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1. 发明专利

JP2006255926A Laminated film 审中-公开
标题翻译：层压膜
公开(公告)号：JP2006255926A
公开(公告)日：2006-09-28
申请号：JP2005072740
申请日：2005-03-15
申请人： Teijin Ltd , 帝人株式会社
发明人： ISHIWATARI TOYOAKI , MATSUO TOMINE , KIDO NOBUAKI
IPC分类号： B32B27/34
摘要： PROBLEM TO BE SOLVED: To provide a laminated film suitably used as an insulating layer in an electronic mounting use or an adhesive film for fixing a semiconductor wafer or a die attach film for use in a semiconductor device, and a laminate using it. SOLUTION: The laminated film is composed of a base material (A) comprising a full aromatic polyimide film and the resin layer (B) formed on one side or both sides of the base material and characterized in that the coefficient of in-plane linear expansion at a temperature of 100-200°C thereof is -3 to 6 ppm/°C and the elastic modulus thereof is 2-13 GPa. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：为了提供适合用作电子安装用途中的绝缘层的层叠膜或用于固定用于半导体器件的半导体晶片或芯片附着膜的粘合剂膜以及使用它的层压体。解决方案：层压膜由包含全芳族聚酰亚胺膜的基材（A）和形成在基材的一侧或两侧上的树脂层（B）组成，其特征在于，在100-200℃的温度下的平面线性膨胀为-3〜6ppm /℃，弹性模量为2〜13GPa。版权所有（C）2006，JPO＆NCIPI

2. 发明专利

JP2004174796A Method for manufacturing biaxially oriented polyimide film 有权
标题翻译：制造双面聚酰亚胺薄膜的方法
公开(公告)号：JP2004174796A
公开(公告)日：2004-06-24
申请号：JP2002341932
申请日：2002-11-26
申请人： Teijin Ltd , 帝人株式会社
发明人： ISHIWATARI TOYOAKI , NAKAMURA TSUTOMU , KOJIMA KAZUNORI , SAWAKI TORU
IPC分类号： C08J5/18 , B29C41/24 , B29C55/12 , B29K79/00 , B29L7/00 , C08G73/10
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a biaxially oriented polyimide film which shows superb stretching stability in a gel stretching process.
SOLUTION: The method for manufacturing the biaxially oriented polyimide film comprises the following steps (1) to (4). (1) A polyamic acid solution is prepared by making an aromatic diamine component and an aromatic tetracarboxylic acid component react with each other in an organic polar solvent. (2) The obtained polyamic acid solution is cast over a support and soaked in an isoimidized solution obtained by dissolving a dehydrating agent in an organic solvent together with the support and thereby, a gel film composed of the polyamic acid, at least a part of which is converted to a polyisoimide, is formed. (3) The obtained gel film is separated from the support and biaxially oriented after cleaning, if necessary. (4) The obtained biaxially oriented gel film is thermally treated to obtain the biaxially oriented polyimide film after cleaning, if necessary. The dehydrating agent used in the step (2) is a diisopropylcarbodiimide.
COPYRIGHT: (C)2004,JPO
摘要翻译：要解决的问题：提供一种在凝胶拉伸工艺中显示出极好的拉伸稳定性的双轴取向聚酰亚胺膜的制造方法。解决方案：制造双轴取向聚酰亚胺膜的方法包括以下步骤（1）至（4）。（1）通过使芳族二胺成分和芳香族四羧酸成分在有机极性溶剂中反应而制备聚酰胺酸溶液。（2）将得到的聚酰胺酸溶液浇铸在支持体上，并浸渍在通过将脱水剂与载体一起溶解在有机溶剂中而获得的异酰化溶液中，由此形成由聚酰胺酸组成的凝胶膜，至少一部分其被转化为聚异酰亚胺。（3）如果需要，将得到的凝胶膜从载体上分离并进行双轴取向。（4）如果需要，将得到的双轴取向凝胶膜进行热处理，得到清洗后的双轴取向聚酰亚胺膜。步骤（2）中使用的脱水剂是二异丙基碳二亚胺。版权所有（C）2004，JPO

