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1. 发明授权

US08455681B2 Mannich condensation products useful as sequestering agents 有权
公开(公告)号：US08455681B2
公开(公告)日：2013-06-04
申请号：US13467336
申请日：2012-05-09
申请人： James J. Harrison , Kenneth D. Nelson
发明人： James J. Harrison , Kenneth D. Nelson
IPC分类号： C10M159/16 , C07C229/00
CPC分类号： C10L1/2235 , C08F8/32 , C10L1/238 , C10L10/04 , C10M133/08 , C10M159/16 , C10M169/045 , C10M2207/027 , C10M2217/043 , C10M2219/046 , C10M2223/045 , C10N2220/02 , C10N2230/04 , C08F10/10
摘要： The present invention is directed to Mannich condensation product sequestering agents or mixtures of Mannich condensation product sequestering agents for use in fuels and lubricating oils. The present invention is also directed to a process for preparing the Mannich condensation product sequestering agents. The present invention is also directed to a product formed by combining, under reaction conditions, a polyisobutyl-substituted hydroxyaromatic compound, an aldehyde, an amino acid or ester thereof, and an alkali metal base to form the Mannich condensation product sequestering agent. The present invention is also directed to a lubricating oil composition, a lubricating oil concentrate, a fuel composition, and a fuel concentrate having the Mannich condensation product sequestering agents of the present invention.

2. 发明授权

US06737387B2 Dispersed hydrated potassium borate compositions having improved properties in lubricating oil compositions 有权
标题翻译：在润滑油组合物中具有改进性能的分散的水合硼酸钾组合物
公开(公告)号：US06737387B2
公开(公告)日：2004-05-18
申请号：US10139444
申请日：2002-05-02
申请人： James J. Harrison , Kenneth D. Nelson , Juan A. Buitrago
发明人： James J. Harrison , Kenneth D. Nelson , Juan A. Buitrago
IPC分类号： C10M12526
CPC分类号： C10M141/06 , C10M141/10 , C10M2201/062 , C10M2201/08 , C10M2201/085 , C10M2201/087 , C10M2207/129 , C10M2215/223 , C10M2215/224 , C10M2215/28 , C10M2219/022 , C10M2219/044 , C10M2219/046 , C10M2219/102 , C10M2223/043 , C10M2223/045 , C10M2223/047 , C10M2223/049 , C10N2210/01 , C10N2210/06 , C10N2230/06 , C10N2240/04 , C10N2240/042 , C10N2240/044 , C10N2240/045 , C10N2240/046 , C10N2240/08 , C10N2240/40
摘要： Disclosed are dispersed hydrated potassium borate compositions, as well as additive packages and finished oil compositions comprising the same. The dispersed hydrated potassium borate compositions of the invention exhibit low turbidity and the finished oil compositions exhibit improved wear performance under high temperature conditions.
摘要翻译：公开了分散的水合硼酸钾组合物，以及包含其的添加剂包和成品油组合物。本发明的分散的水合硼酸钾组合物显示低浊度，并且成品油组合物在高温条件下表现出改进的磨损性能。

3. 发明申请

US20130303416A1 MANNICH CONDENSATION PRODUCTS USEFUL AS SEQUESTERING AGENTS 有权
标题翻译： MANNICH CONDENSATION产品有用作为序列代理
公开(公告)号：US20130303416A1
公开(公告)日：2013-11-14
申请号：US13861552
申请日：2013-04-12
申请人： James J. Harrison , Kenneth D. Nelson
发明人： James J. Harrison , Kenneth D. Nelson
IPC分类号： C10M133/08
CPC分类号： C10L1/2235 , C08F8/32 , C10L1/238 , C10L10/04 , C10M133/08 , C10M159/16 , C10M169/045 , C10M2207/027 , C10M2217/043 , C10M2219/046 , C10M2223/045 , C10N2220/02 , C10N2230/04 , C08F10/10
摘要： The present invention is directed to Mannich condensation product sequestering agents or mixtures of Mannich condensation product sequestering agents for use in fuels and lubricating oils. The present invention is also directed to a process for preparing the Mannich condensation product sequestering agents. The present invention is also directed to a product formed by combining, under reaction conditions, a polyisobutyl-substituted hydroxyaromatic compound, an aldehyde, an amino acid or ester thereof, and an alkali metal base to form the Mannich condensation product sequestering agent. The present invention is also directed to a lubricating oil composition, a lubricating oil concentrate, a fuel composition, and a fuel concentrate having the Mannich condensation product sequestering agents of the present invention.
摘要翻译：本发明涉及Mannich缩合产物螯合剂或用于燃料和润滑油的曼尼期缩合产物螯合剂的混合物。本发明还涉及制备曼尼期缩合产物螯合剂的方法。本发明还涉及通过在反应条件下将聚异丁基取代的羟基芳族化合物，醛，氨基酸或其酯与碱金属碱组合以形成曼尼期缩合产物螯合剂形成的产物。本发明还涉及具有本发明的曼尼期缩合产物螯合剂的润滑油组合物，润滑油浓缩物，燃料组合物和燃料浓缩物。

