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1. 发明专利

JP2014046229A Hydrogen separator 有权
标题翻译：氢分离器
公开(公告)号：JP2014046229A
公开(公告)日：2014-03-17
申请号：JP2012189153
申请日：2012-08-29
申请人： Ngk Spark Plug Co Ltd , 日本特殊陶業株式会社 , Tokyo Gas Co Ltd , 東京瓦斯株式会社
发明人： KAJITANI MASAHIRO , TANAKA HIROYUKI , KAWASE HIROKI , TAKAGI YASUHIRO , ITO MASAYA , IZEKI KOYA , KUME TAKAO , IKEDA YOICHI
IPC分类号： B01D71/02 , B01D69/04 , B01D69/10 , B01D69/12 , C01B3/56 , H01M8/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen separator which can reduce a gas leak in the hydrogen separator.SOLUTION: In a hydrogen separator (1), a dense layer (17) is formed on a ceramic support body (9) so as to cover an exposed portion (15) of an interface (13) and so as to extend over a porous support part (5) and a dense support part (7), and a hydrogen separation metal layer (21) is formed so as to come in contact with the dense layer (17) and so as to cover a surface of the porous support part (5). Specifically, the dense layer (17) is projected toward the porous support part (5) side from the dense support part (7) along the surface of the porous support part (5).
摘要翻译：要解决的问题：提供可以减少氢气分离器中的气体泄漏的氢分离器。解决方案：在氢分离器（1）中，在陶瓷支撑体（9）上形成致密层（17），以便覆盖接口（13）的暴露部分（15）并且延伸到多孔支撑部分（5）和致密支撑部分（7）上，并且形成氢分离金属层（21）以便到达与致密层（17）接触并且覆盖多孔支撑部分（5）的表面。具体地，致密层（17）沿着多孔支撑部（5）的表面从致密支撑部（7）向多孔支撑部（5）侧突出。

2. 发明专利

JP2011195349A Apparatus for producing hydrogen 审中-公开
标题翻译：生产氢气的装置
公开(公告)号：JP2011195349A
公开(公告)日：2011-10-06
申请号：JP2010061419
申请日：2010-03-17
申请人： Ngk Spark Plug Co Ltd , Tokyo Gas Co Ltd , 日本特殊陶業株式会社 , 東京瓦斯株式会社
发明人： NISHII TAKUMI , NAKAGAWA TOMOKI , TOMINAGA RYUICHI , IZEKI KOYA , SHIRASAKI YOSHINORI , YASUDA ISAMU , ITO MASAYA , TAKAGI YASUHIRO , SHIGAKI HIDEKAZU , HIKOSAKA HIDEAKI , TANAKA HIROYUKI
IPC分类号： C01B3/40 , B01D53/22 , B01D69/10 , B01D71/02 , C01B3/56
摘要： PROBLEM TO BE SOLVED: To obtain an apparatus for producing hydrogen that uses a precise hollow support as a support for a reforming catalyst serving also as a support and uses the reforming catalyst serving also as a support as a support for a hydrogen separation membrane, wherein all gases of a feed gas, hydrogen and an offgas are made to flow through the reforming catalyst serving also as a support.SOLUTION: The apparatus for producing hydrogen is composed of the precise hollow support having a hollow part through which the feed gas flows, the porous reforming catalyst serving also as a support adhered to the outer peripheral surface of the precise hollow support, and the hydrogen separation membrane on the outer peripheral surface of the reforming catalyst serving also as a support. The feed gas flows through the hollow part inside the precise hollow support, turning at the end thereof in the direction of flow, and forms a reformed gas from the feed gas while flowing in the reforming catalyst serving also as a support. The formed reformed gas is purified through the hydrogen separation membrane to produce high-purity hydrogen.
摘要翻译：要解决的问题：为了获得使用精确的中空支撑体的氢气的装置作为还用作载体的重整催化剂的载体，并且使用还用作载体的重整催化剂作为氢分离膜的载体，其中使进料气体，氢气和废气的所有气体流过也用作载体的重整催化剂。解决方案：用于生产氢气的装置由具有中空部分的精确中空支撑件构成，进料气体通过该中空部分流动，也用作附着在精密中空支撑体的外周面的支撑体的多孔重整催化剂和也用作载体的重整催化剂的外周面上的氢分离膜。进料气体流过精确的中空支撑体内的中空部分，在其端部沿流动方向转动，并且在还用作支撑体的重整催化剂中流动时，从进料气体形成重整气体。通过氢分离膜纯化形成的重整气体以产生高纯度氢。

