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11. 发明申请

US20090227810A1 METHOD FOR PRODUCING TETRAFLUOROTEREPHTHALIC ACID DIFLUORIDE 失效
标题翻译：生产四氯丙酸二氢吡啶的方法
公开(公告)号：US20090227810A1
公开(公告)日：2009-09-10
申请号：US12096129
申请日：2006-11-21
申请人： Koji Hagiya
发明人： Koji Hagiya
IPC分类号： C07C63/15
CPC分类号： C07C51/60 , C07C67/14 , C07C63/68 , C07C69/76
摘要： A method for producing tetrafluoroterephthalic acid difluoride comprising reacting tetrachloroterephthalic acid dichloride with potassium fluoride in the presence of dimethyl sulfone.
摘要翻译：一种生产四氟对苯二甲酸二氟化物的方法，包括在二甲基砜存在下使四氯对苯二甲酰氯与氟化钾反应。

12. 发明申请

US20090105504A1 PROCESS FOR THE PREPARATION OF SATURATED OR UNSATURATED PRIMARY FATTY AMINES 失效
标题翻译：制备饱和或不饱和脂肪酸原料的方法
公开(公告)号：US20090105504A1
公开(公告)日：2009-04-23
申请号：US11996421
申请日：2006-07-21
申请人： Scott Gibson
发明人： Scott Gibson
IPC分类号： C07C209/46
CPC分类号： C07C211/21 , C07C51/60 , C07C209/50 , C07C231/02 , C07C233/09
摘要： Process for the preparation of unsaturated and saturated primary fatty amines comprising the steps of chlorination, treatment by ammonia, reduction and purification.
摘要翻译：制备不饱和和饱和伯脂肪胺的方法，包括氯化，氨处理，还原和纯化的步骤。

13. 发明授权

US07501543B2 Substituted phenylsulfur trifluoride and other like fluorinating agents 有权
标题翻译：取代的苯基三氟化硫等氟化剂
公开(公告)号：US07501543B2
公开(公告)日：2009-03-10
申请号：US12106460
申请日：2008-04-21
申请人： Teruo Umemoto , Rajendra Singh
发明人： Teruo Umemoto , Rajendra Singh
IPC分类号： C07C325/00
CPC分类号： C07C17/18 , C07B39/00 , C07C17/093 , C07C17/16 , C07C17/361 , C07C45/65 , C07C51/60 , C07C319/14 , C07C319/20 , C07C323/19 , C07C381/00 , C07C2601/14 , C07C19/08 , C07C22/08 , C07C23/10 , C07C323/03 , C07C63/10 , C07C63/04
摘要： Novel substituted phenylsulfur trifluorides that act as fluorinating agents are disclosed. Also disclosed are methods for their preparation and methods for their use in introducing one or more fluorine atoms into target substrate compounds. Finally, various intermediate compounds for use in preparing substituted phenylsulfur trifluorides are provided.
摘要翻译：公开了用作氟化剂的新型取代苯基三氟化硫。还公开了它们的制备方法和它们用于将一个或多个氟原子引入目标底物化合物中的方法。最后，提供用于制备取代的苯基三氟化硫的各种中间体化合物。

14. 发明申请

US20080269517A1 PROCESS FOR THE PREPARATION OF ACID HALIDES 审中-公开
标题翻译：制备酸性抗体的方法
公开(公告)号：US20080269517A1
公开(公告)日：2008-10-30
申请号：US12105339
申请日：2008-04-18
申请人： Ursula Hoffmann
发明人： Ursula Hoffmann
IPC分类号： C07C61/08
CPC分类号： C07C51/60 , C07C55/38 , C07C53/44 , C07C57/70
摘要： A process for the preparation of acid halides of formula I which are useful as intermediates in the preparation of i.a. pharmaceutically active compounds.
摘要翻译：制备式I的酰卤的方法，其可用作制备中间体。药物活性化合物。