4. 发明申请

US20120190863A1 PROCESS FOR PREPARATION OF LOW MOLECULAR WEIGHT MOLYBDENUM SUCCINIMIDE COMPLEXES 有权
标题翻译：低分子量钼多糖复合物的制备方法
公开(公告)号：US20120190863A1
公开(公告)日：2012-07-26
申请号：US13011495
申请日：2011-01-21
申请人： Kenneth D. Nelson , James J. Harrison , Paula Rogers , Mitra Hosseini
发明人： Kenneth D. Nelson , James J. Harrison , Paula Rogers , Mitra Hosseini
IPC分类号： C07F11/00
CPC分类号： C07F11/00 , C07D207/408
摘要： Disclosed is a process for preparing a molybdated succinimide complex, the process comprising: (a) reacting an alkyl or alkenyl succinimide of a polyamine of formula I or formula II or mixtures thereof: wherein R is an about C12 to C30 alkyl or alkenyl group, R′ is a straight or branched-chain alkylene group having 2 to 3 carbon atoms, x is 1 to 11, and y is 1 to 10, with an α,β-unsaturated mono-carboxylic acid or carboxylic acid ester, in a charge mole ratio of the α,β-unsaturated mono-carboxylic acid or carboxylic acid ester to the succinimide of formula I or formula II or mixtures thereof of about 0.1:1 to about 6:1, and wherein the reaction temperature is no greater than about 135° C.; and (b) reacting the succinimide product of step (a) with an acidic molybdenum compound to provide the molybdated succinimide complex, wherein the molybdated succinimide complex prepared is a liquid at room temperature.
摘要翻译：公开了制备钼酸化琥珀酰亚胺络合物的方法，该方法包括：（a）使式I或式II的多胺或其混合物的烷基或链烯基琥珀酰亚胺或其混合物反应：其中R为约C 12至C 30烷基或烯基， R'是具有2至3个碳原子的直链或支链亚烷基，x为1至11，y为1至10，与α，bgr-不饱和单羧酸或羧酸酯反应， α，β-不饱和单羧酸或羧酸酯与式I或式II的琥珀酰亚胺或其混合物的摩尔比为约0.1:1至约6:1，并且其中反应温度不大比约135℃。和（b）使步骤（a）的琥珀酰亚胺产物与酸性钼化合物反应以提供钼酸化琥珀酰亚胺配合物，其中制备的钼酸化琥珀酰亚胺络合物在室温下为液体。