3. 发明专利

JP2011195350A Apparatus for producing hydrogen 有权
标题翻译：生产氢气的装置
公开(公告)号：JP2011195350A
公开(公告)日：2011-10-06
申请号：JP2010061561
申请日：2010-03-17
申请人： Ngk Spark Plug Co Ltd , Tokyo Gas Co Ltd , 日本特殊陶業株式会社 , 東京瓦斯株式会社
发明人： NISHII TAKUMI , NAKAGAWA TOMOKI , TOMINAGA RYUICHI , IZEKI KOYA , SHIRASAKI YOSHINORI , YASUDA ISAMU , ITO MASAYA , TAKAGI YASUHIRO , SHIGAKI HIDEKAZU , HIKOSAKA HIDEAKI , TANAKA HIROYUKI
IPC分类号： C01B3/38 , B01D53/22 , C01B3/56 , H01M8/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To obtain an apparatus for producing hydrogen capable of attaining a high recovery rate of hydrogen by removing an offgas remaining between an inserted tube and a reforming catalyst serving also as a support in the apparatus for producing hydrogen equipped with a cylindrical reactor of external membrane type.SOLUTION: The apparatus for producing hydrogen is composed of the inserted tube having a hollow part through which a feed gas flows, the reforming catalyst serving also as a support installed apart from the outer peripheral surface of the inserted tube, and the hydrogen separation membrane on the outer peripheral surface of the reforming catalyst serving also as a support. The feed gas flows through the hollow part inside the inserted tube, turning at the end thereof in the direction of flow, and forms a reformed gas from the feed gas while flowing between the inserted tube and the reforming catalyst serving also as a support. The formed reformed gas is purified through the hydrogen separation membrane to produce high-purity hydrogen. The feed gas is forced to flow into the reforming catalyst serving also as a support by blocking the passage at the discharge side of the feed gas.
摘要翻译：要解决的问题：为了获得能够获得高氢回收率的氢气的设备，除去在装有圆柱形反应器的氢的制造装置中也用作支撑体的插入管和重整催化剂之间残留的废气的外部膜类型。解决方案：用于生产氢的装置由具有中空部分的插入管组成，进料气通过该中空部分，重整催化剂也用作与插入管的外周表面分离的支撑体，以及重整催化剂的外周面上的氢分离膜也用作载体。进料气体流过插入管内部的中空部分，在其端部沿着流动方向转动，并且在插入管和也用作载体的重整催化剂之间流动时，从进料气体形成重整气体。通过氢分离膜纯化形成的重整气体以产生高纯度氢。通过阻塞进料气体的排出侧的通道，进料气体被迫流入也用作载体的重整催化剂。

4. 发明专利

JP2014184381A Hydrogen separation body 审中-公开
标题翻译：氢分离体
公开(公告)号：JP2014184381A
公开(公告)日：2014-10-02
申请号：JP2013060327
申请日：2013-03-22
申请人： Ngk Spark Plug Co Ltd , 日本特殊陶業株式会社 , Tokyo Gas Co Ltd , 東京瓦斯株式会社
发明人： KAJITANI MASAHIRO , TAKAGI YASUHIRO , IZEKI KOYA , KUME TAKAO , IKEDA YOICHI
IPC分类号： B01D71/02 , B01D69/10 , B01D69/12 , H01M8/04
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen separation body in which a gas leakage can be reduced.SOLUTION: A hydrogen separation body (1) comprises: a ceramic porous support (5) through which a gas can pass; a ceramic dense layer (11) having an airtightness which is formed on a part of a surface of the porous support (5); a ceramic porous layer (13) which covers an area, which is not covered by the dense layer (11), of the surface of the porous layer (5) and a part of the dense layer (11) and through which the gas can pass; and a hydrogen separation layer (15) which has a hydrogen separation metal which can selectively transmit only hydrogen from gaseous matter containing hydrogen, covers the porous layer (13) and of which an end is jointed to the dense layer (11). Further, the hydrogen separation layer (15) is a mixed layer containing a ceramic and the hydrogen separation metal, the interface of the end contacting the dense layer (11) is configured from a ceramic porous base (19) and the hydrogen separation metal filled in a pore (21) of the porous base (19).
摘要翻译：要解决的问题：提供可以降低气体泄漏的氢分离体。解决方案：氢分离体（1）包括：气体可以通过的陶瓷多孔载体（5）; 具有气密性的陶瓷致密层（11），其形成在多孔载体（5）的表面的一部分上; 陶瓷多孔层（13），其覆盖多孔层（5）的表面和致密层（11）的一部分的未被致密层（11）覆盖的区域，并且气体可以通过该陶瓷多孔层通过; 和具有氢分离金属的氢分离层（15），其能够选择性地仅从含有氢的气态物质传输氢气，覆盖多孔层（13），其端部与致密层（11）接合。此外，氢分离层（15）是含有陶瓷和氢分离金属的混合层，与致密层（11）接触的端部的界面由陶瓷多孔质基体（19）构成，氢分离金属填充在多孔基材（19）的孔（21）中。

