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11. 发明授权

US5536876A Formylamino-aminophenol compounds and their use in preparation of fiber-reactive formazan dyes 失效
标题翻译：甲酰氨基 - 氨基苯酚化合物及其在制备纤维反应型甲an染料中的应用
公开(公告)号：US5536876A
公开(公告)日：1996-07-16
申请号：US332095
申请日：1994-10-31
申请人： Claus Marschner , Manfred Patsch
发明人： Claus Marschner , Manfred Patsch
IPC分类号： C07C233/43 , C09B62/04 , C09B62/44 , D06P1/382 , C07C233/07
CPC分类号： C09B62/4407 , C07C233/43 , C09B62/046 , Y02P20/55
摘要： Fiber-reactive formazan dyes are prepared by diazotizing a protectively formylated hydroxyphenylenediamine, coupling with a hydrazone compound, metallizing, eliminating the protective group, and reacting with a halotriazine and optionally thereafter with an amine or a hydroxy compound via novel aminophenol intermediates.
摘要翻译：通过将保护性甲酰化羟基苯二胺重氮化，与腙化合物偶合，金属化，除去保护基，并与卤代三嗪反应，然后任选地通过新的氨基苯酚中间体与胺或羟基化合物反应制备纤维反应性甲an染料。

12. 发明授权

US5175259A Mono- and bis-azo compounds containing 6-hydroxy-3-heterocyclic onium-pyridone-2-groupings coupled to diazo components containing diazine or triazine rings 失效
标题翻译：含有6-羟基-3-杂环基的β-吡咯烷酮-2-基团的单 - 和双 - 异氰酸酯化合物与含有二氮杂环或三嗪环的DIAZO组分相连
公开(公告)号：US5175259A
公开(公告)日：1992-12-29
申请号：US843193
申请日：1992-02-28
申请人： Joerg L. Jessen , Manfred Ruske , Knut Kessel , Manfred Patsch
发明人： Joerg L. Jessen , Manfred Ruske , Knut Kessel , Manfred Patsch
IPC分类号： C09B62/085 , C09B62/04 , C09B62/245 , C09B62/44 , C09B62/51 , D06P1/38
CPC分类号： C09B62/245 , C09B62/04 , C09B62/4411
摘要： Reactive dyes of the formula ##STR1## where n is 1 or 2,X is a six-membered halogen-containing nitrogen heterocycle,L.sup.1, depending on n, is fluorine, chlorine, C.sub.1 -C.sub.4 -alkoxy, phenoxy, C.sub.1 -C.sub.4 -alkyl, substituted or unsubstituted phenyl or a bridge member which has one or two hydroxysulfonyl groups,D is the radical of a diazo component of the aniline or naphthalene series which has at least one hydroxysulfonyl group,L.sup.2 is hydrogen or substituted or unsubstituted C.sub.1 -C.sub.8 -alkyl,L.sup.3 is the cationic radical of an aromatic heterocycle which is linked to the pyridone ring via a nitrogen atom, andL.sup.4 is hydrogen or C.sub.1 -C.sub.4 -alkyl,with the proviso that the number of hydroxysulfonyl groups in the molecule exceeds that of the cationic groups by at least one, are useful for dyeing and printing hydroxyl- or nitrogen-containing substrates.
摘要翻译：式中，n为1或2的反应性染料，X为6元含卤素的氮杂环，L1取决于n，为氟，氯，C 1 -C 4 - 烷氧基，苯氧基，C 1 -C 4 - 烷基，取代或未取代的苯基或具有一个或两个羟基磺酰基的桥连构件，D是具有至少一个羟基磺酰基的苯胺或萘系的重氮组分的基团，L2是氢或取代或未取代的C1-C8 - 烷基，L3是通过氮原子与吡啶酮环连接的芳族杂环的阳离子基团，L4是氢或C1-C4-烷基，条件是分子中羟基磺酰基的数目超过通过至少一个的阳离子基团可用于染色和印刷含羟基或含氮底物。