15. 发明申请

US20080221364A1 SUBSTITUTED PHENYLSULFUR TRIFLUORIDE AND OTHER LIKE FLUORINATING AGENTS 有权
标题翻译：取代的苯基三氟化硼和其他类似的荧光剂
公开(公告)号：US20080221364A1
公开(公告)日：2008-09-11
申请号：US12106460
申请日：2008-04-21
申请人： TERUO UMEMOTO , RAJENDRA P. SINGH
发明人： TERUO UMEMOTO , RAJENDRA P. SINGH
IPC分类号： C07C321/00
CPC分类号： C07C17/18 , C07B39/00 , C07C17/093 , C07C17/16 , C07C17/361 , C07C45/65 , C07C51/60 , C07C319/14 , C07C319/20 , C07C323/19 , C07C381/00 , C07C2601/14 , C07C19/08 , C07C22/08 , C07C23/10 , C07C323/03 , C07C63/10 , C07C63/04
摘要： Novel substituted phenylsulfur trifluorides that act as fluorinating agents are disclosed. Also disclosed are methods for their preparation and methods for their use in introducing one or more fluorine atoms into target substrate compounds. Finally, various intermediate compounds for use in preparing substituted phenylsulfur trifluorides are provided.
摘要翻译：公开了用作氟化剂的新型取代苯基三氟化硫。还公开了它们的制备方法和它们用于将一个或多个氟原子引入目标底物化合物中的方法。最后，提供用于制备取代的苯基三氟化硫的各种中间体化合物。

16. 发明申请

US20080119665A1 Process for the Synthesis of Zirconium Carboxylates 审中-公开
标题翻译：羧酸锆合成方法
公开(公告)号：US20080119665A1
公开(公告)日：2008-05-22
申请号：US11662150
申请日：2005-08-10
申请人： Peter Fritz , Heinz Bolt , Karl-Heinz Scherschlicht , Fuad Mosa , Talal K. Ali , Sultan Al-Otaibi
发明人： Peter Fritz , Heinz Bolt , Karl-Heinz Scherschlicht , Fuad Mosa , Talal K. Ali , Sultan Al-Otaibi
IPC分类号： C07C51/41
CPC分类号： C07C51/412 , C07C51/60 , C07C53/10 , C07C57/30 , C07C57/72 , C07C53/126 , C07C53/40 , C07C53/134 , C07C53/42 , C07C53/44 , C07C53/124 , C07C53/00 , C07C53/122 , C07C53/38
摘要： A process for the synthesis of zirconium tetra carboxylates is disclosed. To overcome the disadvantageous characteristics of the currently used production process, which include highly corrosive starting substances and products, and complex removal of HCl, ZrCI4 is suspended in an apolar solvent and reacted with the anhydride of an organic acid. The sole products of this reaction are slightly corrosive Zr tetra carboxylate and an organic acid chloride, which is a valuable basic chemical in the chemicals and pharmaceuticals industry. The reactors required for the synthesis need not necessarily consist of glass and/or enamel, but may instead be manufactured from stainless steel, which is cheaper. Apparatuses for the removal and treatment of hydrochloric acid are not necessary.
摘要翻译：公开了合成四羧酸锆的方法。为了克服目前使用的包括高腐蚀性起始物质和产物的生产方法的不利特征，以及HCl的复杂去除，将ZrCl 4悬浮于非极性溶剂中并与有机酸酐反应酸。该反应的唯一产物是略微腐蚀性的四羧酸锆和有机酰氯，这是化学和制药行业中有价值的基础化学品。合成所需的反应器不一定由玻璃和/或搪瓷组成，而是可以由不锈钢制成，这是较便宜的。不需要用于去除和处理盐酸的装置。