5. 发明授权

US06632781B2 Lubricant composition comprising alkali metal borate dispersed in a polyalkylene succinic anhydride and a metal salt of a polyisobutenyl sulfonate 有权
标题翻译：包含分散在聚亚烷基琥珀酸酐中的碱金属硼酸盐和聚异丁烯基磺酸盐的金属盐的润滑剂组合物
公开(公告)号：US06632781B2
公开(公告)日：2003-10-14
申请号：US09967049
申请日：2001-09-28
申请人： James J. Harrison , Kenneth D. Nelson
发明人： James J. Harrison , Kenneth D. Nelson
IPC分类号： C01M12526
CPC分类号： C10M141/08 , C10M141/10 , C10M163/00 , C10M2201/062 , C10M2201/08 , C10M2201/082 , C10M2201/084 , C10M2201/085 , C10M2201/087 , C10M2201/102 , C10M2207/129 , C10M2207/34 , C10M2219/044 , C10M2219/046 , C10N2210/02 , C10N2220/021 , C10N2220/142 , C10N2230/04 , C10N2230/26 , C10N2240/04 , C10N2240/08
摘要： Disclosed are lubricant compositions comprising a dispersed hydrated alkali metal borate, a polyalkylene succinic dispersant selected from a polyalkylene succinic anhydride, a mixture of polyalkylene succinic anhydrides or derivatives thereof; and a metal salt of a polyisobutenyl sulfonate. Also disclosed are methods for improving the water tolerance of a lubricant composition and methods for preparing such lubricants comprising a dispersed hydrated alkali metal borate and a dispersant mixture.
摘要翻译：公开了包含分散的水合碱金属硼酸盐，聚亚烷基琥珀酸分散剂的选自聚亚烷基琥珀酸酐，聚亚烷基琥珀酸酐或其衍生物的混合物的润滑剂组合物; 和聚异丁烯基磺酸盐的金属盐。还公开了用于改善润滑剂组合物的耐水性的方法和用于制备这种润滑剂的方法，所述润滑剂包含分散的水合碱金属硼酸盐和分散剂混合物。

6. 发明授权

US08722927B2 Mannich condensation products useful as sequestering agents 有权
公开(公告)号：US08722927B2
公开(公告)日：2014-05-13
申请号：US13861552
申请日：2013-04-12
申请人： James J. Harrison , Kenneth D. Nelson
发明人： James J. Harrison , Kenneth D. Nelson
IPC分类号： C10M133/00 , C07C209/00 , C07C233/00
CPC分类号： C10L1/2235 , C08F8/32 , C10L1/238 , C10L10/04 , C10M133/08 , C10M159/16 , C10M169/045 , C10M2207/027 , C10M2217/043 , C10M2219/046 , C10M2223/045 , C10N2220/02 , C10N2230/04 , C08F10/10
摘要： The present invention is directed to Mannich condensation product sequestering agents or mixtures of Mannich condensation product sequestering agents for use in fuels and lubricating oils. The present invention is also directed to a process for preparing the Mannich condensation product sequestering agents. The present invention is also directed to a product formed by combining, under reaction conditions, a polyisobutyl-substituted hydroxyaromatic compound, an aldehyde, an amino acid or ester thereof, and an alkali metal base to form the Mannich condensation product sequestering agent. The present invention is also directed to a lubricating oil composition, a lubricating oil concentrate, a fuel composition, and a fuel concentrate having the Mannich condensation product sequestering agents of the present invention.