13. 发明授权

US5336800A Mixed oxamides 失效
标题翻译：混合草酰胺
公开(公告)号：US5336800A
公开(公告)日：1994-08-09
申请号：US000295
申请日：1993-01-04
申请人： Bernd Siegel , Manfred Patsch , Knut Kessel
发明人： Bernd Siegel , Manfred Patsch , Knut Kessel
IPC分类号： C07D241/04 , C07C315/04 , C07C317/28 , C07C317/32 , C07C317/40 , C07D295/185 , C09B62/503 , C07C305/12 , C07C69/003 , C07C69/12 , C07C205/06 , C07C205/42 , C07C317/06
CPC分类号： C07D295/185 , C07C317/28 , C07C317/40 , C09B62/503
摘要： Oxamides useful as dye intermediates have the formula ##STR1## where R.sup.1 and R.sup.2 are independently of each other hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,X is hydroxyl, nitro or a radical of the formula --NR.sup.3 R.sup.4, where R.sup.3 is hydrogen or C.sub.1 -C.sub.4 -alkanoyl and R.sup.4 is hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,Z is C.sub.2 -C.sub.8 -alkylene, substituted or unsubstituted phenylene or substituted or unsubstituted naphthylene, or X--Z and R.sup.1 are, together with the nitrogen atom joining them together, the radical of the formula ##STR2## where R.sup.3 is as defined above,L is a bridge member andY is vinyl or a radical of the formula --C.sub.2 H.sub.4 --A, where A is hydroxyl or a group which is detachable under alkaline reaction conditions.
摘要翻译：可用作染料中间体的酰胺具有式“IMAGE”，其中R 1和R 2彼此独立地为氢，C 1 -C 4烷基或苯基，X为羟基，硝基或式-NR 3 R 4基团，其中R 3为氢或C 1 -C4-烷酰基和R4是氢，C1-C4-烷基或苯基，Z是C2-C8-亚烷基，取代或未取代的亚苯基或取代或未取代的亚萘基，或XZ和R1与连接在一起的氮原子一起，式为“IMAGE”的基团，其中R3如上所定义，L为桥连构件，Y为乙烯基或式-C 2 H 4 -A的基团，其中A为羟基或在碱性反应条件下可分离的基团。

14. 发明授权

US5493057A Chloroethylsulfonylbenzaldehydes 失效
标题翻译：氯乙磺酰苯甲醛
公开(公告)号：US5493057A
公开(公告)日：1996-02-20
申请号：US57830
申请日：1993-05-07
申请人： Claus Marschner , Manfred Patsch
发明人： Claus Marschner , Manfred Patsch
IPC分类号： C07C317/24 , C07C317/14
CPC分类号： C07C317/24
摘要： Chloroethylsulfonylbenzaldehydes of the formula ##STR1## where n is 1 or 2 and the ring A may be substituted with halogen, C.sub.1 -C.sub.4 alkyl, C.sub.1 -C.sub.4 alkoxy, C.sub.1 -C.sub.4 alkysulfonyl, nitro or hydroxysulfonyl, are prepared.
摘要翻译：其中n为1或2并且环A可以被卤素，C 1 -C 4烷基，C 1 -C 4烷氧基，C 1 -C 4亚烷基磺酰基，硝基或羟基磺酰基取代的式（I）的氯乙基磺酰基苯甲醛。

15. 发明授权

US5488100A Formazan-based reactive dyes with at least two reactive groups, and aminophenols 失效
标题翻译：具有至少两个反应性基团的甲an基活性染料和氨基苯酚
公开(公告)号：US5488100A
公开(公告)日：1996-01-30
申请号：US407955
申请日：1995-03-22
申请人： Claus Marschner , Manfred Patsch
发明人： Claus Marschner , Manfred Patsch
IPC分类号： C07C323/44 , C07C317/28 , C07D295/20 , C09B62/018 , C09B62/44 , C09B62/503 , C09B62/463 , D06P1/384
CPC分类号： C09B62/4401 , C07C317/28 , C09B62/018 , C09B62/5036
摘要： There are described formazan dyes of the formula ##STR1## where m and n are each 1 or 2,Kat.sup..sym. is the equivalent of a cation,Me is copper or nickel,X is oxygen or a radical of the formula CO--O or SO.sub.2 --O,Y is vinyl or a radical of the formula C.sub.2 H.sub.4 --Q, wherein Q is a group that is detachable under alkaline reaction conditions,E is a fiber-reactive radical,the rings A and B may be substituted and benzofused, andthe ring C may be substituted,the use thereof for dyeing or printing hydroxyl- or nitrogen-containing organic substrates, novel aminophenols and a process for preparing same.
摘要翻译：描述了式IMAMA的甲an染料，其中m和n各自为1或2，Kat（+）为阳离子的当量，Me为铜或镍，X为氧或式CO-O基团或SO 2 -O，Y是乙烯基或式C 2 H 4 -Q的基团，其中Q是在碱性反应条件下可分离的基团，E是纤维反应性基团，环A和B可以被取代和苯并，并且环C可以被取代，其用于染色或印刷羟基或含氮有机底物，新型氨基苯酚及其制备方法的用途。

