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11. 发明授权

US08110149B2 Process for continuous preparation of high molecular weight polyesters by esterification of dicarboxylic acids and/or transesterification of dicarboxylic acids with diols and/or mixtures thereof and an apparatus therefor 有权
公开(公告)号：US08110149B2
公开(公告)日：2012-02-07
申请号：US12302254
申请日：2007-05-31
申请人： Eike Schulz Van Endert
发明人： Eike Schulz Van Endert
IPC分类号： B01J19/18 , B01J19/00 , B01J8/00 , B01J8/04 , B01J8/02 , B01J35/02 , C08F2/00 , C08G63/00
CPC分类号： B01J19/247 , B01J19/18 , B01J19/1862 , B01J19/20 , B01J2219/00006 , B01J2219/00081 , B01J2219/00083 , B01J2219/00085 , B01J2219/00087 , B01J2219/00092 , B01J2219/00094 , B01J2219/00103 , B01J2219/0011 , B01J2219/00159 , B01J2219/00768 , B01J2219/0077 , B01J2219/00779 , B01J2219/182 , B01J2219/185 , B01J2219/1943 , C08G63/78 , C08G63/785 , C08G63/83 , C08G63/85
摘要： The present invention relates to a method for the continuous production of high-molecular polyesters by esterification of dicarboxylic acids and/or transesterification of dicarboxylic acid esters with diols and/or mixtures thereof in the presence of catalysts with formation of a prepolymer in a tower reactor and polycondensation thereof to form a high-molecular polyester in a polycondensation reactor, a prepolymer with >40 to 70 repeat units (DP) being produced in the tower reactor and this prepolymer being polycondensed in only one further reactor to form a polyester with >150 to 205 DP.

12. 发明授权

US07897805B2 Polyisocyanate production method and polyisocyanate production system 有权
标题翻译：多异氰酸酯生产方法和多异氰酸酯生产系统
公开(公告)号：US07897805B2
公开(公告)日：2011-03-01
申请号：US11597757
申请日：2006-03-08
申请人： Masaaki Sasaki , Takao Naito , Fumiaki Hirata , Masato Saruwatari , Hirofumi Takahashi , Kouji Maeba , Tsugio Imaizumi , Takuya Saeki , Takashi Yamaguchi , Kouichirou Terada
发明人： Masaaki Sasaki , Takao Naito , Fumiaki Hirata , Masato Saruwatari , Hirofumi Takahashi , Kouji Maeba , Tsugio Imaizumi , Takuya Saeki , Takashi Yamaguchi , Kouichirou Terada
IPC分类号： C07C263/10
CPC分类号： C07C263/10 , B01J8/0453 , B01J2208/00256 , B01J2208/00265 , B01J2208/00274 , B01J2208/00283 , B01J2208/00646 , B01J2208/00716 , B01J2219/0004 , B01J2219/00103 , B01J2219/00105 , B01J2219/00108 , B01J2219/0011 , C07C265/14
摘要： A polyisocyanate production method that can allow effective use of hydrogen chloride produced secondarily in a polyisocyanate production process, while allowing reduction of environmental burdens, and a polyisocyanate production system for performing the polyisocyanate production method. After chlorine is allowed to react with carbon monoxide to produce carbonyl chloride in a carbonyl chloride producing reactor, the carbonyl chloride produced in the carbonyl chloride producing reactor is allowed to react with polyamine in an isocyanate producing reactor to produce polyisocyanate. Then, after hydrochloric gas produced secondarily in the isocyanate producing reactor is purified in a hydrogen chloride purifying column, the purified hydrochloric gas is oxidized in a hydrogen chloride oxidizing reactor to produce chlorine. Thereafter, the chlorine thus produced is supplied to the carbonyl chloride producing reactor from a chlorine resupply line, so that it is allowed to react with carbon monoxide to produce carbonyl chloride.
摘要翻译：能够有效利用多异氰酸酯制造方法中二次生成的氯化氢，同时可以减少环境负荷的多异氰酸酯的制造方法，以及进行多异氰酸酯的制造方法的多异氰酸酯的制造方法。在碳酰氯生成反应器中使氯与一氧化碳反应生成碳酰氯之后，使碳酰氯生产反应器中产生的碳酰氯与异氰酸酯生成反应器中的多胺反应，生成聚异氰酸酯。然后，在异氰酸酯制造反应器中二次生成的盐酸气体在氯化氢精制塔中纯化，在氯化氢氧化反应器中将纯化的氯化氢气体氧化，生成氯。此后，将由此产生的氯从氯再供给管路供给到碳酰氯生成反应器中，使其与一氧化碳反应，生成碳酰氯。

