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11. 发明授权

US4144093A Process for machine washing of soiled articles using a water-insoluble cation-exchange polymer 失效
标题翻译：使用水不溶性阳离子交换聚合物对脏物进行机洗的方法
公开(公告)号：US4144093A
公开(公告)日：1979-03-13
申请号：US821968
申请日：1977-08-04
申请人： Elmar Reinwald , Milan J. Schwuger , Heinz Smolka , Peter Krings
发明人： Elmar Reinwald , Milan J. Schwuger , Heinz Smolka , Peter Krings
IPC分类号： A47L15/42 , B01J47/10 , C11D3/37 , C11D11/00 , D06F39/10 , B08B7/04
CPC分类号： D06F39/10 , A47L15/4229 , B01J47/10 , C11D11/0017 , C11D3/37 , C11D3/3761 , C11D3/3769
摘要： The machine washing of solid material (e.g. dishes and clothes) in hard water areas is enhanced when the washing solution has a dissolved content of a sequestering agent for calcium ions and is contacted with an insoluble cation exchange resin in particulate state, the washing solution being passed through a filter containing the resin during the course of the washing operation. The filter is maintained separate and spaced from the washing area. The cation exchange resin may be contained in a filter of the whirlpool type, so that the particles are maintained in aqueous suspension without coming into contact with the materials being washed, or it may be contained as a unitary porous lining of a filter.
摘要翻译：当洗涤溶液具有溶解的钙离子螯合剂的含量并且与颗粒状态的不溶性阳离子交换树脂接触时，在硬水区域中的固体材料（例如餐具和衣物）的机洗被增强，洗涤溶液为在洗涤操作过程中通过含有树脂的过滤器。过滤器与洗涤区分离并保持间隔。阳离子交换树脂可以包含在漩涡型过滤器中，使得颗粒保持在水性悬浮液中而不与被洗涤的材料接触，或者可以作为过滤器的整体多孔衬里包含。

12. 发明授权

US4071377A Method of mechanical dishwashing and compositions 失效
标题翻译：机械洗碗和组合物的方法
公开(公告)号：US4071377A
公开(公告)日：1978-01-31
申请号：US458333
申请日：1974-04-05
申请人： Milan Johann Schwuger , Heinz Smolka , Theodor Altenschopfer , Manfred Rostek
发明人： Milan Johann Schwuger , Heinz Smolka , Theodor Altenschopfer , Manfred Rostek
IPC分类号： C11D7/60 , A47L15/44 , C11D3/00 , C11D3/02 , C11D3/08 , C11D3/10 , C11D3/12 , A47L15/00 , C02B1/44 , C11D3/60
CPC分类号： C11D3/128 , C11D1/72 , C11D11/0023 , C11D3/044 , C11D3/08 , C11D3/10 , C11D3/3955 , Y10S423/24
摘要： A method for the mechanical washing of dishes, wherein the soiled dishes are treated with an aqueous alkaline liquor having a pH of from 8 to 13 which contains at least one compound inhibiting alkaline earth metal ion precipitation, rinsing and recovering cleaned dishes comprising using finely-dispersed, water-insoluble silicate compounds having a calcium-binding power of at least 50 mg CaO/gm of anhydrous substance and having the formula, combined water not shown, of(M.sub.2/n O).sub.x .multidot. Me.sub.2 O.sub.3 .multidot. (SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a number of from 0.7 to 1.5, Me is a member selected from aluminum and boron and y is a number of from 0.8 to 6, as said compound inhibiting alkaline earth metal ion precipitation as well as alkaline-reacting mechanical dish washing compositions containing said silicate compounds.
摘要翻译：一种用于机械洗涤餐具的方法，其中用含有至少一种抑制碱土金属离子沉淀的化合物的pH为8至13的碱性水溶液处理污染的菜肴，冲洗并回收清洁的菜肴，（M2 / nO）xxMe2O3 x（SiO2）y WHERE M为（M2 / nO）xxMe2O3 x（SiO2）y的组合水，分散的水不溶性硅酸盐化合物，其钙结合能力为至少50mg CaO / gm无水物质，化合价n的阳离子可与钙交换，x为0.7〜1.5，Me为选自铝和硼的成员，y为0.8〜6的数，作为所述抑制碱土金属离子析出的化合物以及含有所述硅酸盐化合物的碱性反应机械洗碗组合物。