16. 发明授权

US5446193A Formazan-based reactive dyes with at least two reactive groups, and aminophenols 失效
标题翻译：具有至少两个反应性基团的甲an基活性染料和氨基苯酚
公开(公告)号：US5446193A
公开(公告)日：1995-08-29
申请号：US136131
申请日：1993-10-15
申请人： Claus Marschner , Manfred Patsch
发明人： Claus Marschner , Manfred Patsch
IPC分类号： C07C323/44 , C07C317/28 , C07D295/20 , C09B62/018 , C09B62/44 , C09B62/503 , C07C305/12 , C07C309/29 , C07D213/02
CPC分类号： C09B62/4401 , C07C317/28 , C09B62/018 , C09B62/5036
摘要： There are described formazan dyes of the formula ##STR1## where m and n are each 1 or 2,Kat is the equivalent of a cation,Me is copper or nickel,X is oxygen or a radical of the formula CO-O or SO.sub.2 -O,Y is vinyl or a radical of the formula C.sub.2 H.sub.4 -Q, wherein Q is a group that is detachable under alkaline reaction conditions,E is a fiber-reactive radical,the rings A and B may be substituted and benzofused, andthe ring C may be substituted,the use thereof for dyeing or printing hydroxyl- or nitrogen-containing organic substrates, novel aminophenols and a process for preparing same.
摘要翻译：描述了通式“IMAGE”的甲an染料，其中m和n各自为1或2，Kat为阳离子的等价物，Me为铜或镍，X为氧或式CO-O或SO2- O，Y是乙烯基或式C2H4-Q的基团，其中Q是在碱性反应条件下可分离的基团，E是纤维反应性基团，环A和B可以被取代和苯并稠合，环 C可以被取代，其用于染色或印刷含羟基或含氮有机底物，新型氨基苯酚及其制备方法的用途。

17. 发明授权

US5405993A Reactive formazan dyes and hydrazones 失效
标题翻译：活性甲an染料和腙
公开(公告)号：US5405993A
公开(公告)日：1995-04-11
申请号：US288242
申请日：1994-08-09
申请人： Claus Marschner , Manfred Patsch
发明人： Claus Marschner , Manfred Patsch
IPC分类号： C07C317/32 , C07C317/44 , C07C381/02 , C09B62/503 , C07C251/86 , C07C309/29 , C07C309/35
CPC分类号： C09B62/5036 , C07C317/44 , C07C381/02
摘要： There are described formazan dyes of the formula ##STR1## where n is 1 or 2,Kat.cndot. is the equivalent of a cation,Me is copper or nickel,X is a radical of the formula CO-O or SO.sub.2 -O,Y is vinyl or a radical of the formula C.sub.2 H.sub.4 -Q, where Q is a group which is detachable under alkaline reaction conditions,the ring A may be substituted and benzofused,the ring B is substituted and may be benzofused, andthe ring C may be substituted,the use thereof for dyeing or printing hydroxyl- or nitrogen-containing organic substrates, and novel hydrazones.
摘要翻译：描述了通式为“IMAGE”的甲an染料，其中n为1或2，Kat。相当于阳离子，Me是铜或镍，X是式CO-O或SO2-O的基团，Y是乙烯基或式C2H4-Q的基团，其中Q是可以在碱性反应条件下，环A可以被取代和苯并稠合，环B被取代并且可以是苯并稠合的，并且环C可以被取代，其用于染色或印刷含羟基或含氮有机底物的用途以及新的腙。