13. 发明申请

US20110028684A1 POLYMER STREAM TRANSFER 有权
标题翻译：聚合物流转移
公开(公告)号：US20110028684A1
公开(公告)日：2011-02-03
申请号：US12736450
申请日：2009-04-15
申请人： Daniel Marissal , Marc Parisel , Brent Walworth
发明人： Daniel Marissal , Marc Parisel , Brent Walworth
IPC分类号： C08F6/00
CPC分类号： B01J19/2415 , B01J19/2425 , B01J2208/00672 , B01J2219/00015 , B01J2219/00038 , B01J2219/00085 , B01J2219/00094 , B01J2219/00108 , B01J2219/0011 , B01J2219/00114 , B01J2219/00135 , B01J2219/00164 , B01J2219/00184 , B01J2219/00247 , B01J2219/00254 , B01J2219/182 , B01J2219/185 , B01J2219/1943 , B01J2219/1946 , C08F6/001 , F28F27/00 , C08L23/00
摘要： A process for heating a polymer-containing stream being transferred from a polymerization reactor to a separation zone or device, comprising passing the stream through at least two heaters operating in parallel, each heater comprising at least one transfer line for the stream and means for heating the transfer line, wherein the temperature of the polymer-containing stream at the outlet of all heaters is maintained above the dew point of the stream, and no heater has a volumetric flowrate of polymer-containing stream more than three times that of any other heater.
摘要翻译：一种用于加热从聚合反应器转移到分离区或装置的含聚合物流的方法，包括使所述流通过至少两个平行操作的加热器，每个加热器包括用于流的至少一个输送管线和加热装置传输线，其中所有加热器出口处的含聚合物流的温度保持在流的露点之上，并且没有加热器具有比任何其它加热器的加热器的体积流量高三倍以上的加热器。

14. 发明申请

US20100168473A1 PROCESS FOR THE PREPARATION OF UREA 有权
标题翻译：制备尿素的方法
公开(公告)号：US20100168473A1
公开(公告)日：2010-07-01
申请号：US12518118
申请日：2007-12-03
申请人： Stephen Rudolf Alexander Zwart , Johannes Henricus Mennen
发明人： Stephen Rudolf Alexander Zwart , Johannes Henricus Mennen
IPC分类号： C07C273/04
CPC分类号： B01D3/343 , B01D5/006 , B01J3/04 , B01J2219/00006 , B01J2219/00108 , B01J2219/0011 , B01J2219/00162 , C07C273/04
摘要： Process for the preparation of urea from ammonia and carbon dioxide in a urea production process comprising, in a high-pressure synthesis section: a. a reactor, wherein ammonia and carbon dioxide react to form a urea-comprising synthesis solution; b. a stripper, wherein the urea-comprising synthesis solution is heated and stripped, optionally in counter-current with a stripping agent; c. a submerged condenser, wherein the gas leaving the top of the stripper is, at least partially, condensed to form a condensate solution and d. an ejector, in the line connecting the submerged condenser and the reactor, supporting the transport of the condensate solution from the submerged condenser to the reactor, wherein a gas stream leaving the top of the submerged condenser is controlled by one or more controlling elements.
摘要翻译：在尿素生产过程中由氨和二氧化碳制备尿素的方法，包括在高压合成段：a。反应器，其中氨和二氧化碳反应以形成含尿素的合成溶液; b。汽提器，其中所述含脲的合成溶液被加热和汽提，任选地与汽提剂逆流; C。浸没冷凝器，其中离开汽提器顶部的气体至少部分地被冷凝以形成冷凝液和d。喷射器，在连接浸没冷凝器和反应器的管线中，支持将冷凝液从浸没冷凝器输送到反应器，其中离开浸没式冷凝器顶部的气流由一个或多个控制元件控制。