7. 发明授权

US08426608B2 Process for preparation of high molecular weight molybdenum succinimide complexes 有权
标题翻译：制备高分子量琥珀酰亚胺复合物的方法
公开(公告)号：US08426608B2
公开(公告)日：2013-04-23
申请号：US13011520
申请日：2011-01-21
申请人： Kenneth D. Nelson , James J. Harrison , Paula Rogers , Mitra Hosseini
发明人： Kenneth D. Nelson , James J. Harrison , Paula Rogers , Mitra Hosseini
IPC分类号： C07D207/404
CPC分类号： C07D403/12 , C10M159/18 , C10M2201/062 , C10M2201/08 , C10M2201/081 , C10M2215/28 , C10M2227/09 , C10N2210/06 , C10N2270/00
摘要： Disclosed is a process for preparing a molybdated succinimide complex, the process comprising: (a) reacting an alkyl or alkenyl mono- or bis-succinimide of a polyamine of formula I or formula II or mixtures thereof: wherein R is an alkyl or alkenyl group having a number average molecular weight of about 500 to about 5,000, R′ is a straight or branched-chain alkylene group having 2 to 3 carbon atoms, x is 2 to 11, and y is 1 to 10, with an α,β-unsaturated mono-carboxylic acid or carboxylic acid ester, in a charge mole ratio of the α,β-unsaturated mono-carboxylic acid or carboxylic acid ester to the succinimide of formula I or formula II or mixtures thereof of greater than 1.05:1 to about 6:1, and wherein the reaction temperature is in the range of from greater than 80° C. to no greater than about 150° C.; and (b) reacting the succinimide product of step (a) with an acidic molybdenum compound to provide the molybdated succinimide complex, wherein the molybdated succinimide complex is a liquid at room temperature.
摘要翻译：公开了一种制备钼酸化琥珀酰亚胺复合物的方法，该方法包括：（a）使式I或式II的多胺或其混合物的烷基或烯基单 - 或二 - 琥珀酰亚胺反应：其中R是烷基或链烯基数均分子量为约500至约5,000，R'为具有2至3个碳原子的直链或支链亚烷基，x为2至11，y为1至10，其中α，β- 不饱和单羧酸或羧酸酯，α，β-不饱和单羧酸或羧酸酯与式I或式II的琥珀酰亚胺或其混合物的电荷摩尔比大于1.05:1至约 6：1，其中反应温度在大于80℃至不大于约150℃的范围内。和（b）使步骤（a）的琥珀酰亚胺产物与酸性钼化合物反应以提供钼酸化琥珀酰亚胺配合物，其中钼酸化琥珀酰亚胺络合物在室温下为液体。

8. 发明授权

US07884058B2 Stable colloidal suspensions and lubricating oil compositions containing same 有权
标题翻译：稳定的胶体悬浮液和含有它的润滑油组合物
公开(公告)号：US07884058B2
公开(公告)日：2011-02-08
申请号：US10675631
申请日：2003-09-30
申请人： Kenneth D. Nelson , James J. Harrison
发明人： Kenneth D. Nelson , James J. Harrison
IPC分类号： B01F17/00 , C07C309/62 , C08G81/02 , C10L1/22 , C10L1/24 , C10M159/24 , C10M173/02
CPC分类号： C10M169/045 , C10M159/18 , C10M163/00 , C10M2201/18 , C10M2207/127 , C10M2207/129 , C10M2207/283 , C10M2215/02 , C10M2215/222 , C10M2215/224 , C10M2215/28 , C10M2219/022 , C10M2219/044 , C10M2219/046 , C10M2219/106 , C10M2223/04 , C10M2223/045 , C10M2227/066 , C10N2210/01 , C10N2210/03 , C10N2210/05 , C10N2210/06 , C10N2220/082 , C10N2250/02 , C10N2210/02
摘要： A stable colloidal suspension comprising: (a) a dispersed phase comprising a major amount of one or more dispersed hydrated polymeric compounds selected from the group consisting of polymolybdates, polytungstates, polyvanadates, polyniobates, polytantalates, polyuranates, and mixtures thereof, and, (b) an oil phase comprising one or more dispersing agents and a diluent oil. Processes for preparing the stable colloidal suspensions and their use in lubricating oil compositions are also provided.
摘要翻译：一种稳定的胶体悬浮液，其包含：（a）包含主要量的一种或多种分散的水合聚合物的分散相，所述分散的水合聚合物选自聚钼酸盐，聚钨酸盐，聚钒酸盐，聚异戊二烯酸盐，聚丁二酸盐，聚脲酸盐及其混合物，和（b ）包含一种或多种分散剂和稀释油的油相。还提供了制备稳定的胶体悬浮液的方法及其在润滑油组合物中的用途。