17. 发明申请

US20080097131A1 Synthesis of carbon-labeled perfluoroalkyl compounds 有权
标题翻译：碳标记的全氟烷基化合物的合成
公开(公告)号：US20080097131A1
公开(公告)日：2008-04-24
申请号：US12001269
申请日：2007-12-11
申请人： Alexander Shtarov , Jon Howell
发明人： Alexander Shtarov , Jon Howell
IPC分类号： C07C19/16
CPC分类号： C07B59/001 , C07B2200/05 , C07C19/16 , C07C21/18 , C07C41/18 , C07C43/123 , C07C51/15 , C07C51/60 , C07C51/62 , C07C309/06 , C07C53/21 , C07C53/50 , C07C59/135
摘要： Various 13C and 14C carbon labeled compounds Rf—bCF(U)y(T)z Formula 1A or Rf—bCF2bCF(U)y(T)z Formula 1B wherein Rf is a linear or branched perfluoroalkyl radical Z(CmF2m)—, m is 1, 3 to 20, or a mixture thereof; Z is F when m is 1, and Z is F, Cl, or H when m is 3 to 20 or a mixture thereof; b is 13 or 14; y is 1, and z is 0 or 1; and when y and z are each 1, U is F, and T is selected from the group consisting of monovalent radicals —X wherein X is I or Br, —CH2—CH2—X, —CH═CH2, —CH2—CH2—OH, —CH2—COOH, —CH2OH, —bCH2OH, —COOH, —bCOOH, —O—CF(CF3)—C(O)F, —O—CF(CF3)—X, —SO2Y wherein Y is H, F or Cl, and —SO3H; and when y is 1, and z is 0, U is selected from the group consisting of divalent radicals ═CH—COOH, ═CH—CH2—OH, and =0, are disclosed, and a process for their preparation which selectively introduces 13C and 14C carbon labels into a fluoroalkyl chain.
摘要翻译：各种 13 C和14 C碳标记的化合物<？in-line-formula description =“In-line Formulas”end =“lead”？> R f 式（1A）或<β在线公式描述=“In” -line公式“end =”tail“？> <？in-line-formula description =”In-line Formulas“end =”lead“？> R CF（U）y（T）>>>>> formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas formulas>>>>>>>>>>>>>>>>>>> formulas formulas formulas formulas formulas description =“In-line Formulas”end =“tail”？>其中R f是直链或支链的全氟烷基Z（C m 2 F 2 m） SUB-） - ，m为1,3至20，或其混合物; 当m为1时，Z为F，当m为3至20时Z为F，Cl或H或其混合物; b为13或14; y为1，z为0或1; 当y和z各自为1时，U为F，T选自单价基团-X，其中X为I或Br，-CH 2 -CH 2， -X，-CH-CH 2，-CH 2 -CH 2 -OH，-CH 2 CH 2， SO 2 -COOH，-CH 2 OH， - CH 2 CH 2 OH，-COOH， - CO 2 COOH ，-O-CF（CF 3） - C（O）F，-O-CF（CF 3） - X，-SO 2

18. 发明申请

US20070299282A1 Method for the Production of Phthalic Dichloride 审中-公开
标题翻译：邻苯二甲酸二氯生产方法
公开(公告)号：US20070299282A1
公开(公告)日：2007-12-27
申请号：US11719983
申请日：2005-11-24
申请人： Thorsten Rohde , Jochem Henkelmann
发明人： Thorsten Rohde , Jochem Henkelmann
IPC分类号： C07C51/60
CPC分类号： C07C51/60 , C07C63/22
摘要： A process for preparing phthaloyl chloride by reacting phthalic anhydride with a chlorinating agent (I) selected from the group of thionyl chloride and phosgene in the presence of a catalyst at a temperature of from 80 to 200° C. and a pressure of from 0.01 to 10 MPa abs, in which the catalyst (II) used is triphenylphosphine, triphenylphosphine oxide or a mixture thereof.
摘要翻译：一种通过邻苯二甲酸酐与选自亚硫酰氯和光气的氯化剂（I）在催化剂存在下，在80-200℃和0.01〜 10MPa abs，其中使用的催化剂（II）是三苯基膦，三苯基氧化膦或其混合物。

19. 发明授权

US07311890B2 Process for the production of fluorinated organic compounds and fluorinating agents 有权
标题翻译：用于生产氟化有机化合物和氟化剂的方法
公开(公告)号：US07311890B2
公开(公告)日：2007-12-25
申请号：US10885042
申请日：2004-07-07
申请人： Norihiko Yoneda , Tsuyoshi Fukuhara , Kazuhiro Shimokawa , Kenji Adachi , Satoshi Oishi
发明人： Norihiko Yoneda , Tsuyoshi Fukuhara , Kazuhiro Shimokawa , Kenji Adachi , Satoshi Oishi
IPC分类号： C01B7/24
CPC分类号： C07C67/307 , C07B39/00 , C07C17/093 , C07C17/16 , C07C17/18 , C07C29/64 , C07C37/62 , C07C41/22 , C07C45/30 , C07C51/60 , C07C201/12 , C07C209/74 , C07C245/04 , C07C245/06 , C07C319/20 , C07C2601/14 , C07C2603/18 , C07C211/52 , C07C323/03 , C07C323/22 , C07C323/52 , C07C323/60 , C07C323/65 , C07C33/46 , C07C205/11 , C07C69/75 , C07C53/42 , C07C39/27 , C07C49/697 , C07C49/687 , C07C69/716 , C07C43/225
摘要： A process for the production of a fluorinated organic compound, characterized by fluorinating an organic compound having a hydrogen atoms using IF5; and a novel fluorination process for fluorinating an organic compound having a hydrogen atoms by using a fluorinating agent containing IF5 and at least one member selected from the group consisting of acids, bases, salts and additives.
摘要翻译：一种制备氟化有机化合物的方法，其特征在于使用IF 5氟化具有氢原子的有机化合物; 以及通过使用含有IF 5的氟化剂和选自酸，碱，盐和添加剂中的至少一种的氟化有氢化物的有机化合物的新的氟化方法。