18. 发明授权

US5210187A Double attachment reactive dyes having alkyl- or alkenylsulfonyl and alkyl- or alkenylsulfonylalkyl groups 失效
标题翻译：具有烷基或烯基磺酰基和烷基 - 或烯基磺酰基烷基的双连接活性染料
公开(公告)号：US5210187A
公开(公告)日：1993-05-11
申请号：US865744
申请日：1992-04-09
申请人： Manfred Patsch , Uwe Nahr , Friedrich Wirsing , Joerg L. Jessen , Klaus Pandl , Claus Marschner , Matthias Dust
发明人： Manfred Patsch , Uwe Nahr , Friedrich Wirsing , Joerg L. Jessen , Klaus Pandl , Claus Marschner , Matthias Dust
IPC分类号： C07C317/14 , C07C317/32 , C09B62/02 , C09B62/44 , C09B62/503
CPC分类号： C09B62/4403 , C07C317/14 , C07C317/32 , C09B62/02 , C09B62/503
摘要： Double attachment reactive dyes have the formula ##STR1## where U.sup.1 is C.sub.1 -C.sub.4 -alkyl, phenyl, C.sub.2 -C.sub.10 -alkenyl or the radical ##STR2## where Q.sup.1 and Q.sup.2 are each independently of the other hydrogen or C.sub.1 -C.sub.4 -alkyl and Q.sup.3 is a group which is detachable under alkaline reaction conditions,Z is the radical ##STR3## where each Q.sup.4 is independently of the other hydrogen or C.sub.1 -C.sub.4 -alkyl which may be substituted by cyano, U.sup.2 is C.sub.1 -C.sub.4 -alkyl, phenyl, C.sub.2 -C.sub.10 -alkenyl or the radical ##STR4## where Q.sup.5 and Q.sup.6 are each independently of the other hydrogen or C.sub.1 -C.sub.4 -alkyl and Q.sup.7 is a group which is detachable under alkaline reaction conditions, and w is 0, 1 or 2,t is 0, 1 or 2,v is 1 or 2 and X and L are each as defined in the description, with the proviso that at least one of the two radicals U.sup.1 and U.sup.2 is not C.sub.1 -C.sub.4 -alkyl or phenyl, and are prepared from benzyl compounds of the formula ##STR5## where A is nitro or amino and U.sup.1, Z and t are each as defined above. The reactive dyes are useful for dyeing hydroxyl-containing fibers such as cotton and wool and provide high yields and high wet fastness.
摘要翻译：双连接活性染料具有式“IMAGE”，其中U1是C1-C4-烷基，苯基，C2-C10-烯基或基团，其中Q1和Q2各自独立地是氢或C1-C4-烷基， Q3是在碱性反应条件下可分离的基团，Z是基团，其中每个Q 4独立于可被氰基取代的另一个氢或C 1 -C 4 - 烷基，U 2是C 1 -C 4 - 烷基，苯基，C 2 -C 10 - 烯基或基团，其中Q 5和Q 6各自独立地为氢或C 1 -C 4 - 烷基，Q 7为在碱性反应条件下可分离的基团，w为0,1或2 ，t为0,1或2，v为1或2，X和L各自如说明书中所定义，条件是两个基团U1和U2中的至少一个不是C 1 -C 4 - 烷基或苯基，并且由式为“IMAGE”的苄基化合物制备，其中A是硝基或氨基，并且U1，Z和t各自如上所定义。活性染料可用于染色含有羟基的纤维如棉和羊毛，并提供高产率和高耐湿牢度。