3. 发明专利

JP2003064172A Method for producing wholly aromatic polyester 审中-公开
标题翻译：生产纯粹芳香聚酯的方法
公开(公告)号：JP2003064172A
公开(公告)日：2003-03-05
申请号：JP2001256738
申请日：2001-08-27
申请人： Teijin Ltd , 帝人株式会社
发明人： SAKURAI HIROSHI , ISHIWATARI TOYOAKI , JOKAI MASAYUKI , MATSUMURA SHUNICHI
IPC分类号： C08G63/80 , C08G63/64
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a wholly aromatic polyester, which enables the improvement in troubles and handling difficulty due to powder and the shortage of a solid phase polymerization time.
SOLUTION: This method for producing the wholly aromatic polyester comprises sequentially subjecting three components comprising an aromatic diol component, an aromatic dicarboxylic acid component, and a diaryl carbonate to a preliminary polymerization process, a crystallization process, a crushing process, a coagulation process, and a solid phase polymerization process.
COPYRIGHT: (C)2003,JPO
摘要翻译：要解决的问题：提供一种全芳香族聚酯的制造方法，其能够改善由于粉末引起的故障和处理困难以及固相聚合时间的不足。解决方案：用于制备全芳族聚酯的方法包括将包含芳族二醇组分，芳族二羧酸组分和碳酸二芳基酯的三种组分顺序进行预聚合过程，结晶过程，破碎过程，凝结过程和固相聚合法。

4. 发明专利

JP2002080579A METHOD FOR CRYSTALLIZING LOW-MOLECULAR WEIGHT POLYCARBONATE AND METHOD FOR POLYMERIZING THE SAME 失效
公开(公告)号：JP2002080579A
公开(公告)日：2002-03-19
申请号：JP2000271395
申请日：2000-09-07
申请人： TEIJIN LTD
发明人： SUZUKI HIROTAKA , MATSUMURA SHUNICHI , KONO KAZUTERU , ISHIWATARI TOYOAKI
IPC分类号： C08G64/40 , C08G64/20
摘要： PROBLEM TO BE SOLVED: To provide a method for crystallizing a low-molecular weight polycarbonate efficiently and a method for manufacturing a polycarbonate resin having a desired intrinsic viscosity by using a polycarbonate crystallized through the above method. SOLUTION: A low-molecular weight polycarbonate (preferably, a low- molecular weight polycarbonate produced by melt polycondensation) is brought into contact with an aromatic monohydroxy compound or a mixture of the compound with water to crystallize it. The resultant crystallized carbonate is heated at a temperature lower than its melting point under a reduced pressure or in an inert gas stream to increase the degree of polymerization of the polycarbonate, and thus a polycarbonate resin having a desired intrinsic viscosity is manufactured.

5. 发明专利

JP2002003583A TOTALLY AROMATIC POLYESTER AND METHOD OF PRODUCING THE SAME 失效
公开(公告)号：JP2002003583A
公开(公告)日：2002-01-09
申请号：JP2000184331
申请日：2000-06-20
申请人： TEIJIN LTD
发明人： SAKURAI HIROSHI , MIYOSHI TAKANORI , ISHIWATARI TOYOAKI , MATSUMURA SHUNICHI
IPC分类号： C08G63/193 , C08G63/86 , C08G63/87
摘要： PROBLEM TO BE SOLVED: To provide a totally aromatic polyester having excellent tone of color, and to provide a method of producing it. SOLUTION: This totally aromatic polyester is obtained by melt-polymerizing an aromatic dicarboxylic acid, an aromatic diol and diaryl carbonate, all of which having specific structural formulae, in the existence of a specific pyridine compound and a specific germanium compound, under such conditions of the melt-polymerization that the finally arrived temperature is in the range of 270 deg.C to 370 deg.C, the pressure is maintained in the range of 1 Pa to 200 Pa, and the holding time at the finally arrived temperature is within 3 hours. The totally aromatic polyester has a specific structural unit, containing at least one free radical component having g-value of 2.0032 to 2.0037 in the polymer before heat treatment, and total amount of free radicals in 1 g of polymer is 1.0×1017 spins or less. The polymer after heat treatment contains free radicals having g-value of 2.0032 or less in an amount of 5.0×1016 spins or less, and the light absorbance at 400 nm of the solution dissolved 0.1 g of the polymer after heat treatment in 5 mL of dichloromethane is 0.1 or lower.

