms; cycloalkyl radicals having from about three to about 40 carbon atoms, preferably from about three to about 30 carbon atoms; aralkyl and alkaryl radicals having from about six to about 40 carbon atoms, preferably from about six to about 30 carbon atoms; a halogen radical selected from the group consisting of fluorine, chlorine, bromine and iodine, preferably chlorine; a hydroxyl group; an alkoxy or aryloxy group; and a hydrocarbyl group, such as defined above, carrying halogen, hydroxyl or alkoxy or aryloxy; provided that at least one, preferably from about one to about four, of each of R.sub.1 to R.sub.8 is a sulfonato group (--SO.sub.3.sup.-) or an alkyl, aryl, alkenyl, cycloalkyl, aralkyl or alkaryl group carrying a sulfonato group; M is sulfur or oxygen, preferably oxygen; E is phosphorus, arsenic, antimony or nitrogen, preferably phosphorus; and F is phosphorus, arsenic or antimony, preferably phosphorus. This process is characterized by a relatively high reaction rate at low temperatures and pressures and results in the production of relatively high proportions of desirable trimer, tetramer, pentamer, and higher olefinic products.
摘要翻译：乙烯通过在低聚条件下与乙烯接触，通过下列通式I所定义的镍叶立德使其低聚：其中R1，R2，R3，R4，R5，R6，R7和R8是相同或不同的成员，的氢，具有约1至约24个碳原子，优选约1至约10个碳原子的烷基; 具有约6至约20个碳原子，优选约6至约10个碳原子的芳基; 具有约2至约30个碳原子，优选约2至约20个碳原子的烯基; 具有约3至约40个碳原子，优选约3至约30个碳原子的环烷基; 具有约6至约40个碳原子，优选约6至约30个碳原子的芳烷基和烷芳基; 选自氟，氯，溴和碘的卤素，优选氯; 羟基; 烷氧基或芳氧基; 和如上所定义的含有卤素，羟基或烷氧基或芳氧基的烃基; 条件是R 1至R 8中的至少一个，优选约1至约4个为磺酸基（-SO 3 - ）或带有磺酸基的烷基，芳基，烯基，环烷基，芳烷基或烷芳基; M是硫或氧，优选氧; E是磷，砷，锑或氮，优选磷; F是磷，砷或锑，优选磷。该方法的特征在于在低温和低压下的相对较高的反应速率，并导致产生相对较高比例的所需三聚体，四聚体，五聚物和更高级烯烃产物。

22. 发明授权

US08455681B2 Mannich condensation products useful as sequestering agents 有权
公开(公告)号：US08455681B2
公开(公告)日：2013-06-04
申请号：US13467336
申请日：2012-05-09
申请人： James J. Harrison , Kenneth D. Nelson
发明人： James J. Harrison , Kenneth D. Nelson
IPC分类号： C10M159/16 , C07C229/00
CPC分类号： C10L1/2235 , C08F8/32 , C10L1/238 , C10L10/04 , C10M133/08 , C10M159/16 , C10M169/045 , C10M2207/027 , C10M2217/043 , C10M2219/046 , C10M2223/045 , C10N2220/02 , C10N2230/04 , C08F10/10
摘要： The present invention is directed to Mannich condensation product sequestering agents or mixtures of Mannich condensation product sequestering agents for use in fuels and lubricating oils. The present invention is also directed to a process for preparing the Mannich condensation product sequestering agents. The present invention is also directed to a product formed by combining, under reaction conditions, a polyisobutyl-substituted hydroxyaromatic compound, an aldehyde, an amino acid or ester thereof, and an alkali metal base to form the Mannich condensation product sequestering agent. The present invention is also directed to a lubricating oil composition, a lubricating oil concentrate, a fuel composition, and a fuel concentrate having the Mannich condensation product sequestering agents of the present invention.

