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1. 发明专利

JP2018150255A 融解性多孔性高分子金属錯体、ガス吸着材、これを用いたガス分離装置およびガス貯蔵装置审中-公开
公开(公告)号：JP2018150255A
公开(公告)日：2018-09-27
申请号：JP2017046145
申请日：2017-03-10
申请人：新日鐵住金株式会社 , 国立大学法人京都大学
发明人：上代洋 , 永井徹 , 堀毛悟史 , 北川進 , 蔵所春菜
IPC分类号： B01J20/26 , C07F1/08 , B01D53/02 , C01C3/20 , C07D213/22
摘要：【課題】新規な多孔性高分子金属錯体及びこれを用いた優れた特性を有するガス吸着材を提供すること。ガス吸着材を内部に収容してなるガス分離装置およびガス貯蔵装置を提供すること。【解決手段】下記式(1) [MXY] n (1) (式中、Mは遷移金属イオン、Xは2個以上の配位点を有する配位子、Yは1価の対負電荷を有する対イオンである。nは、[MXY]から成る構成単位が多数集合しているという特性を示すもので、nの大きさは特に限定されない。) で表され、前記Yが、SCN - イオンである、融解性多孔性高分子金属錯体。【選択図】図2

2. 发明专利

JP2009227540A Method for producing ceramic precursor, ceramic precursor, method for producing ceramic, and ceramic 审中-公开
标题翻译：用于生产陶瓷前体的方法，陶瓷前体，用于生产陶瓷的方法和陶瓷
公开(公告)号：JP2009227540A
公开(公告)日：2009-10-08
申请号：JP2008077646
申请日：2008-03-25
申请人： Ngk Insulators Ltd , 日本碍子株式会社
发明人： YAMADA NAOHITO , FURUKAWA MASAHIRO , NANBA MASAHARU
IPC分类号： C04B35/48 , C01C3/11 , C01C3/14 , C01C3/20 , C01G25/00 , C04B35/626
摘要： PROBLEM TO BE SOLVED: To more satisfactorily disperse the additional component of a ceramic precursor into the main component. SOLUTION: The atom-configurated ceramic can be obtained by coordinating a ligand 21 having an easily coordinatable part 22 which can be coordinated into an a component as the main component and a b component as an additional component and a hardly coordinatable part 23 in which the coupling with the a component and the b component is suppressed into the a component and the b component, so as to produce an a complex ligand 24 and a b complex ligand 25, adding an ion or a complex comprising a c component which can be coupled with two or more hardly coordinatable parts 23 (a c component 26) to a solution comprising the a complex ligand 24 and the b complex ligand 25, so as to produce a precursor 28 and firing the produced precursor 28 under mild conditions. Upon the production of the precursor 28, in the b complex ligands 25, mutual coupling is suppressed by the hardly coordinatable parts 23, and the c component lies therebetween, thus the phenomenon that the b components as an additional component are made adjacent does not occur, and the adjoining presence of the b components can be sufficiently suppressed. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：为了使陶瓷前体的附加成分更均匀地分散到主要成分中。解决方案：原子构型陶瓷可以通过配位具有易配位的部分22的配位体21，其可以配位成作为主要成分的组分和作为附加组分的ab组分和难以配位的部分23 其与a组分和b组分的偶联被抑制到组分和b组分中，以便产生复合配体24和ab络合配体25，加入离子或包含交联组分的络合物，其可以偶联具有两个或多个难以配位的部分23（交流部件26）至包含络合配体24和b络合配体25的溶液，以便产生前体28并在温和条件下烧制所制备的前体28。在制备前体28时，在b络合配体25中，互不耦合部分被几乎不配合的部分23抑制，并且c部件位于它们之间，因此不会发生作为附加部件的b成分相邻的现象并且能够充分地抑制b成分的相邻存在。版权所有（C）2010，JPO＆INPIT

