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91. 发明授权

US4623749A Synthesis of triconjugated dienones and novel intermediates used in said process 失效
标题翻译：三氯联二烯酮的合成和所述方法中使用的新型中间体
公开(公告)号：US4623749A
公开(公告)日：1986-11-18
申请号：US620163
申请日：1984-08-17
申请人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
发明人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
IPC分类号： C07C45/67 , C07C49/203 , C07C69/145 , C07C69/157 , C11B9/00 , C11D3/50
CPC分类号： C11D3/50 , C07C45/673 , C07C45/676 , C07C49/203 , C07C67/293 , C11B9/0015 , C11B9/0061
摘要： Described is a process for preparing triconjugated dienones defined according to the structure: ##STR1## wherein R.sub.1 represents C.sub.1 -C.sub.8 alkyl, phenyl or phenyl methyl and wherein R.sub.2 represents hydrogen or C.sub.1 -C.sub.5 lower alkyl; and wherein the wavy lines are indicative of a "cis" or a "trans" juxtaposition of the R.sub.2, methyl, acyl or vinyl moieties about one or both of the carbon-carbon double bonds which process involves the reaction of an acyl halide with a substituted or unsubstituted prenyl ester having the structure: ##STR2## wherein R.sub.3 represents C.sub.1 -C.sub.5 alkyl in the presence of an aluminum chloride catalyst and a methylene dichloride solvent in order to form a halogen-ester intermediate defined according to the structure: ##STR3## then dehydrohalogenating said halogen-ester intermediate using an alkali metal carbonate and a dimethylformamide solvent in order to form a ketoester having the structure: ##STR4## wherein one of the dashed lines represents a carbon-carbon double bond and the other of the dashed lines represents a carbon-carbon single bond; and then dehydroacyloxylating the ketoester in the presence of an alkali metal carbonate and dimethylformamide solvent in order to form the triconjugated dienone.
摘要翻译：描述了根据以下结构定义的三结合双酮的方法：其中R 1表示C 1 -C 8烷基，苯基或苯基甲基，并且其中R 2表示氢或C 1 -C 5低级烷基; 并且其中波浪线表示R2，甲基，酰基或乙烯基部分在一个或两个碳 - 碳双键上的“顺式”或“反式”并置，该方法涉及酰卤与具有以下结构的取代或未取代的异戊二烯基酯：其中R 3在氯化铝催化剂和二氯甲烷溶剂的存在下代表C 1 -C 5烷基，以形成根据以下结构定义的卤素 - 酯中间体：然后使用碱金属碳酸盐和二甲基甲酰胺溶剂将所述卤代酯中间体脱卤化氢，以形成具有以下结构的酮酯：其中虚线中的一条代表碳 - 碳双键，另一条虚线表示碳 - 碳单键; 然后在碱金属碳酸盐和二甲基甲酰胺溶剂的存在下，使酮酯脱羟基酰化，以形成三羟甲基封端的二烯酮。

92. 发明授权

US4575570A Process for producing alpha, beta-unsaturated ketones 失效
标题翻译：生产α，β-不饱和酮的方法
公开(公告)号：US4575570A
公开(公告)日：1986-03-11
申请号：US636379
申请日：1984-07-31
申请人： Hideaki Kataoka , Toshiro Yamada , Kuniaki Goto , Jiro Tsuji
发明人： Hideaki Kataoka , Toshiro Yamada , Kuniaki Goto , Jiro Tsuji
IPC分类号： C07C45/67 , C07C49/203 , C07C45/65
CPC分类号： C07C49/203 , C07C45/673 , C07C45/676
摘要： A process for producing alpha,beta-unsaturated ketones represented by the following general formula ##STR1## wherein R.sub.1 represents a hydrocarbon radical, R.sub.2 represents an organic radical bonded through a carbon-carbon bond, R.sub.3 and R.sub.4 represent a hydrogen atom or a hydrocarbon radical, and R.sub.1, R.sub.2, R.sub.3 and R.sub.4 may be straight-chained or form a ring in arbitrary combinations,which comprises contacting an alpha-disubstituted-beta-keto acid ester represented by the general formula ##STR2## wherein R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are as defined, and R.sub.5, R.sub.6, R.sub.7 and R.sub.8 represent a hydrogen atom or a hydrocarbon radical,with a catalyst consisting essentially of (a) a compound of a platinum-group metal and optionally (b) a monodentate ligand (b).
摘要翻译：一种制备由下列通式（II）表示的α，β-不饱和酮的方法，其中R1表示烃基，R2表示通过碳 - 碳键键合的有机基团，R3和R4表示氢原子或烃基，R 1，R 2，R 3和R 4可以是直链或以任意组合形成环，其包括使通式（I）表示的α-二取代β-酮酸酯与下式 R 1，R 2，R 3和R 4如上所定义，R 5，R 6，R 7和R 8表示氢原子或烃基，催化剂基本上由（a）铂族金属化合物和任选的（b）单齿配体（b）。