23. 发明申请

US20130085235A1 POST-TREATED ADDITIVE COMPOSITION AND METHOD OF MAKING THE SAME 有权
标题翻译：后处理添加剂组合物及其制备方法
公开(公告)号：US20130085235A1
公开(公告)日：2013-04-04
申请号：US13685904
申请日：2012-11-27
申请人： James J. Harrison , Mitra Hosseini
发明人： James J. Harrison , Mitra Hosseini
IPC分类号： C08F8/32
CPC分类号： C08F8/32 , C08F8/00 , C08F2810/20 , C10L1/221 , C10L1/2364 , C10L10/18 , C10M133/56 , C10M177/00 , C10M2215/28 , C10N2230/041 , C10N2230/68 , C10N2240/10 , C10N2260/06 , C10N2260/00 , C08F255/08 , C08F8/48
摘要： An oil-soluble lubricating oil additive composition prepared by the process which comprises reacting (A) reacting a copolymer of an (i) an unsaturated acidic reagent; and (ii) a mono-olefin, with at least one linking hydrocarbyl di-primary amine, thereby producing a hybrid succinic anhydride copolymer having from about 10% to about 90% unreacted anhydride groups; and subsequently (B) reacting the hybrid succinic anhydride copolymer with a second amine compound, thereby producing the succinimide; and (C) reacting the succinimide with at least one post-treating agent selected from a cyclic carbonate, a linear mono-carbonate, a linear poly-carbonate, an aromatic polycarboxylic acid, an aromatic polycarboxylic anhydride, an aromatic polycarboxylic acid ester, or mixtures thereof.
摘要翻译：一种通过该方法制备的油溶性润滑油添加剂组合物，其包括使（A）使（i）不饱和酸性试剂的共聚物与和（ii）具有至少一个连接的烃基二伯胺的单烯烃，从而产生具有约10％至约90％未反应的酸酐基团的杂化琥珀酸酐共聚物; 然后（B）使杂化琥珀酸酐共聚物与第二胺化合物反应，从而制备琥珀酰亚胺; 和（C）使琥珀酰亚胺与至少一种选自环状碳酸酯，直链单碳酸酯，直链多元碳酸酯，芳族多元羧酸，芳族多羧酸酐，芳族多元羧酸酯的后处理剂反应，或其混合物。

24. 发明授权

US08207380B2 Alkylated hydroxyaromatic compound substantially free of endocrine disruptive chemicals and method of making the same 有权
标题翻译：基本上不含内分泌破坏性化学品的烷基化羟基芳族化合物及其制备方法
公开(公告)号：US08207380B2
公开(公告)日：2012-06-26
申请号：US11741687
申请日：2007-04-27
申请人： Curt B. Campbell , James J. Harrison
发明人： Curt B. Campbell , James J. Harrison
IPC分类号： C07C37/00 , C07C15/067 , A61K31/05
CPC分类号： C07C39/06 , C07C37/14 , C07C39/10 , C10M129/10 , C10M2207/023 , C10M2207/026 , C10N2230/64
摘要： An alkylated hydroxyaromatic compound prepared by reacting at least one hydroxyaromatic compound with a branched olefinic oligomer having from about 20 to about 80 carbon atoms in the presence of a acid catalyst. The alkylated hydroxyaromatic compound has been determined to be substantially free of endocrine disruptive chemicals when the effects were quantified on pubertal development and thyroid function in the intact juvenile female rat.
摘要翻译：通过使酸性催化剂存在下使至少一种羟基芳族化合物与具有约20至约80个碳原子的支链烯属低聚物反应制备的烷基化羟基芳族化合物。当完整的青少年雌性大鼠的青春期发育和甲状腺功能的影响量化时，烷基化羟基芳族化合物被确定为基本上不含内分泌破坏性化学物质。