3. 发明专利

JPH09208220A METHOD FOR PREVENTING SOLIDIFICATION OF AMMONIUM THIOCYANATE DURING STORAGE 失效
公开(公告)号：JPH09208220A
公开(公告)日：1997-08-12
申请号：JP4052296
申请日：1996-02-02
申请人： SUMIKIN CHEMICAL
发明人： HOSHINO TAKASHI , YAMANE TOSHIO , YAGI SATOSHI
IPC分类号： B32B27/10 , C01C3/20
摘要： PROBLEM TO BE SOLVED: To prevent solidification of ammonium thiocyanate during storage by drying a ammonium thiocyanate crystal to decrease the water content and then housing the crystal in a bag comprising a bag having specified permeability of water vapor and a craft paper bag. SOLUTION: An ammonium thiocyanate crystal prepared by crystallization is dried to decrease the water content to .24Hr permeability of water vapor and a craft paper bag. The bag having specified permeability of water vapor consists of a composite film bag or a laminated bag of an Al foil and a moisture-preventing film. Thereby, absorption of water from air during storage is almost prevented. Since the permeating rate of the air in the bag to the outside due to the load given downward on the bag is small, the load on the ammonium thiocyanate crystal is decreased and solidification of the ammonium thiocyanate crystal can be prevented.

4. 发明专利

JPH0379346B2 失效
公开(公告)号：JPH0379346B2
公开(公告)日：1991-12-18
申请号：JP1471983
申请日：1983-02-02
申请人： DEGUSSA
发明人： AKUSERU KUREEMAN , HERUBERUTO KURENKU , UORUFUGANGU SHURUTSU
IPC分类号： C07C337/06 , C01B21/093 , C01C3/20 , C07C67/00 , C07C325/00

5. 发明专利

JPH03257014A PRODUCTION OF HIGH PURITY RHODAN SALT 失效
公开(公告)号：JPH03257014A
公开(公告)日：1991-11-15
申请号：JP5238490
申请日：1990-03-02
申请人： KANSAI COKE & CHEMICALS
发明人： FUJITA HIDEO
IPC分类号： C01C3/20
摘要： PURPOSE:To obtain high purity rhodan salt advantageously and industrially by allowing such an amine which itself is hardly soluble with water and an form water-insoluble addition product with rhodanic acid to contact with an aq. soln. containing sodium rhodanide to obtain an addition product, and bringing this product into contact with an aq. soln. of alkali material to decompose the addition product. CONSTITUTION:For example, an aq. soln. of sodium rhodanide having desired concn. obtained from waste liquid of desulferized gas from coke oven is treated with acid to change into an isolated acid type (namely, rhodanic acid) and controlled to show pH1-7. To this liquid treated with acid, the amine above described such as dicyclohexylamine or its N-alkylate is added, and preferably little by little, under stirred. Precipitate of the addition product which is hardly soluble with water is then separated by filtering, etc. The addition product thus separated is brought into contact with an aq. soln. of alkali material such as NaOH to decompose the addition product almost quantitatively. The water phase separated contains rhodanide salt in a dissolved state, which is recovered in the form of crystals as a industrial product.

6. 发明专利

JPH03257013A PRODUCTION OF RHODAN SALT AND THIOUREA FROM RHODAN AMMONIUM 失效
公开(公告)号：JPH03257013A
公开(公告)日：1991-11-15
申请号：JP5238390
申请日：1990-03-02
申请人： KANSAI COKE & CHEMICALS
发明人： FUJITA HIDEO
IPC分类号： C01C3/20 , C07C335/02
摘要： PURPOSE:To produce both of thiourea which has high additional value and high purity rhodan salt by adding amine to an aq. soln. of thiourea and unreacted NH4SCN prepared by dissolving transition reaction product of NH4 SCN in water and bringing the nonreacted NH4SCN into contact with an aq. soln. of alkali material. CONSTITUTION:Process (A); NH4SCN obtained from an aq. soln. containing NH4SCN such as waste water of desulfurized gas from coke oven is heated and dissolved to have a part of NH4SCN to transit to thiourea. Process (B); the above product is dissolved in water and brought into contact with amine, particularly comprising dicyclohexylamine to precipitate the addition product of NH4SCN and amine from which NH3 is removed. Process (C); The addition product is separated. Process (D); the addition product is brought into contact with an aq. soln. of alkali material such as NH3 to dissociate the addition product into rhodan salt and the original amine. Process (E); Thiourea is isolated from the filtrate containing thiourea in the process (C). Thus, rhodan salt and thiourea are both obtained from NH4SCN.