13. 发明授权

US3962116A Compositions of optical brightness and aluminosilicates and methods of their production 失效
标题翻译：光学亮度和铝酸盐的组成及其生产方法
公开(公告)号：US3962116A
公开(公告)日：1976-06-08
申请号：US541208
申请日：1975-01-15
申请人： Helmut Bloching , Heinz Smolka , Milan Johann Schwuger
发明人： Helmut Bloching , Heinz Smolka , Milan Johann Schwuger
IPC分类号： D06L3/12 , C09K11/30
CPC分类号： D06L3/1264
摘要： Heat dried, finely-divided compositions of optical brighteners and fillers comprising as said fillers at least partly of a finely-divided water-insoluble silicate compound containing at least some combined water and having a calcium binding power of at least 50 mg CaO/gm of anhydrous active substance and the formula on the anhydrous basis(M.sub.2 /.sub.n O).sub.x . Me.sub.2 O.sub.3 . (SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a member of from 0.7 to 1.5, Me is a member selected from the group consisting of aluminum and boron, and y is a number from 0.8 to 6, preferably from 1.3 to 4, in an amount of at least 5% by weight of the mixture, as well as a process for producing the same comprising the steps of mixing said silicate compound, while at least still moist from its production, with said optical brighteners and converting the entire mixture of components into a pourable product.
摘要翻译： 1499902荧光增白剂和填充剂DEUTSCHE GOLD - UND SILBER-SCHEIDEAN雪松和HENKEL＆CIE GmbH 1975年1月16日[1974年1月17日] 1869/75标题D1P干粉状组合物含有荧光增白剂和细分（最大粒径0.1mm）具有至少50mg CaO / g无水硅酸盐（= AS）的钙结合能力和通式的水不溶性铝 - 或硼硅酸盐; 其中Cat表示可与钙交换的阳离子和n价的x，x表示0.7至1.5的数，M表示硼或铝，y表示0.8至6的数。可交换阳离子可以是氢，锂，钾，铵或镁或水溶性有机碱的阳离子，但优选为钠。增白剂对棉，聚酰胺或聚酯可能是实质的，并且可以是二氨基芪二磺酸，二芳基吡唑啉喹诺酮，1,2-二（2-苯并恶唑基） - 或1,2-二 - （2-苯甲酰亚氨基唑基） - 乙烯，苯并恶唑基噻吩，香豆素或曲辛二烯二苯基衍生物。组合物可以通过热干燥形成。通过单一喷雾或辊子，组分的浆料。在改性中，形成硅酸盐，例如，通过将铝酸钠和硅酸钠混合在水性悬浮液中，在光亮剂存在下，其在干燥时由硅酸盐涂覆。因此可以形成空心珠。硅酸盐可以是无定形或微晶的。其他水溶性或细分散的水不溶性惰性物质也可能存在。