93. 发明授权

US4563365A Flavoring with 5-methyl-hept-2-en-4-one 失效
标题翻译：用5-甲基 - 庚-2-烯-4-酮调味
公开(公告)号：US4563365A
公开(公告)日：1986-01-07
申请号：US679180
申请日：1984-12-07
申请人： Roland Emberger , Manfred Kopsel , Jurgen Bruning , Rudolf Hopp , Theodor Sand
发明人： Roland Emberger , Manfred Kopsel , Jurgen Bruning , Rudolf Hopp , Theodor Sand
IPC分类号： A23L27/20 , A61K8/35 , A61L9/01 , A61Q13/00 , C07C45/29 , C07C49/203 , C11B9/00 , C11D3/50 , A23L1/226
CPC分类号： C11B9/0015 , C07C45/292 , C07C49/203
摘要： A perfumed or edible composition comprising an appropriate carrier and an amount of 5-methyl-hept-2-en-4-one effective to impart its fragrance or flavor to the composition. It imparts a fragrance and flavor reminiscent of hazelnut.
摘要翻译：一种加香或可食用的组合物，其包含合适的载体和一定量的5-甲基 - 庚-2-烯-4-酮，其有效地赋予组合物其香味或风味。它赋予榛子香味和香味。

94. 发明授权

US4546104A Pyrazolopyridine cycloalkanones and process for their preparation 失效
标题翻译：吡唑并吡啶环烷酮及其制备方法
公开(公告)号：US4546104A
公开(公告)日：1985-10-08
申请号：US659615
申请日：1984-10-11
申请人： James B. Campbell, Jr. , Thomas M. Bare
发明人： James B. Campbell, Jr. , Thomas M. Bare
IPC分类号： A61K31/435 , A61P25/00 , B01J23/00 , B01J31/00 , C07B61/00 , C07C45/51 , C07C45/67 , C07C45/68 , C07C45/71 , C07C45/72 , C07C45/74 , C07C49/203 , C07D231/38 , C07D471/04 , C07F7/08 , A61K31/47
CPC分类号： C07D231/38 , C07C403/02 , C07C45/513 , C07C45/673 , C07C45/676 , C07C45/68 , C07C45/71 , C07C45/72 , C07C45/74 , C07C49/203 , C07D471/04 , C07F7/0803 , C07F7/0812 , C07C2101/14 , C07C2101/16
摘要： Novel tetrahydropyrazolo-[3,4-b]quinolinones, cyclopenta[b]pyrazolo-[4,3-e]pyridinones and cyclohepta[b]-pyrazolo[4,3-e]pyridinones, useful as anxiolytics having reduced side effects, are disclosed, including methods of preparation, pharmaceutical compositions containing them and intermediates used in their preparation.
摘要翻译：新的四氢吡唑并[3,4-b]喹啉酮，环戊二烯并[b]吡唑并[4,3-e]吡啶酮和环庚三烯并[b] - 吡唑并[4,3-e]吡啶酮，包括制备方法，含有它们的药物组合物和其制备中使用的中间体。

95. 发明授权

US4535187A Preparation of isophorone and mesityl oxide from acetone 失效
标题翻译：从丙酮制备异佛尔酮和三甲氧基硅烷
公开(公告)号：US4535187A
公开(公告)日：1985-08-13
申请号：US564023
申请日：1983-12-21
申请人： Anthony J. Papa , Steven W. Kaiser
发明人： Anthony J. Papa , Steven W. Kaiser
IPC分类号： C07C49/203 , B01J21/04 , B01J23/02 , C07B61/00 , C07C45/00 , C07C45/74 , C07C49/603 , C07C67/00 , C07C45/45
CPC分类号： C07C45/74 , B01J23/02
摘要： The aldol condensation of acetone to isophorone and mesityl oxides in high conversions and efficiencies is achieved by a catalyst comprising a calcined calcium salt deposited on an alumina support.
摘要翻译：通过包含沉积在氧化铝载体上的煅烧钙盐的催化剂来实现丙酮与异佛尔酮和均三甲苯氧化物的高转化率和效率的醛醇缩合。