5. 发明专利

JP2013071849A Hydrogen production apparatus 审中-公开
标题翻译：氢生产设备
公开(公告)号：JP2013071849A
公开(公告)日：2013-04-22
申请号：JP2011209604
申请日：2011-09-26
申请人： Ngk Spark Plug Co Ltd , 日本特殊陶業株式会社 , Tokyo Gas Co Ltd , 東京瓦斯株式会社
发明人： TANAKA HIROYUKI , TAKAGI YASUHIRO , HIKOSAKA HIDEAKI , IZEKI KOYA , KUME TAKAO , IKEDA YOICHI
IPC分类号： C01B3/38 , C01B3/56
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen production apparatus preventing damage of a hydrogen separation layer, and having high capability for separating hydrogen from raw material gas.SOLUTION: A hydrogen separation cylinder 3 used in this hydrogen production apparatus 1 is constituted by combining a first molding 23 (for separating hydrogen) and a second molding 25 (for reforming raw material gas) which are different members, and at least a part of the surface of the second molding 25 has a contact with the surface of a porous ceramic protection layer 31 of the first molding 25. When the first molding 23 and the second molding 25 are arranged in contact with each other in this way, hydrogen can be separated and produced efficiently. Further, even when the first molding 23 and the second molding 25 which are different bodies are arranged in contact with each other, since there is a slight clearance 33 therebetween, even if stress is applied onto the first molding 23 and the second molding 25, there is such an advantage that a hydrogen separation layer 29 is hardly damaged.
摘要翻译：解决的问题：提供一种防止氢分离层损坏的氢制造装置，并且具有从原料气体分离氢的高能力。解决方案：在该氢气制备装置1中使用的氢气分离筒3通过组合作为不同构件的第一模制件23（用于分离氢气）和第二模制件25（用于重整原料气体），并且至少第二模制件25的表面的一部分与第一模制件25的多孔陶瓷保护层31的表面接触。当第一模塑件23和第二模塑件25以这种方式彼此接触时，可以有效地分离和生产氢。此外，即使不同体的第一模塑件23和第二模塑件25彼此接触，由于它们之间存在轻微的间隙33，即使在第一模塑件23和第二模塑件25上施加应力，存在氢分离层29几乎不被损坏的优点。版权所有（C）2013，JPO＆INPIT

6. 发明专利

JP2012228640A Gas separation apparatus 有权
标题翻译：气体分离装置
公开(公告)号：JP2012228640A
公开(公告)日：2012-11-22
申请号：JP2011097515
申请日：2011-04-25
申请人： Ngk Spark Plug Co Ltd , 日本特殊陶業株式会社 , Tokyo Gas Co Ltd , 東京瓦斯株式会社
发明人： KAWASE HIROKI , KAJITANI MASAHIRO , HIKOSAKA HIDEAKI , TAKAGI YASUHIRO , ITO MASAYA , IZEKI KOYA , KUME TAKAO , IKEDA YOICHI
IPC分类号： B01D53/22 , B01D69/10 , B01D69/12 , B01D71/02 , C01B3/38 , C01B3/56 , H01M8/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide a gas separation apparatus in which a cause of the occurrence of a pinhole is removed and consequently the occurrence of the pinhole can be prevented effectively.SOLUTION: A hydrogen separation cylinder 1 includes a mixed layer 13 between a hydrogen separation membrane 9 and a support 11 (barrier layer 7, in detail). In the mixed layer 13, a material of the hydrogen separation membrane and a material of the support are contained, in more detail, a mixing ratio of the material of the hydrogen separation membrane with that of the support is neither inclined nor varied in the thickness direction of the mixed layer 13. The mixed layer 13, when arranged between the hydrogen separation membrane 9 and the support 11, has such an effect that the pinhole hardly occurs on the hydrogen separation membrane 9.
摘要翻译：要解决的问题：提供一种除去针孔发生的原因的气体分离装置，从而可以有效地防止针孔的发生。解决方案：氢分离筒1包括氢分离膜9和支撑体11（详细的阻挡层7）之间的混合层13。在混合层13中，包含氢分离膜的材料和载体的材料，更详细地说，氢分离膜的材料与载体的材料的混合比既不倾斜也不改变厚度混合层13当配置在氢分离膜9和支撑体11之间时具有这样的效果：在氢分离膜9上几乎不发生针孔。（C）2013 ，JPO＆INPIT