7. 发明专利

JPH02137717A PRODUCTION OF AMMONIUM THIOCYANATE 失效
公开(公告)号：JPH02137717A
公开(公告)日：1990-05-28
申请号：JP28854188
申请日：1988-11-15
申请人： SUMIKIN CHEMICAL
发明人： YAMANE TOSHIO , KAWAMURA SHIGEO
IPC分类号： C01C3/20
摘要： PURPOSE:To obtain high-purity ammonium thiocyanate in high yield at a low cost by washing coke oven gas with a circulated aqueous solution of ammonium polysulfide containing suspended fine particulate sulfur, collecting HCN as ammonium thiocyanate, crystallizing and separating the resultant ammonium thiocyanate according to a specific method. CONSTITUTION:Coke oven gas is washed with a circulated aqueous solution of ammonium polysulfide containing suspended fine particulate sulfur to collect hydrogen cyanide contained in the coke oven gas as ammonium thiocyanate. The circulated aqueous solution is then partially taken out, thermally concentrated to the saturation solubility of the ammonium thiocyanate to filter and separate ammonium thiosulfate depositing in a hot state. Cooling is then carried out to deposit, filter and collect the ammonium thiocyanate. The resultant ammonium thiocyanate is useful as a raw material for dyeing assistants, agricultural chemicals, etc.

8. 发明专利

JPH0193415A PRODUCTION OF CALCIUM THIOCYANATE 失效
公开(公告)号：JPH0193415A
公开(公告)日：1989-04-12
申请号：JP24851587
申请日：1987-10-01
申请人： SUMIKIN CHEMICAL
发明人： SATO TOSHIO , TANAKA YASUSHI , TAKEDA KYOICHI
IPC分类号： C01C3/20
摘要： PURPOSE:To enable mass production of calcium thiocyanate at a low cost, by subjecting a rhodax solution formed in a decyanogenation step of coke oven gas to decarbonation treatment and then metathetic reaction with calcium hydroxide, etc. CONSTITUTION:A solution (rhodax solution), containing ammonium thiocyanate and obtained in a decyanogenation step for washing coke oven gas with a sulfur suspension or polysulfide-containing solution is heated until water, e.g. in a given amount, is distilled and then subjected to decarbonation treatment. Ca(OH)2 or CaO both are subsequently added to the solution obtained after the treatment to carry out metathetic reaction with the ammonium thiocyanate. Thereby calcium thiocyanate expectable in demand as a cement hardening promoter can be supplied in a large amount at a low cost by this method.

9. 发明专利

JPS63117909A PRODUCTION OF CALCIUM THIOCYANATE 失效
公开(公告)号：JPS63117909A
公开(公告)日：1988-05-21
申请号：JP26400886
申请日：1986-11-07
申请人： NIPPON KOKAN KK , NISSAN CHEMICAL IND LTD
发明人： NATORI YOSHIAKI , OTA YASUMASA , KAWAHARA MITSUNORI , WATANABE YOSHIAKI , KOBAYASHI SHIGEKATSU , NAKAJIMA HIDEO
IPC分类号： C01C3/20 , C10K1/12
摘要： PURPOSE:To easily and inexpensively obtain the title calcium thiocyanate by adding excess calcium hydroxide to the waste liq. from ammonia-process wet desulfurization for coke-oven gas, etc., and carrying out deammoniation reaction under specified conditions. CONSTITUTION:A waste liq. contg. ammonium thiocyanate and ammonium thiosulfate and generated in the ammonia-process wet desulfurization for coke- oven gas, etc., is used as the starting material. Calcium hydroxide or calcium oxide in the amt. sufficient to substitute all the ammonium salts in the waste liq. for the calcium salts is added to the waste liq., and then deammoniation reaction is carried out under the conditions where the formed calcium thiosulfate is decomposed. The calcium sulfite, sulfur, and calcium sulfate formed in the deammoniated liq. and substantially insoluble in the liq. are separated and removed as cake. The liq. freed of the cake is concentrated and then cooled to obtain calcium thiocyanate.

10. 发明专利

JPS6323128B2 失效
公开(公告)号：JPS6323128B2
公开(公告)日：1988-05-14
申请号：JP9810480
申请日：1980-07-16
申请人： SUMIKIN KAKO KK
发明人： SATO TOSHIO , TAKEDA KYOICHI
IPC分类号： C01C3/20 , C01C1/24

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