6. 发明专利

JPH1180339A PRODUCTION OF POLYESTER ELASTOMER 失效
公开(公告)号：JPH1180339A
公开(公告)日：1999-03-26
申请号：JP24533497
申请日：1997-09-10
申请人： TEIJIN LTD
发明人： ISHIWATARI TOYOAKI , SADANOBU JIROU
IPC分类号： C08G63/66 , C08G63/78
摘要： PROBLEM TO BE SOLVED: To provide a method for producing the subject elastomer, by which the elastomer having a high molecular weight is produced in a short time in good reproducibility by adding a specific compound to a specific polyester elastomer, and reacting the obtained mixture under melting. SOLUTION: (B) A bis(epsilon-caprolactam)-based compound of the formula in an amount of 0.01-10% is added to (A) a polyester elastomer consisting essentially of an elastomer consisting of (i) a hard segment comprising an aromatic polyester component and (ii) a soft segment comprising a poly(oxyalkyleneoxide) glycol component having 500-5, 000 number average molecular weight, regulated so that the content of the component (ii) may be 30-95 wt.% and having 0.3-10 intrinsic viscosity (IV), and the obtained mixture is reacted preferably at 180-300 deg.C preferably under a reduced pressure in a molten state preferably for 30 sec to one hour to provide the objective polyester elastomer in the method for producing the polyester elastomer.

7. 发明专利

JPH10237001A MANUFACTURE OF DIARYLOXY ALKANE 失效
公开(公告)号：JPH10237001A
公开(公告)日：1998-09-08
申请号：JP4201797
申请日：1997-02-26
申请人： TEIJIN LTD
发明人： YOSHISATO AKINOBU , ISHIWATARI TOYOAKI , MURAMOTO MASAHARU , SADANOBU JIROU
IPC分类号： C07C41/01 , C07C43/205
摘要： PROBLEM TO BE SOLVED: To obtain a diaryloxy alkane in high yield by carrying out a reaction of an alkane dihalide with phenol derivatives in the presence of an aprotic organic solvent at high temperature. SOLUTION: The subject compound of formula II is obtained by carrying out the reaction of the alkane dihalide (for example, methylene chloride) of formula X-A-Y (X, Y are each a halogen; A is a lower alkylene) and the phenols (for example, 2-bromophenol) expressed in formula I (R1 -R5 are each H, a halogen, a lower alkyl, etc.), while keeping the amount of alkali (for example, sodium hydroxide) used at the starting step at 0.5-1.0 mole per one mole of the phenol of the formula I, and adding the remaining alkali so that the total amount of the alkali is more than one mole per one mole of the starting phenol of the formula I.

8. 发明专利

JP2004224994A Biaxially-oriented polyimide film and its production method 审中-公开
公开(公告)号：JP2004224994A
公开(公告)日：2004-08-12
申请号：JP2003017052
申请日：2003-01-27
申请人： Teijin Ltd , 帝人株式会社
发明人： ISHIWATARI TOYOAKI , NAKAMURA TSUTOMU , TANGE SHINYA , SAWAKI TORU
IPC分类号： B29C55/12 , B29K79/00 , B29L7/00 , C08G73/10 , C08J5/18
摘要： PROBLEM TO BE SOLVED: To provide a polyimide film having excellent mechanical properties particularly in flexibility, improving Young's modulus, which are obtained by controlling a crystalline microstructure, wherein no conventional technology can be utilized; and to provide its production method.
SOLUTION: The polyimide film is formed through the following processes. After preparing a polyamic acid solution comprising a polyamic acid composed substantially of an aromatic diamine component having ≥40 mol% and ≤100 mol% p-phenylenediamine component and a tetracarboxylic acid component having >80 mol% pyromellitic acid component, and at least one solvent selected from the group consisting of N, N-dimethylformamide, N, N-dimethylacetamide, N-methyl-2-pyrrolidone and 1, 3-dimethylimidazolidinone, the prepared polyamic acid solution and a dehydrating agent are reacted, forming a gel film, wherein at least a part of the polyamic acid is converted to a polyisoimide. The content of N, N-dimethylformamide, N, N-dimethylacetoamide, N-methyl-2-pyrrolidone and 1, 3-dimethylimidazolidinone in the film is ≤500 ppm.
COPYRIGHT: (C)2004,JPO&NCIPI