96. 发明授权

US4518790A 15-Deoxy-16-hydroxy-16-vinyl and cyclopropyl substituted prostanoic acids and congeners 失效
标题翻译： 15-脱氧-16-羟基-16-乙烯基和环丙基取代的前列腺酸和同系物
公开(公告)号：US4518790A
公开(公告)日：1985-05-21
申请号：US466751
申请日：1980-07-18
申请人： Middleton B. Floyd, Jr. , Martin J. Weiss , Charles V. Grudzinskas , Sow-Mei L. Chen
发明人： Middleton B. Floyd, Jr. , Martin J. Weiss , Charles V. Grudzinskas , Sow-Mei L. Chen
IPC分类号： C07C29/10 , C07C29/40 , C07C29/42 , C07C45/30 , C07C49/203 , C07C49/227 , C07C49/293 , C07C405/00 , C07F7/18 , C07F7/22 , C07C177/00
CPC分类号： C07F7/2212 , C07C29/10 , C07C29/40 , C07C29/42 , C07C405/00 , C07C45/305 , C07C49/203 , C07C49/227 , C07C49/293 , C07F7/1804 , C07F7/1896 , C07C2101/02
摘要： This disclosure describes novel 15-deoxy-16-hydroxy-16- substituted prostanoic acids and congeners thereof having utility as bronchodilators as hypotensive agents, and as agents for the control of excessive gastric secretion, and particularly, alkyl esters, such as the methyl ester, of such acids.
摘要翻译：本公开描述了新型的15-脱氧-16-羟基-16-取代的前列腺酸及其同系物，其具有作为降血压药物的支气管扩张剂的用途，以及用于控制过度胃分泌的药剂，特别是烷基酯，例如甲酯，这些酸。

97. 发明授权

US4513757A Branched chain saturated ketones, organoleptic uses thereof and process for preparing same 失效
标题翻译：支链饱和酮，其感官用途及其制备方法
公开(公告)号：US4513757A
公开(公告)日：1985-04-30
申请号：US589454
申请日：1984-03-14
申请人： Richard M. Boden
发明人： Richard M. Boden
IPC分类号： A23L27/20 , A24B15/32 , C07C45/45 , C07C49/203 , C11B9/00 , C11D1/24 , C11D3/395 , C11D3/50 , A24B3/12
CPC分类号： C11D3/50 , A23L27/202 , A24B15/32 , C07C45/455 , C07C49/203 , C11B9/0007 , C11B9/0015 , C11B9/0076 , C11D1/24 , C11D3/3956
摘要： Described is the novel compound genus defined according to the structure: ##STR1## wherein R.sub.1 is C.sub.1 -C.sub.3 lower alkyl useful in augmenting or enhancing the aroma or taste of consumable materials including perfumes, colognes, perfumed articles (including solid or liquid anionic, cationic, nonionic or zwitterionic detergents and perfumed polymers) smoking tobacco or smoking tobacco articles.
摘要翻译：描述了根据以下结构定义的新化合物：其中R 1是可用于增强或增强消耗材料的香味或味道的C 1 -C 3低级烷基，包括香料，古龙水，加香制品（包括固体或液体阴离子，阳离子，非离子或两性离子洗涤剂和加香聚合物）吸烟或吸烟制品。

98. 发明授权

US4504398A Process for augmenting or enhancing the aroma of perfumed articles by adding thereto triconjugated dienones 失效
标题翻译：通过向其中加入三环酮二烯酮来增强或增强香料制品香气的方法
公开(公告)号：US4504398A
公开(公告)日：1985-03-12
申请号：US551482
申请日：1983-11-14
申请人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
发明人： William J. Evers , Gilbert Stork , Braja D. Mookherjee , Howard H. Heinsohn, Jr.
IPC分类号： C07C45/67 , C07C49/203 , C11B9/00 , C11D3/50 , D06M13/20
CPC分类号： C11D3/50 , C07C45/673 , C07C45/676 , C07C49/203 , C07C67/293 , C07C67/297 , C11B9/0015 , C11B9/0061
摘要： Described is a process for augmenting or enhancing the aroma of a perfumed article which is a solid or liquid anionic, cationic, nonionic or zwitterionic detergent or a fabric softener composition or a dryer-added fabric softener article comprising the step of adding to said perfumed article at least one compound having a structure selected from the group consisting of: ##STR1##
摘要翻译：描述了一种用于增强或增强作为固体或液体阴离子，阳离子，非离子或两性离子洗涤剂或织物柔软剂组合物或干衣剂添加的织物柔软剂制品的香料的香气的方法，其包括将所述香料至少一种具有选自以下的结构的化合物：（i）和（iii）（ii）