14. 发明授权

US4092261A Process for the production of powdery washing and cleansing agent compositions 失效
标题翻译：生产粉状洗涤剂和清洁剂组合物的方法
公开(公告)号：US4092261A
公开(公告)日：1978-05-30
申请号：US620386
申请日：1975-10-07
申请人： Gerhard Sperling , Dieter Jung , Klaus Hachmann , Milan Johann Schwuger , Heinz Smolka
发明人： Gerhard Sperling , Dieter Jung , Klaus Hachmann , Milan Johann Schwuger , Heinz Smolka
IPC分类号： C11D1/02 , C11D1/66 , C11D1/72 , C11D1/88 , C11D3/00 , C11D3/12 , C11D10/04 , C11D11/00 , C02B1/44 , C11D9/18 , C11D11/02
CPC分类号： C11D11/0082 , C11D10/04 , C11D3/128 , C11D1/02 , C11D1/66 , C11D1/72 , C11D1/88
摘要： An improvement in the process for the production of powdery washing and cleansing agent compositions containing finely-divided water-insoluble silicate compounds, capable of binding calcium, soap, and, optionally, other surface-active compounds, builders and other customary detergent additives by spray-drying a slurry and recovering said powdery washing and cleansing agent composition which comprises separately spray-drying a slurry rich in said silicate compounds and combining the spray-dried powders with the remaining ingredients in powdery form; as well as the powdery washing and cleansing agents so produced.
摘要翻译：生产含有精细分散的水不溶性硅酸盐化合物的粉末洗涤和清洁剂组合物的方法的改进，其能够通过喷雾结合钙，皂和任选的其它表面活性化合物，助洗剂和其它常规洗涤剂添加剂干燥浆料并回收所述粉末洗涤和清洁剂组合物，其包括分别喷雾富含所述硅酸盐化合物的浆料并将喷雾干燥的粉末与粉末形式的其余成分组合; 以及如此生产的粉末洗涤和清洁剂。

15. 发明授权

US4121903A Method of machine washing of solid soiled materials by contacting the circulating wash liquid with aluminosilicates 失效
标题翻译：通过使循环洗涤液与铝硅酸盐接触来洗涤固体污染物质的方法
公开(公告)号：US4121903A
公开(公告)日：1978-10-24
申请号：US847791
申请日：1977-11-02
申请人： Heinz Smolka
发明人： Heinz Smolka
IPC分类号： B08B3/08 , A47L15/42 , B01D15/04 , C11D3/12 , C11D11/00 , D06F39/10 , D06L1/12 , B08B3/00
CPC分类号： C11D11/0017 , A47L15/4229 , C11D11/0023 , C11D11/007 , C11D3/12 , C11D3/1246 , C11D3/128 , D06F39/10 , D06L1/12
摘要： An improvement in the machine washing of solid soiled materials comprising withdrawing and recycling the tap water in contact with said solid soiled materials through a silicate cation exchange compound having some combined water and a particle size of between 10 .mu. and 100 .mu. of the formula(M.sub.2/n O).sub.x . Me.sub.2 O.sub.3 . (SiO.sub.2).sub.ywherein M is a cation of valence n exchangeable with calcium, Me is a member selected from aluminum and boron, x is a number from 0.7 to 1.5 and y is a number from 0.8 to 6, said agent having a calcium binding power of at least 50 mg of CaO per gram, said agent being maintained out of contact with said solid soiled materials, for such time until the water has a hardness of not more than 70 mg CaO/liter, then adding other soluble washing and cleaning compounds to said softened tap water and washing said solid materials while continuing the recycling of the wash solution through said silicate cation exchange compound.
摘要翻译：固体污染材料的机器洗涤改进包括通过具有一定组合水和粒径为10-100微米的式（M2）的硅酸盐阳离子交换化合物来回收和再循环与所述固体污染物接触的自来水 / nO）x。 Me2O3。（SiO 2）y WHEREIN M是可与钙交换的价态的阳离子，Me是选自铝和硼的成员，x是0.7至1.5的数，y是0.8至6的数，所述试剂具有钙结合每克至少50mg CaO的功率，所述试剂与所述固体污染的材料保持脱离接触直到水具有不超过70mg CaO /升的硬度，然后加入其它可溶性洗涤和清洁化合物到所述软化的自来水并洗涤所述固体材料，同时继续通过所述硅酸盐阳离子交换化合物再循环洗涤溶液。