9. 发明申请

US20120253065A1 MANNICH CONDENSATION PRODUCTS USEFUL AS SEQUESTERING AGENTS 有权
标题翻译： MANNICH CONDENSATION产品有用作为序列代理
公开(公告)号：US20120253065A1
公开(公告)日：2012-10-04
申请号：US13467336
申请日：2012-05-09
申请人： James J. Harrison , Kenneth D. Nelson
发明人： James J. Harrison , Kenneth D. Nelson
IPC分类号： C07C229/14 , C07C227/18
CPC分类号： C10L1/2235 , C08F8/32 , C10L1/238 , C10L10/04 , C10M133/08 , C10M159/16 , C10M169/045 , C10M2207/027 , C10M2217/043 , C10M2219/046 , C10M2223/045 , C10N2220/02 , C10N2230/04 , C08F10/10
摘要： The present invention is directed to Mannich condensation product sequestering agents or mixtures of Mannich condensation product sequestering agents for use in fuels and lubricating oils. The present invention is also directed to a process for preparing the Mannich condensation product sequestering agents. The present invention is also directed to a product formed by combining, under reaction conditions, a polyisobutyl-substituted hydroxyaromatic compound, an aldehyde, an amino acid or ester thereof, and an alkali metal base to form the Mannich condensation product sequestering agent. The present invention is also directed to a lubricating oil composition, a lubricating oil concentrate, a fuel composition, and a fuel concentrate having the Mannich condensation product sequestering agents of the present invention.
摘要翻译：本发明涉及Mannich缩合产物螯合剂或用于燃料和润滑油的曼尼期缩合产物螯合剂的混合物。本发明还涉及制备曼尼期缩合产物螯合剂的方法。本发明还涉及通过在反应条件下将聚异丁基取代的羟基芳族化合物，醛，氨基酸或其酯与碱金属碱组合以形成曼尼期缩合产物螯合剂形成的产物。本发明还涉及具有本发明的曼尼期缩合产物螯合剂的润滑油组合物，润滑油浓缩物，燃料组合物和燃料浓缩物。

10. 发明申请

US20120190864A1 PROCESS FOR PREPARATION OF HIGH MOLECULAR WEIGHT MOLYBDENUM SUCCINIMIDE COMPLEXES 有权
标题翻译：高分子量钼多糖复合物的制备方法
公开(公告)号：US20120190864A1
公开(公告)日：2012-07-26
申请号：US13011520
申请日：2011-01-21
申请人： Kenneth D. Nelson , James J. Harrison , Paula Rogers , Mitra Hosseini
发明人： Kenneth D. Nelson , James J. Harrison , Paula Rogers , Mitra Hosseini
IPC分类号： C07F11/00
CPC分类号： C07D403/12 , C10M159/18 , C10M2201/062 , C10M2201/08 , C10M2201/081 , C10M2215/28 , C10M2227/09 , C10N2210/06 , C10N2270/00
摘要： Disclosed is a process for preparing a molybdated succinimide complex, the process comprising: (a) reacting an alkyl or alkenyl mono- or bis-succinimide of a polyamine of formula I or formula II or mixtures thereof: wherein R is an alkyl or alkenyl group having a number average molecular weight of about 500 to about 5,000, R′ is a straight or branched-chain alkylene group having 2 to 3 carbon atoms, x is 2 to 11, and y is 1 to 10, with an α,β-unsaturated mono-carboxylic acid or carboxylic acid ester, in a charge mole ratio of the α,β-unsaturated mono-carboxylic acid or carboxylic acid ester to the succinimide of formula I or formula II or mixtures thereof of greater than 1.05:1 to about 6:1, and wherein the reaction temperature is in the range of from greater than 80° C. to no greater than about 150° C.; and (b) reacting the succinimide product of step (a) with an acidic molybdenum compound to provide the molybdated succinimide complex, wherein the molybdated succinimide complex is a liquid at room temperature.
摘要翻译：公开了一种制备钼酸化琥珀酰亚胺复合物的方法，该方法包括：（a）使式I或式II的多胺或其混合物的烷基或烯基单 - 或二 - 琥珀酰亚胺反应：其中R是烷基或链烯基数均分子量为约500〜约5000，R'为碳原子数2〜3的直链或支链亚烷基，x为2〜11，y为1〜10，α，bgr; - 不饱和单羧酸或羧酸酯，以α，bgr-不饱和单羧酸或羧酸酯与式I或式II的琥珀酰亚胺或其混合物的摩尔比大于1.05:1 至约6:1，并且其中反应温度在大于80℃至不大于约150℃的范围内。和（b）使步骤（a）的琥珀酰亚胺产物与酸性钼化合物反应以提供钼酸化琥珀酰亚胺配合物，其中钼酸化琥珀酰亚胺络合物在室温下为液体。

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