7. 发明专利

JP2014156362A Hydrogen production apparatus 有权
标题翻译：氢生产设备
公开(公告)号：JP2014156362A
公开(公告)日：2014-08-28
申请号：JP2013026894
申请日：2013-02-14
申请人： Tokyo Gas Co Ltd , 東京瓦斯株式会社 , Ngk Spark Plug Co Ltd , 日本特殊陶業株式会社
发明人： IZEKI KOYA , KUME TAKAO , IKEDA YOICHI , ITO MASAYA , TAKAGI YASUHIRO , HIKOSAKA HIDEAKI , TANAKA HIROYUKI
IPC分类号： C01B3/38 , B01D53/22 , B01D63/06 , B01J33/00 , C01B3/56
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen production apparatus having a catalyst housing body in which an air permeable case is packed with pellet type catalyst of a quota evenly, being superior in hydrogen production efficiency, and preventing deterioration of a hydrogen separation body.SOLUTION: A hydrogen production apparatus 1 has a device shell 2, a hydrogen separation body 3, and a catalyst housing body 4. The catalyst housing body 4 is a unit in which a double tubular air permeable case 10 having a permeable inner peripheral wall 11 and outer peripheral wall 12 is packed with granular reforming catalyst 15. A plurality of catalyst housing bodies 4 is put on the hydrogen separation body 3 from outside and is arranged to be piled up within the device shell 2 by multistage. Reformed gas containing hydrogen gas is provided by source gas contacting with the reforming catalyst 15, and the hydrogen having passed through the hydrogen separation body 3 selectively is taken out from an extraction opening 6.
摘要翻译：要解决的问题：提供一种具有催化剂壳体的氢制造装置，其中透气性壳体均匀地填充有配量的颗粒状催化剂，氢生产效率优异，并且防止氢分离体的劣化。氢制造装置1具有装置壳体2，氢分离体3和催化剂壳体4.催化剂壳体4是具有透气性内周壁11和双层管状透气性壳体10的单体，外周壁12填充有粒状重整催化剂15.多个催化剂壳体4从外部放置在氢分离体3上，并且被布置成通过多段堆积在装置壳体2内。含有氢气的改性气体由与重整催化剂15接触的原料气提供，选择性地通过氢分离体3的氢从抽出口6取出。

8. 发明专利

JP2014111239A Hydrogen separation device 审中-公开
标题翻译：氢分离装置
公开(公告)号：JP2014111239A
公开(公告)日：2014-06-19
申请号：JP2012266347
申请日：2012-12-05
申请人： Ngk Spark Plug Co Ltd , 日本特殊陶業株式会社 , Tokyo Gas Co Ltd , 東京瓦斯株式会社
发明人： MITSUYA KOHEI , ITO MASAYA , TAKAGI YASUHIRO , HIKOSAKA HIDEAKI , IZEKI KOYA , KUME TAKAO , IKEDA YOICHI
IPC分类号： B01D53/22 , B01D63/00 , B01D63/06 , C01B3/56 , H01M8/04
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen separation device that can be made compact, and can make a wall member thin and simplify a structure in the wall member.SOLUTION: In a hydrogen separation device (1), a hydrogen separator (9) is fixed to a wall member (3) by a fixing mechanism (11) at a part of the wall member (3) which projects from a through hole (17). Specifically, when an outside fixation part (45) is threadably engaged with a wall member fixation part (43), first and second seal members (47, 51) made of expanded graphite are pressed (through a press member (53) etc.), so the first and second seal members (47, 51) spread radially to fasten a dense part (21) which is the projection part of the hydrogen separator (9). Consequently, the hydrogen separator (9) is fixed to the wall member (3).
摘要翻译：要解决的问题：提供一种可以制造得紧凑的氢分离装置，并且可以使壁构件变薄并且简化壁构件的结构。解决方案：在氢分离装置（1）中，氢气分离器（9）在壁构件（3）的从通孔（17）突出的一部分处通过固定机构（11）固定在壁构件（3）上。具体而言，当外壁固定部45与壁部件固定部43螺纹接合时，由膨胀石墨制成的第一密封部件47和第二密封部件51通过按压部件53被按压）因此第一和第二密封构件（47,51）径向扩张以紧固作为氢分离器（9）的突出部分的致密部分（21）。因此，氢分离器（9）固定在壁部件（3）上。