9. 发明专利

JP2004131598A Wholly aromatic polyester carbonate and method for producing the same 审中-公开
公开(公告)号：JP2004131598A
公开(公告)日：2004-04-30
申请号：JP2002297482
申请日：2002-10-10
申请人： Teijin Ltd , 帝人株式会社
发明人： JOKAI MASAYUKI , SAKURAI HIROSHI , MATSUMURA SHUNICHI , ISHIWATARI TOYOAKI , ITO TAKASHI
IPC分类号： C08G63/64
摘要： PROBLEM TO BE SOLVED: To provide a stabilized wholly aromatic polyester carbonate with high hydrolysis resistance, good in color tone and slight in hue change after subjected to dry heat treatment, wherein at least part of terminal aromatic hydroxy groups and terminal carboxy groups are blocked.
SOLUTION: The terminal-blocked wholly aromatic polyester carbonate is obtained by the following process: copolymerization is carried out between a specified aromatic dicarboxylic acid, a specified aromatic diol and a diaryl carbonate in specified proportions, and when the reduced viscosity of the resulting wholly aromatic polyester carbonate reached at least 0.1 dL/g, a compound of the formula(1)( wherein, R
7 is a halogen atom selected from Cl, Br and I, methoxycarbonyl or ethoxycarbonyl; and R
8 is a 1-30C alkyl, 1-30C alkoxy, 6-30C aryl or 6-30C aryloxy ) is added to the system.
COPYRIGHT: (C)2004,JPO

10. 发明专利

JP2003301036A Granular wholly aromatic polyester molding and process for producing wholly aromatic polyester by using it 审中-公开
标题翻译：颗粒状芳香族聚酯模塑制品及使用其制造纯粹芳香族聚酯的方法
公开(公告)号：JP2003301036A
公开(公告)日：2003-10-21
申请号：JP2002108011
申请日：2002-04-10
申请人： Teijin Ltd , 帝人株式会社
发明人： ITO TAKASHI , SAKURAI HIROSHI , JOKAI MASAYUKI , MATSUMURA SHUNICHI , ISHIWATARI TOYOAKI
IPC分类号： C08G63/64 , C08G63/82
摘要： PROBLEM TO BE SOLVED: To provide a process for producing an aromatic polyester having a high degree of polymerization, wherein process handling is reduced, the solid- phase polymerization time is shortened, and a reduction in yield due to fine powders is prevented.
SOLUTION: This granular wholly aromatic polyester molding comprises mainly a wholly aromatic polyester substantially consisting of repeating units of formula (1) and having a reduced viscosity of 0.05-0.3 dl/g and a heat of crystal fusion, measured by DSC at a temperature rise rate of 10°C/min, of 0.5-60 J/g. It has a specific surface area of 0.001-1 m
2 /g and a bulk density of 0.4-1.3 g/cc.
COPYRIGHT: (C)2004,JPO
摘要翻译：要解决的问题：为了提供具有高聚合度的芳族聚酯的制备方法，其中工艺处理降低，固相聚合时间缩短，并且防止由于细粉末导致的产率降低。解决方案：这种颗粒状全芳族聚酯成型体主要包含基本上由式（1）的重复单元组成的具有0.05-0.3dl / g的比浓粘度和结晶熔化热的全芳族聚酯，其通过DSC测量升温速度为10℃/分钟，为0.5-60J / g。其比表面积为0.001-1m 2 / SP / g，堆积密度为0.4-1.3g / cc。版权所有（C）2004，JPO

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