25. 发明申请

US20080269351A1 ALKYLATED HYDROXYAROMATIC COMPOUND SUBSTANTIALLY FREE OF ENDOCRINE DISRUPTIVE CHEMICALS AND METHOD OF MAKING THE SAME 有权
标题翻译：碱性羟基化合物大量无内源性破坏性化学物质及其制备方法
公开(公告)号：US20080269351A1
公开(公告)日：2008-10-30
申请号：US11741687
申请日：2007-04-27
申请人： Curt B. Campbell , James J. Harrison
发明人： Curt B. Campbell , James J. Harrison
IPC分类号： A61K31/05 , A61P43/00 , C07C39/06
CPC分类号： C07C39/06 , C07C37/14 , C07C39/10 , C10M129/10 , C10M2207/023 , C10M2207/026 , C10N2230/64
摘要： An alkylated hydroxyaromatic compound prepared by reacting at least one hydroxyaromatic compound with a branched olefinic oligomer having from about 20 to about 80 carbon atoms in the presence of a acid catalyst. The alkylated hydroxyaromatic compound has been determined to be substantially free of endocrine disruptive chemicals when the effects were quantified on pubertal development and thyroid function in the intact juvenile female rat.
摘要翻译：通过使酸性催化剂存在下使至少一种羟基芳族化合物与具有约20至约80个碳原子的支链烯属低聚物反应制备的烷基化羟基芳族化合物。当完整的青少年雌性大鼠的青春期发育和甲状腺功能的影响量化时，烷基化羟基芳族化合物被确定为基本上不含内分泌破坏性化学物质。

26. 发明授权

US06737387B2 Dispersed hydrated potassium borate compositions having improved properties in lubricating oil compositions 有权
标题翻译：在润滑油组合物中具有改进性能的分散的水合硼酸钾组合物
公开(公告)号：US06737387B2
公开(公告)日：2004-05-18
申请号：US10139444
申请日：2002-05-02
申请人： James J. Harrison , Kenneth D. Nelson , Juan A. Buitrago
发明人： James J. Harrison , Kenneth D. Nelson , Juan A. Buitrago
IPC分类号： C10M12526
CPC分类号： C10M141/06 , C10M141/10 , C10M2201/062 , C10M2201/08 , C10M2201/085 , C10M2201/087 , C10M2207/129 , C10M2215/223 , C10M2215/224 , C10M2215/28 , C10M2219/022 , C10M2219/044 , C10M2219/046 , C10M2219/102 , C10M2223/043 , C10M2223/045 , C10M2223/047 , C10M2223/049 , C10N2210/01 , C10N2210/06 , C10N2230/06 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/045 , C10N2240/046 , C10N2240/08 , C10N2240/40
摘要： Disclosed are dispersed hydrated potassium borate compositions, as well as additive packages and finished oil compositions comprising the same. The dispersed hydrated potassium borate compositions of the invention exhibit low turbidity and the finished oil compositions exhibit improved wear performance under high temperature conditions.
摘要翻译：公开了分散的水合硼酸钾组合物，以及包含其的添加剂包和成品油组合物。本发明的分散的水合硼酸钾组合物显示低浊度，并且成品油组合物在高温条件下表现出改进的磨损性能。