15. 发明申请

US20100168412A1 Continuous Neutralizer Mixer Reactor and a Continuous Process for Quenching Chlorination Reaction Mixture in Production of Chlorinated Sucrose 审中-公开
标题翻译：连续中和器搅拌器和氯化蔗糖生产中淬灭氯化反应混合物的连续方法
公开(公告)号：US20100168412A1
公开(公告)日：2010-07-01
申请号：US12226566
申请日：2007-04-19
申请人： Rakesh Ratnam , Sundeep Aurora , Sanjiv Shankar Anand , Subramaniyam
发明人： Rakesh Ratnam , Sundeep Aurora , Sanjiv Shankar Anand , Subramaniyam
IPC分类号： C07H1/06 , C07H1/00 , B01J19/18
CPC分类号： C07B39/00 , B01J19/0013 , B01J19/0066 , B01J19/0086 , B01J19/1881 , B01J2219/00006 , B01J2219/00033 , B01J2219/00063 , B01J2219/00094 , B01J2219/0011 , B01J2219/00177 , B01J2219/002 , B01J2219/00238 , C07H1/00 , C07H1/06 , C07H5/02
摘要： An improved process of production of a chlorinated sugar is described comprising chlorination of a partially protected sugar, wherein quenching as well as neutralization of chlorinated reaction mass is carried out concurrently and continuously in a reactor which is a continuous mixer as well as quencher providing continuous mixing of chlorination reaction mixture and pH adjusting solution and also provides for continuous quenching and continuous removal of quenched chlorinated reaction mixture.
摘要翻译：描述了制备氯化糖的改进方法，其包括氯化部分保护的糖，其中在连续混合器的反应器中同时且连续地进行淬灭和氯化反应物质的中和，以及提供连续混合的猝灭剂的氯化反应混合物和pH调节溶液，并且还提供连续淬火和连续除去淬灭的氯化反应混合物。

16. 发明申请

US20100093932A1 PROCESS FOR THE CONTINUOUS HYDROGENATION OF CARBON-CARBON DOUBLE BONDS IN AN UNSATURATED POLYMER 审中-公开
标题翻译：在不饱和聚合物中碳碳双重连续加氢的方法
公开(公告)号：US20100093932A1
公开(公告)日：2010-04-15
申请号：US12506528
申请日：2009-07-21
申请人： GARRY REMPEL , QINMIN PAN , CHANDRA MOULI MADHURANTHAKAM
发明人： GARRY REMPEL , QINMIN PAN , CHANDRA MOULI MADHURANTHAKAM
IPC分类号： C08F8/04
CPC分类号： C08F236/08 , B01F5/0619 , B01F5/10 , B01F7/18 , B01J10/00 , B01J19/1881 , B01J19/32 , B01J2219/00094 , B01J2219/0011 , B01J2219/00184 , B01J2219/32206 , B01J2219/32262 , B01J2219/32265 , B01J2219/3306 , B01J2219/3322 , C08C19/02 , C08F236/10 , C08F236/12
摘要： Proposed is a process for the continuous hydrogenation of carbon-carbon double bonds in an unsaturated polymer based on a conjugated diolefin and at least one other copolymerizable monomer to produce a hydrogenated polymer, in the presence of a solvent and a homogeneous or heterogeneous catalyst, wherein said unsaturated polymer, said homogeneous or heterogeneous catalyst and hydrogen are passed through a reactor equipped with static internal elements.
摘要翻译：提出了在溶剂和均相或非均相催化剂存在下，基于共轭二烯烃和至少一种其它可共聚单体的不饱和聚合物中碳 - 碳双键的连续氢化生产氢化聚合物的方法，其中所述不饱和聚合物，所述均相或非均相催化剂和氢气通过装有静态内部元件的反应器。

17. 发明授权

US07649109B2 Polyester production system employing recirculation of hot alcohol to esterification zone 有权
标题翻译：聚酯生产系统采用热酒精再循环到酯化区
公开(公告)号：US07649109B2
公开(公告)日：2010-01-19
申请号：US11635411
申请日：2006-12-07
申请人： Bruce Roger DeBruin
发明人： Bruce Roger DeBruin
IPC分类号： C07C51/16
CPC分类号： B01J10/002 , B01D3/14 , B01D19/0036 , B01J19/24 , B01J2219/00006 , B01J2219/00103 , B01J2219/0011 , B01J2219/0025 , B01J2219/182 , B01J2219/185 , B01J2219/1943 , C08G63/78
摘要： A polyester production process employing an esterification system that uses a distillation column to recover alcohol produced from an esterification zone and then recirculates the recovered alcohol back to the esterification zone without substantially cooling the recovered alcohol.
摘要翻译：使用酯化系统的聚酯制备方法，其使用蒸馏塔来回收由酯化区产生的醇，然后将回收的醇再循环回酯化区，而基本上不回收醇。