19. 发明授权

US5194607A Reactive dyes with a triphendioxazine chromophore 失效
标题翻译：与TRIPHENDIOXAZINE CHROMOPHORE的反应性染料
公开(公告)号：US5194607A
公开(公告)日：1993-03-16
申请号：US722108
申请日：1991-06-27
申请人： Manfred Patsch , Claus Marschner , Claus-Ulrich Priester
发明人： Manfred Patsch , Claus Marschner , Claus-Ulrich Priester
IPC分类号： C09B19/00 , C09B62/02 , C09B62/04 , C09B62/44 , C09B62/503
CPC分类号： C09B62/046 , C09B62/021 , C09B62/4405
摘要： Triphendioxazine dyes suitable for dyeing or printing hydroxyl- or amido-containing substrates have the formula ##STR1## where n is 0 or 1,m is 1 or 2,R.sup.1 and R.sup.2 are each independently of the other hydrogen, chlorine, bromine, hydroxysulfonyl, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, substituted or unsubstituted phenyl or substituted or unsubstituted phenoxy,R.sup.3 is halogen, carboxyl, C.sub.1 -C.sub.4 -alkyl, C.sub.1 -C.sub.4 -alkoxy, vinylsulfonyl or the radical --SO.sub.2 --CH.sub.2 CH.sub.2 --Z, where Z is a leaving group, andQ.sup.1 and Q.sup.2 are each independently of the other a radical of the formula ##STR2## where R.sup.4 and R.sup.5 are each independently of the other hydrogen, C.sub.1 -C.sub.4 -alkyl or phenyl,R.sup.6 is hydrogen or a fiber-reactive radical,L.sup.1 and L.sup.2 are each independently of the other substituted or unsubstituted C.sub.2 -C.sub.8 -alkylene or phenylene,X is a chemical bond, oxygen, sulfur, imino, C.sub.1 -C.sub.4 -alkylimino, carbonyl or methylene, andY is oxygen or sulfur,with the proviso that if n is 0, R.sup.6 is a fiber-reactive radical, and that the hydroxysulfonyl groups are each ortho to the substituents Q.sup.1 and Q.sup.2.
摘要翻译：适用于染色或印刷含羟基或酰胺基底物的三苯并二恶嗪染料具有式“IMAGE”，其中n为0或1，m为1或2，R 1和R 2各自独立地为氢，氯，溴，羟基磺酰基， C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，取代或未取代的苯基或取代或未取代的苯氧基，R 3是卤素，羧基，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，乙烯基磺酰基或-SO 2 -CH 2 CH 2 - 其中Z是离去基团，并且Q 1和Q 2各自独立地为下式的基团：其中R 4和R 5各自独立地为氢，C 1 -C 4 - 烷基或苯基，R 6是氢或纤维反应性基团L1和L2各自独立地为其它取代或未取代的C 2 -C 8亚烷基或亚苯基，X为化学键，氧，硫，亚氨基，C 1 -C 4烷基亚氨基，羰基或亚甲基，Y 是氧或硫，条件是如果n为0，则R6为纤维反应性基团，羟基磺酰基 s各自为取代基Q1和Q2的邻位。

20. 发明授权

US6011140A Reactive azo dyes with an aminonaphthalenesulfonic acid coupling component and intermediates therefor 失效
标题翻译：反应性偶氮染料与氨基萘磺酸偶合成分及其中间体
公开(公告)号：US6011140A
公开(公告)日：2000-01-04
申请号：US101183
申请日：1998-07-06
申请人： Andrea Zamponi , Manfred Patsch , Hermann Loffler
发明人： Andrea Zamponi , Manfred Patsch , Hermann Loffler
IPC分类号： C07C309/47 , C07C309/50 , C09B62/44 , C09B62/51 , C09B62/513 , C09B62/08 , C09B62/507 , D06P1/38
CPC分类号： C09B62/4415 , C07C309/47 , C07C309/50 , C09B62/513
摘要： Reactive dyes of the formula ##STR1## where n is 1 or 2,G.sup.1 is hydrogen or hydroxyl,G.sup.2 is hydrogen or hydroxysulfonyl,G.sup.3 is hydrogen or arylazo,R.sup.1 is hydrogen or hydroxysulfonylmethyl,R.sup.2 is hydrogen or hydroxysulfonylmethyl, andD is the radical of a diazo or tetraazo component having in each case at least one anchor radical of the formula SO.sub.2 --Y, where Y is vinyl or substituted ethyl,their use for dyeing or printing hydroxyl-containing or nitrogenous organic substrates, and naphthylamines as intermediates therefor.
摘要翻译： PCT No.PCT / EP97 / 00013 Sec。 371日期：1998年7月6日 102（e）日期1998年7月6日PCT 1997年1月3日PCT PCT。公开号WO97 / 25377 PCT 日期：1997年7月17日，其中n为1或2，G1为氢或羟基，G2为氢或羟基磺酰基，G3为氢或芳基偶氮，R1为氢或羟基磺酰基甲基，R2为氢或羟基磺酰基甲基，在每种情况下，重氮或四氮组分的基团具有至少一个式SO 2 -Y的锚定基团，其中Y是乙烯基或取代的乙基，它们用于染色或印刷含羟基或含氮有机底物和萘胺作为中间体的用途因此。

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