9. 发明专利

JP2014046228A Method for manufacturing hydrogen separator 有权
标题翻译：制氢分离器的方法
公开(公告)号：JP2014046228A
公开(公告)日：2014-03-17
申请号：JP2012189152
申请日：2012-08-29
申请人： Ngk Spark Plug Co Ltd , 日本特殊陶業株式会社 , Tokyo Gas Co Ltd , 東京瓦斯株式会社
发明人： KAWASE HIROKI , HIKOSAKA HIDEAKI , TAKAGI YASUHIRO , KAJITANI MASAHIRO , IZEKI KOYA , KUME TAKAO , IKEDA YOICHI
IPC分类号： B01D71/02 , B01D69/10 , B01D69/12 , C01B3/56 , C22C1/05 , C22C1/08
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a hydrogen separator, capable of reducing the occurrence of pin holes in a hydrogen separation metal layer.SOLUTION: A method for manufacturing a hydrogen separator includes: a first step of mixing Pd being a hydrogen separation metal, or metal powder containing the Pd and a metal (e.g., Ag) alloyed with the Pd for improving a hydrogen permeability as the main component with ceramics (e.g., YSZ) powder to make past-like materials; a second step of forming a surface forming layer (77) on support molded body (73) by covering the surface of the porous support molded body (73) before sintering using the past-like materials; and a third step of co-firing the support molded body (73) with the surface forming layer (77), and performing the sintering thereof. Consequently, a porous medium (20) comprising the hydrogen separation metal layer (19) inside is made.
摘要翻译：要解决的问题：提供一种能够减少氢分离金属层中的针孔的发生的氢分离器的制造方法。解决方案：氢分离器的制造方法包括：将作为氢的Pd 分离金属或包含Pd的金属粉末和与Pd合金化的金属（例如，Ag），以提高渗透性作为主要成分的陶瓷（例如YSZ）粉末以制造过去的材料; 第二步骤，在使用过去的材料烧结之前，通过覆盖多孔支撑成型体（73）的表面，在支撑成型体（73）上形成表面形成层（77）以及将所述支撑成型体（73）与所述表面形成层（77）共烧的第三工序，进行烧结。因此，制成内部包含氢分离金属层（19）的多孔介质（20）。

10. 发明专利

JP2013034913A Hydrogen separation apparatus 审中-公开
标题翻译：氢分离装置
公开(公告)号：JP2013034913A
公开(公告)日：2013-02-21
申请号：JP2011170421
申请日：2011-08-03
申请人： Ngk Spark Plug Co Ltd , 日本特殊陶業株式会社 , Tokyo Gas Co Ltd , 東京瓦斯株式会社
发明人： KAJITANI MASAHIRO , HIKOSAKA HIDEAKI , TAKAGI YASUHIRO , ITO MASAYA , IZEKI KOYA , KUME TAKAO , IKEDA YOICHI
IPC分类号： B01D53/22 , B01D63/00 , B01D69/10 , B01D69/12 , B01D71/02 , C01B3/38 , H01M8/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To provide a hydrogen separation apparatus capable of preventing a gas to be separated (gas before separation) from leaking outside the apparatus.SOLUTION: The hydrogen separation apparatus 1 is provided with an airtight mixture layer 15 which contains, between a hydrogen-permeable membrane 17 and a compact support part 13, the component (Pd) of the hydrogen-permeable membrane 17 and the component, yttria-stabilized zirconia (YSZ) of the compact support part 13. Since the mixture layer 15 joins solidly to the membrane 17 and the support part 13, the hydrogen separation apparatus can prevent a raw material gas from leaking out of a joint portion even when feeding high-pressure raw material gas to the central hole 9 of a hydrogen separation tube 3.
摘要翻译：解决的问题：提供能够防止气体分离（分离前的气体）在设备外部泄漏的氢分离装置。解决方案：氢分离装置1设置有气密混合层15，其在透氢膜17和致密支撑部13之间包含氢透膜17的成分（Pd）和成分，紧凑型支撑部13的氧化钇稳定化氧化锆（YSZ）。由于混合层15牢固地与膜17和支撑部13连接，氢分离装置可以防止原料气体甚至从接合部分泄漏出来将高压原料气体供给到氢分离管3的中心孔9时。（C）2013，JPO＆INPIT

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