16. 发明授权

US4120653A Method of machine washing of solid soiled materials by contacting the circulating wash liquid with organic cationic exchange resins 失效
标题翻译：通过使循环洗涤液与有机阳离子交换树脂接触来清洗固体污染物的方法
公开(公告)号：US4120653A
公开(公告)日：1978-10-17
申请号：US847792
申请日：1977-11-02
申请人： Heinz Smolka
发明人： Heinz Smolka
IPC分类号： B08B3/08 , C11D3/37 , C11D11/00 , D06F39/10 , B08B3/00
CPC分类号： C11D11/0011 , C11D3/3788 , D06F39/10
摘要： An improvement in the machine washing of solid soiled materials comprising withdrawing and recycling the tap water in contact with said solid soiled materials through a water-insoluble cation exchange polymer in particulate state having a swelled average particle diameter in excess of 20 .mu. and having a calcium binding power of at least 2 mVal per gram, said polymers being maintained out of contact with said solid soiled materials, for such time until the water has a hardness of not more than 70 mg CaO/liter, then adding other soluble washing and cleaning compounds to said softened tap water and washing said solid materials while continuing the recycling of the wash solution through said cation exchange polymer.
摘要翻译：固体污染物质的机洗方面的改进包括：通过水溶性阳离子交换聚合物将具有膨胀的平均粒径超过20微米并具有钙的水不溶性阳离子交换聚合物取出并再循环与所述固体污染物接触的自来水所述聚合物与所述固体污染的材料保持不接触的时间直到水具有不超过70mg CaO /升的硬度，然后加入其它可溶性洗涤和清洁化合物到所述软化的自来水并洗涤所述固体材料，同时继续通过所述阳离子交换聚合物再循环洗涤溶液。

17. 发明授权

US4083793A Washing compositions containing aluminosilicates and nonionics and method of washing textiles 失效
标题翻译：含有硅铝酸盐和非离子表面活性剂的洗涤组合物和洗涤纺织品的方法
公开(公告)号：US4083793A
公开(公告)日：1978-04-11
申请号：US723728
申请日：1976-09-16
申请人： Gunter Jakobi , Peter Krings , Milan Johann Schwuger , Heinz Smolka
发明人： Gunter Jakobi , Peter Krings , Milan Johann Schwuger , Heinz Smolka
IPC分类号： C11D1/83 , C11D3/08 , C11D3/12 , B01J1/04 , C11D1/825 , C11D1/831
CPC分类号： C11D3/08 , C11D1/8305 , C11D3/1286
摘要： A method of washing soiled textiles, wherein the soiled textiles are immersed in an aqueous liquor which contains at least one compound inhibiting alkaline earth metal ion precipitation on said soiled textiles and surface-active compounds comprising using finely-dispersed, water-insoluble silicate compounds having a calcium-binding power of at least 50 mg CaO/gm of anhydrous active substance and having the formula, combined water not shown(M.sub.2/n O).sub.x . Me.sub.2 O.sub.3 . (SiO.sub.2).sub.ywhere M is a cation of the valence n, exchangeable with calcium, x is a number of from 0.7 to 1.5, Me is a member selected from aluminum and boron and y is a number of from 0.8 to 6, as said compound inhibiting alkaline earth metal ion precipitation, together with surface-active compounds including non-ionic surface-active compounds being constituted by a mixture of compounds of different degrees of ethoxylation where one of the ethoxylated compounds has 8 to 20 ethylene oxide units and the other has from 2 to 6 ethylene oxide units; as well as washing compositions containing said silicate compounds and said surface-active compounds.
摘要翻译：一种洗涤污染织物的方法，其中将污染的纺织品浸入含有至少一种抑制碱土金属离子沉淀的化合物的水性液体中，所述化合物在所述污染的纺织品和表面活性化合物上包括使用细分散的水不溶性硅酸盐化合物，具有至少50mg CaO / gm无水活性物质并具有下式的组合水（M2 / nO）x的钙结合力。 Me2O3。（SiO 2）y其中M是价数为n的阳离子，可与钙交换，x为0.7至1.5的数，Me为选自铝和硼的成员，y为0.8至6的数，如所述化合物抑制碱土金属离子沉淀，以及包括非离子表面活性化合物在内的表面活性化合物由不同程度乙氧基化的化合物的混合物构成，其中一种乙氧基化合物具有8至20个环氧乙烷单元，另一种具有2至6个环氧乙烷单元; 以及含有所述硅酸盐化合物和所述表面活性化合物的洗涤组合物。

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