18. 发明授权

US07608225B2 Tower reactor and use thereof for the continuous production of high molecular weight polyesters 失效
标题翻译：塔式反应器及其用于连续生产高分子量聚酯的用途
公开(公告)号：US07608225B2
公开(公告)日：2009-10-27
申请号：US10573937
申请日：2004-10-29
申请人： Eike Schulz Van Endert , Christian Atlas
发明人： Eike Schulz Van Endert , Christian Atlas
IPC分类号： B01J19/00 , C08F2/00
CPC分类号： C08G63/785 , B01J19/1887 , B01J19/247 , B01J2219/00094 , B01J2219/00103 , B01J2219/0011 , B01J2219/00162 , B01J2219/00166 , B01J2219/00247
摘要： The invention relates to a tower reactor and the use thereof for producing high-molecular weight polyesters, such as e.g. polyethylene terephthalate (PET), polybutylene terephthalate (PBT), polynaphthalene terephthalate (PEN), polytrimethylene terephthalate (PTT) and/or polyesters of other dicarboxylic acids and diols including copolymers thereof. It thereby concerns a single-stage tower reactor.
摘要翻译：本发明涉及塔式反应器及其用于生产高分子量聚酯的用途，聚对苯二甲酸乙二醇酯（PET），聚对苯二甲酸丁二醇酯（PBT），聚萘二甲酸对苯二甲酸酯（PEN），聚对苯二甲酸丙二醇酯（PTT）和/或其他二羧酸和二醇的聚酯，包括它们的共聚物。因此涉及单级塔式反应器。

19. 发明申请

US20090192285A1 Method and device for the production of polyesters and copolyesters 审中-公开
标题翻译：用于生产聚酯和共聚酯的方法和装置
公开(公告)号：US20090192285A1
公开(公告)日：2009-07-30
申请号：US10585470
申请日：2004-12-14
申请人： Fritz Wilhelm , Stefan Deiss
发明人： Fritz Wilhelm , Stefan Deiss
IPC分类号： C08G63/78 , B01J19/00
CPC分类号： B01J19/0013 , B01D5/0027 , B01J2219/0011 , B01J2219/00123 , B01J2219/0013 , C08G63/181 , C08G63/785
摘要： Disclosed is a method for producing polyesters by means of esterification or re-esterification, precondensation of the esterified/re-esterified product, and polycondensation of the precondensed product at a pressure of 0.2 to 500 mbar and a temperature of 230 to 330° C. According to said method, the vapors formed during precondensation and polycondensation are condensed and the obtained cooled diol is redirected into the condensation stage. In order to improve the degree of separation, the vapors are directed into a bottomless direct contact condenser, the base of which is immersed into the top funnel-shaped section of a barometrically dipped downpipe so as to form an annular space, cooled diol is sprayed into the vapors in the top section of the direct contact condenser, the remaining vapors are recovered via the annular space, and the formed polymer aggregates are removed.
摘要翻译：公开了通过酯化或再酯化制备聚酯的方法，酯化/再酯化产物的预缩合，以及在0.2至500毫巴的压力和230至330℃的温度下预缩合产物的缩聚。根据所述方法，在预缩合和缩聚期间形成的蒸气被冷凝，并将获得的冷却的二醇重新导向冷凝阶段。为了提高分离度，将蒸气引导到无底直接接触冷凝器中，将其底部浸入气压下降管的顶部漏斗形部分中以形成环形空间，冷却的二醇被喷射进入直接接触冷凝器顶部的蒸气中，剩余的蒸气经由环形空间回收，并且形成的聚合物聚集体被去除。

20. 发明申请

US20090187052A1 REACTOR AND METHOD FOR REACTING AT LEAST TWO GASES IN THE PRESENCE OF A LIQUID PHASE 失效
标题翻译：在液相存在下反应至少两种气体的反应器和方法
公开(公告)号：US20090187052A1
公开(公告)日：2009-07-23
申请号：US11719652
申请日：2005-11-18
申请人： Michel Strebelle , Michel Lempereur
发明人： Michel Strebelle , Michel Lempereur
IPC分类号： C07C17/02 , B01J19/26
CPC分类号： B01J12/00 , B01F5/0453 , B01F5/046 , B01J19/26 , B01J2219/0011 , C07C17/02 , C07C17/04 , C07C19/045 , C07C19/05
摘要： A reactor for reacting at least two gases in the presence of a liquid phase, provided with an external liquid phase circulation device and including at least one injector for injecting the gases and the externally circulated liquid phase. In the injector the mixing of the gases together and with the externally circulated liquid phase only begins at the outlet of the injector.
摘要翻译：一种在液相存在下使至少两种气体反应的反应器，其具有外部液相循环装置，并且包括至少一个注入气体和外部循环液相的注射器。在注射器中，气体与外部循环液相的混合仅在注射器的出口处开始。

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