20. 发明申请

US20050113567A1 Perfluoroisopropylbenzene derivative 失效
标题翻译：全氟异丙基苯衍生物
公开(公告)号：US20050113567A1
公开(公告)日：2005-05-26
申请号：US10969974
申请日：2004-10-22
申请人： Masanobu Onishi , Kenichi Ikeda , Takashi Shimaoka , Masanori Yoshida
发明人： Masanobu Onishi , Kenichi Ikeda , Takashi Shimaoka , Masanori Yoshida
IPC分类号： C07C17/093 , C07C17/35 , C07C22/08 , C07C25/13 , C07C39/24 , C07C43/225 , C07C43/23 , C07C45/51 , C07C47/55 , C07C49/80 , C07C51/09 , C07C51/60 , C07C69/157 , C07C69/76 , C07C233/65 , C07C243/22 , C07C255/50 , C07C265/12 , C07C309/86 , C07C309/87 , C07C311/16 , C07C317/44 , C07C331/28 , C07C255/10 , C07C323/09
CPC分类号： C07C331/28 , C07C17/093 , C07C17/35 , C07C22/08 , C07C25/13 , C07C39/24 , C07C43/225 , C07C43/23 , C07C45/515 , C07C47/55 , C07C49/80 , C07C51/09 , C07C51/60 , C07C69/76 , C07C233/65 , C07C243/22 , C07C255/50 , C07C265/12 , C07C309/86 , C07C309/87 , C07C311/16 , C07C317/44 , C07C63/70
摘要： Perfluoroisopropylbenzene derivatives of the general formula (I) or salts thereof, useful as intermediates or raw materials in the synthesis of various industrial materials including agricultural chemicals, drugs and surfactants: wherein X1 is H, halogen, formyl, optionally halogenated (C1-C6) alkyl, (C1-C6) alkylthio, or the like; X2 is H, halogen, formyl, hydroxyl, (C1-C6) alkyl, —C(═O)—R1 (wherein R1 is H, halogen, hydroxyl, (C1-C6) alkyl, or NR2R3, with R2 and R3 being each H, C1-6 alkyl, or the like), or the like; X3 is H, halogen, hydroxyl, cyano, isocyanate, hydrazino, diazo, —C(═O)—R1, —SO2—R4 (wherein R4 is halogen, hydroxyl, (C1-C6) alkyl, or NR5R6, with R5 and R6 being each H or (C1-C6) alkyl), or the like; and X4 is H, halogen, (C1-C6) alkyl, or (C1-C6) alkoxy, with publicly known compounds being excepted.
摘要翻译：通式（I）的全氟异丙基苯衍生物或其盐，可用作合成各种工业材料（包括农药，药物和表面活性剂）的中间体或原料：其中X 1是H，卤素，甲酰基，任选卤代（C 1 -C 6 -C 6）烷基，（C 1 -C 6 -C 6）烷硫基，或类似; X 2是H，卤素，甲酰基，羟基，（C 1 -C 6）烷基，-C（-O）-R 6，（其中R 1是H，卤素，羟基，（C 1 -C 6 -C 6）烷基或NR R 2 R 3和R 3各自为H，C 1-6烷基，烷基等）等; X 3是H，卤素，羟基，氰基，异氰酸酯，肼基，重氮基，-C（-O）-R 1，-SO 2 R 4是（其中R 4是卤素，羟基，（C 1 -C 6 -C 6）烷基，或NR 5 R 6，其中R 5和R 6各自为H或（C 1） C 6 -C 6烷基）等; 和X 4是H，卤素，（C 1 -C 6 -C 6）烷基或（C 1 -C 6 - C 6 -C 6烷氧基，其中公知的化合物除外。

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