27. 发明授权

US5821205A Polyalkylene succinimides and post-treated derivatives thereof 失效
标题翻译：聚亚烷基琥珀酰亚胺及其后处理衍生物
公开(公告)号：US5821205A
公开(公告)日：1998-10-13
申请号：US566231
申请日：1995-12-01
申请人： James J. Harrison , William R. Ruhe, Jr.
发明人： James J. Harrison , William R. Ruhe, Jr.
IPC分类号： C10L1/224 , C08F8/32 , C08G73/10 , C08K5/01 , C08L79/08 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/22 , C10L1/234 , C10L1/236 , C10L1/238 , C10L1/24 , C10L1/26 , C10L1/30 , C10L10/00 , C10L10/08 , C10L10/18 , C10M101/02 , C10M133/56 , C10M149/06 , C10M161/00 , C10M145/00 , C10M149/00
CPC分类号： C10L10/08 , C08F8/32 , C10L1/143 , C10L1/221 , C10L1/234 , C10L1/236 , C10L1/2364 , C10L1/2366 , C10L1/238 , C10L1/303 , C10L10/02 , C10L10/04 , C10M133/56 , C10M149/06 , C10M161/00 , C10L1/1608 , C10L1/1616 , C10L1/1824 , C10L1/2368 , C10L1/2383 , C10L1/2493 , C10L1/2691 , C10M2215/04 , C10M2215/26 , C10M2215/28 , C10M2217/024 , C10M2217/046 , C10M2217/06 , C10M2227/061 , C10N2270/02
摘要： A succinimide composition is prepared by reacting a mixture of an alkenyl or alkylsuccinic acid derivative, an unsaturated acidic reagent copolymer, and a polyamine under reactive conditions. The alkenyl or alkyl substituent of the alkenyl or alkylsuccinic acid derivative has a Mn of from 1000 to 5000. The unsaturated acidic reagent copolymer is a copolymer of an unsaturated acidic reagent and an alkylene group. That alkylene group can be an .alpha.-olefin having 8 to 42 carbon atoms, a polyalkylene having from 8 to 28 carbon atoms, ethylene, styrene, 1,3-butadiene, vinyl alkyl ether having at least 3 carbon atoms, or vinyl alkanoate having at least 4 carbon atoms. The polyamine has at least three nitrogen atoms and 4 to 20 carbon atoms. The mixture contains from 0.5 to 10 equivalents of the alkenyl or alkylsuccinic acid derivative per equivalent of unsaturated acidic reagent copolymer and from 0.4 to 1.0 moles of polyamine per equivalent of alkenyl or alkylsuccinic acid derivative plus unsaturated acidic reagent copolymer.
摘要翻译：琥珀酰亚胺组合物通过在反应条件下使烯基或烷基琥珀酸衍生物，不饱和酸性试剂共聚物和多胺的混合物反应来制备。烯基或烷基琥珀酸衍生物的烯基或烷基取代基的Mn为1000-5000。不饱和酸性试剂共聚物是不饱和酸性试剂和亚烷基的共聚物。该亚烷基可以是具有8至42个碳原子的α-烯烃，具有8至28个碳原子的聚亚烷基，乙烯，苯乙烯，1,3-丁二烯，具有至少3个碳原子的乙烯基烷基醚或链烷酸乙烯酯，至少4个碳原子。多胺具有至少三个氮原子和4-20个碳原子。该混合物每当量不饱和酸性试剂共聚物含有0.5至10当量链烯基或烷基琥珀酸衍生物，每当量链烯基或烷基琥珀酸衍生物加不饱和酸性试剂共聚物为0.4至1.0摩尔多胺。

28. 发明授权

US5286799A Two-step free radical catalyzed process for the preparation of alkenyl succinic anhydride 失效
标题翻译：用于制备烯基琥珀酸酐的两步自由基催化方法
公开(公告)号：US5286799A
公开(公告)日：1994-02-15
申请号：US918180
申请日：1992-07-23
申请人： James J. Harrison , William R. Ruhe, Jr.
发明人： James J. Harrison , William R. Ruhe, Jr.
IPC分类号： C07D307/60 , C08F8/46 , C08F255/00 , C08F255/02 , C08F255/10 , C10L1/14 , C10L1/16 , C10L1/18 , C10L1/198 , C10L1/22 , C10L1/2383 , C10L1/2387 , C10M129/93 , C10M133/56 , C10M145/16 , C10M149/06 , C10N20/04 , C10N30/04 , C10N70/00 , C10M145/02 , C08F255/08
CPC分类号： C10M149/06 , C08F255/02 , C08F255/10 , C08F8/46 , C10L1/143 , C10L1/198 , C10L1/2383 , C10L1/2387 , C10M129/93 , C10M133/56 , C10M145/16 , C10L1/1616 , C10M2207/123 , C10M2207/129 , C10M2207/22 , C10M2209/086 , C10M2215/04 , C10M2215/26 , C10M2217/046 , C10M2217/06 , C10N2270/02
摘要： A process for the preparation of an alkenyl-substituted succinic anhydride wherein the alkenyl substituent has a number average molecular weight of from about 500 to 5000 and the average number of succinic groups per alkenyl group is greater than 1.2 which comprises:(a) reacting a polyolefin having an alkylvinylidene isomer content of less than about 10 percent and a number average molecular weight of about 500 to 5000 with maleic anhydride in the presence of a free radical initiator at a temperature in the range of about 100.degree. C. to 220.degree. C. to provide a mixture of alkenyl succinic anhydride having an average of greater than 1.2 succinic groups per alkenyl group and unreacted polyolefin, wherein the conversion of polyolefin is from about 30 to about 65 percent, and(b) reacting the mixture of alkenyl succinic anhydride and unreacted polyolefin with maleic anhydride at a temperature in the range of about 200.degree. C. to 250.degree. C. to thereby provide an alkenyl succinic anhydride having an average of greater than 1.2 succinic groups per alkenyl group, wherein the total conversion of polyolefin is about 5 to 40 percentage points higher than the conversion in step (a).
摘要翻译：一种制备链烯基取代的琥珀酸酐的方法，其中烯基取代基的数均分子量为约500至5000，并且每个烯基的琥珀酸基团的平均数大于1.2，其包括：（a）使在约100℃至220℃的温度范围内，在自由基引发剂存在下，马来酸酐具有小于约10％的烷基亚乙烯基异构体含量和约500至5000的数均分子量的聚烯烃提供每个烯基平均具有大于1.2个琥珀酸基的链烯基琥珀酸酐与未反应聚烯烃的混合物，其中聚烯烃的转化率为约30至约65％，和（b）使烯基琥珀酸酐的混合物和未反应的聚烯烃与马来酸酐在约200℃至250℃的温度范围内，从而提供烯基琥珀酸每个烯基平均具有大于1.2个琥珀酸基团的酸酐，其中聚烯烃的总转化率比步骤（a）中的转化率高约5至40个百分点。