99. 发明授权

US4451403A Substituted methyl isopropyl oxocyclohexane derivatives, organoleptic uses thereof and process for preparing same 失效
标题翻译：取代甲基异丙基氧代环己烷衍生物，其感官用途及其制备方法
公开(公告)号：US4451403A
公开(公告)日：1984-05-29
申请号：US343571
申请日：1982-04-26
申请人： Philip T. Klemarczyk
发明人： Philip T. Klemarczyk
IPC分类号： C07C35/18 , C07C45/62 , C07C45/72 , C07C49/203 , C07C49/647 , C11B9/00 , C07C50/02 , C07C69/025
CPC分类号： C11B9/0034 , C07C35/18 , C07C45/62 , C07C45/72 , C07C49/203 , C07C49/647
摘要： Described is the genus of compounds defined according to the structure: ##STR1## wherein at least one of the lines:[++++]represents a carbon-carbon single bond and the other of the lines:[++++]represents a carbon-carbon double bond or a carbon-carbon single bond; wherein the moiety X represents one of the moieties: ##STR2## wherein when the moiety X has the structure: ##STR3## then one of the lines:[++++]is a carbon-carbon double bond and the other of the lines:[++++]is a carbon-carbon single bond and when the moiety X has the structure: ##STR4## then both of the lines:[++++]represent carbon-carbon single bonds; wherein, one of R.sub.1, R.sub.2 and R.sub.3 represent 2-methyl-1-propenyl or 2-methyl-1-propylidenyl; and the other of R.sub.1, R.sub.2 and R.sub.3 represent hydrogen; with the provisos that:(i) when the line:[++++] at the 3-4 position is a double bond, then R.sub.3 is hydrogen or 2-methyl-1-propenyl; and(ii) when the line:[++++] at the 2-3 position is a double bond, then R.sub.2 is hydrogen or 2-methyl-1-propenyl.with the members of said genus being novel compounds useful in augmenting or enhancing the aroma or taste of consumable materials including perfume compositions, colognes and perfumed articles (e.g., solid or liquid anionic, cationic, nonionic or zwitterionic detergents, cosmetic powder compositions, fabric softener compositions and fabric softener articles).
摘要翻译：描述根据以下结构定义的化合物属：其中至少一行：[++++]表示碳 - 碳单键，另一行：[++++]表示碳 - 碳双键或碳 - 碳单键; 其中部分X表示以下部分之一：其中当部分X具有以下结构时：其中一行：[++++]是碳 - 碳双键，另一条线：[++++]是碳 - 碳单键，当X部分具有以下结构时：，则两行：[++++]表示碳 - 碳单键; 其中，R 1，R 2和R 3中的一个表示2-甲基-1-丙烯基或2-甲基-1-亚丙基; R1，R2和R3中的另一个表示氢; 条件是：（i）当3-4位上的线：[++++]是双键时，则R3是氢或2-甲基-1-丙烯基; 和（ii）当2-3位上的线：[++++]是双键时，则R2是氢或2-甲基-1-丙烯基。所述属的成员是用于增强或增强消耗材料（包括香料组合物，古龙水和香料制品）（例如固体或液体阴离子，阳离子，非离子或两性离子洗涤剂，化妆品粉末组合物，织物柔软剂）的香味或味道的新化合物组合物和织物柔软剂制品）。

100. 发明授权

US4433695A Process for the production of isosolanone and solanone, intermediates useful in said process and organoleptic uses of said intermediates 失效
标题翻译：用于生产异溶胶酮和溶胶酮的方法，可用于所述方法的中间体和所述中间体的感官用途
公开(公告)号：US4433695A
公开(公告)日：1984-02-28
申请号：US380542
申请日：1982-05-20
申请人： John B. Hall , James M. Sanders , James N. Siano
发明人： John B. Hall , James M. Sanders , James N. Siano
IPC分类号： A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/75 , C07C49/203 , C11D3/50 , A24B3/12
CPC分类号： C11D3/50 , A24B15/32 , C07C29/40 , C07C33/02 , C07C45/54 , C07C45/67 , C07C45/676 , C07C45/75 , C07C49/203 , C07C67/03
摘要： A process for augmenting or enhancing the aroma or taste of a smoking tobacco or smoking tobacco article comprising the step of adding to a smoking tobacco or smoking tobacco article component, an aroma or taste augmenting or enhancing quantity of a mixture of cis and trans isomers of a compound having the structure: ##STR1## wherein the wavy lines represent cis or trans juxtaposition of the hydrogen and 2-methyl-1-propenyl moieties around the carbon-carbon double bond.
摘要翻译：一种用于增强或增强吸烟烟草或吸烟烟草制品的香气或味道的方法，其包括向吸烟烟草或烟草制品组分添加香味或味道增加或增加量的顺式和反式异构体混合物的步骤具有以下结构的化合物：其中波浪线代表碳 - 碳双键周围的氢和2-甲基-1-丙烯基部分的顺式或反式并置。

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