29. 发明授权

US5232616A Lubricating compositions 失效
标题翻译：润滑组合物
公开(公告)号：US5232616A
公开(公告)日：1993-08-03
申请号：US570581
申请日：1990-08-21
申请人： James J. Harrison , Curtis B. Campbell
发明人： James J. Harrison , Curtis B. Campbell
IPC分类号： C10M133/56 , C10M141/00 , C10M159/12 , C10M163/00 , C10N10/02 , C10N10/04 , C10N20/00 , C10N30/04 , C10N40/25 , C10N70/00
CPC分类号： C10M141/00 , C10M133/56 , C10M2201/062 , C10M2207/023 , C10M2207/026 , C10M2207/027 , C10M2215/04 , C10M2215/042 , C10M2215/26 , C10M2215/28 , C10M2217/046 , C10M2217/06 , C10M2219/044 , C10M2219/087 , C10M2219/088 , C10M2219/089 , C10M2223/045 , C10N2210/01 , C10N2240/10 , C10N2240/101 , C10N2240/104 , C10N2240/106
摘要： Provided are lubricating oil compositions which contain (a) a mixture comprising an oil-soluble alkali metal compound and certain polyalkenyl succinimide or (b) alkali metal salts of said polyalkenyl succinimides.

30. 发明授权

US4662943A Cement compositions containing a polysaccharide and a salt and method of cementing casing in a well 失效
标题翻译：含有多糖和盐的水泥组合物以及将套管固定在井中的方法
公开(公告)号：US4662943A
公开(公告)日：1987-05-05
申请号：US684659
申请日：1984-06-12
申请人： Wilford S. Baker , James J. Harrison
发明人： Wilford S. Baker , James J. Harrison
IPC分类号： C04B24/38 , C04B28/02 , C09K8/42 , C09K8/46 , C04B7/353
CPC分类号： C04B24/383 , C04B28/02 , C09K8/42 , C09K8/46
摘要： A novel cement composition comprising (1) cement, (2) at least one salt, and (3) at least one polysaccharide or mixture of polysaccharides having a solution time greater than about 10 minutes; aqueous slurries prepared from these novel cement compositions and a method of cementing casing in the borehole of a well using such novel aqueous cement slurries.
摘要翻译：一种新型水泥组合物，其包含（1）水泥，（2）至少一种盐，和（3）溶液时间大于约10分钟的至少一种多糖或多糖混合物; 由这些新型水泥组合物制备的水性浆料以及使用这种新型水性水泥浆料将套管固定在井眼中的方法。

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