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    • 2. 发明专利
    • Oxide superconducting thin film and method for producing the same
    • 氧化物超导薄膜及其制造方法
    • JP2012174564A
    • 2012-09-10
    • JP2011036535
    • 2011-02-23
    • Sumitomo Electric Ind LtdNational Institute Of Advanced Industrial & Technology住友電気工業株式会社独立行政法人産業技術総合研究所
    • NAGAISHI TATSUOKIHONDA GENKIYAMAGUCHI IWAOMANABE TAKAAKIHIKATA TAKESHIMATSUI HIROAKIKONDO WAKICHIYAMAZAKI HIROFUMIKUMAGAI TOSHIYA
    • H01B12/06C01G1/00H01B13/00H01L39/24
    • Y02E40/642
    • PROBLEM TO BE SOLVED: To provide an oxide superconducting thin film which can obtain a sufficiently high Ic, and to provide a method for producing the same.SOLUTION: The oxide superconducting thin film 2 contains nano fine particles 3 which are dispersed in the flim and function as pinning of a magnetic flux. The oxide superconducting thin film of which the dispersion density of the nano fine particles in the oxide superconducting thin film is 10-10pieces/m. The oxide superconducting thin film of which a particle diameter of the nano fine particle is 5-100 nm. The method for producing the oxide superconducting thin film comprises the steps of: adding a predetermined amount of a solution prepared by dissolving the nano fine particles that function as pinning of the magnetic flux in a solvent, to a solution prepared by dissolving an organic metallic compound in a solvent, to prepare a raw material solution for the oxide superconducting thin film; and forming the oxide superconducting thin film by using the raw material solution with metal organic deposition. The method for producing the oxide superconducting thin film further comprises adding a dispersion liquid to the solution prepared by dissolving the nano fine particles in the solvent.
    • 要解决的问题:提供可以获得足够高的Ic的氧化物超导薄膜,并提供其制造方法。 解决方案:氧化物超导薄膜2含有纳米微粒3,其分散在薄膜中并用作磁通的钉扎。 氧化物超导薄膜中的氧化物超导薄膜中的纳米细颗粒的分散密度为10 24 件/ m 3 。 其纳米微粒的粒径为5〜100nm的氧化物超导薄膜。 制造氧化物超导薄膜的方法包括以下步骤:将通过将作为磁通的钉扎的纳米微粒溶解在溶剂中而制备的预定量的溶液添加到通过将有机金属化合物 在溶剂中制备氧化物超导薄膜的原料溶液; 并通过使用具有金属有机沉积的原料溶液形成氧化物超导薄膜。 制造氧化物超导薄膜的方法还包括向通过将纳米细颗粒溶解在溶剂中而制备的溶液中加入分散液。 版权所有(C)2012,JPO&INPIT
    • 3. 发明专利
    • Method of manufacturing oxide superconducting thin film
    • 氧化物超导薄膜的制造方法
    • JP2011198521A
    • 2011-10-06
    • JP2010061373
    • 2010-03-17
    • National Institute Of Advanced Industrial Science & TechnologySumitomo Electric Ind Ltd住友電気工業株式会社独立行政法人産業技術総合研究所
    • MANABE TAKAAKIYAMAGUCHI IWAOHIKATA TAKESHIOKI YASUTARO
    • H01B13/00C01G1/00C01G3/00
    • PROBLEM TO BE SOLVED: To provide a method of manufacturing an oxide superconducting thin film, enabling manufacture of the oxide superconducting thin film having uniform-crystal-orientation high Ic by stacking calcined films produced in a MOD method to produce a thick calcined film and then applying glost firing heat treatment thereto.SOLUTION: The method is provided for manufacturing the oxide superconducting thin film in an application thermal decomposition method using a metal organic compound as a raw material. The method includes a stacked calcined film layer producing step of producing stacked calcined film layers by applying metal organic compound solution onto a substrate 10 to produce a coating film and then giving heat treatment to the coating film at a calcining heat treatment temperature for thermally decomposing organic components to be removed from the metal organic compound to produce the calcined film 20, in a repetitive manner, a crystallization suppressing layer producing step of producing a crystallization suppressing layer 30 on the uppermost layer out of the stacked calcined film layers for suppressing the crystallization of the stacked calcined film layers, and an oxide superconducting thin film producing step of producing the oxide superconducting thin film by giving heat treatment at a glost firing heat treatment temperature to the stacked calcined film layers to be crystallized.
    • 要解决的问题:为了提供一种制造氧化物超导薄膜的方法,能够通过将通过MOD方法制造的煅烧膜堆叠以制备厚的煅烧膜,从而制造具有均匀晶体取向的高Ic的氧化物超导薄膜,然后 对其进行烧灼热处理。解决方案:该方法用于在以金属有机化合物为原料的应用热分解方法中制造氧化物超导薄膜。 该方法包括:堆叠的煅烧膜层的制造步骤,通过将金属有机化合物溶液施加到基板10上以制备涂膜,然后在焙烧热处理温度下对涂膜进行热分解有机物 从金属有机化合物除去的成分,以重复的方式制造结晶抑制层的制造工序,在叠层的煅烧膜层的最上层制造结晶抑制层30,以抑制结晶化 堆叠的煅烧膜层和氧化物超导薄膜的生产步骤,通过在烧结热处理温度下进行热处理以生成氧化物超导薄膜,使堆叠的煅烧膜层结晶化。
    • 4. 发明专利
    • Method for producing oxide superconductive thin film
    • 生产氧化物超导薄膜的方法
    • JP2011230946A
    • 2011-11-17
    • JP2010101261
    • 2010-04-26
    • National Institute Of Advanced Industrial Science & TechnologySumitomo Electric Ind Ltd住友電気工業株式会社独立行政法人産業技術総合研究所
    • YAMAGUCHI IWAOKUMAGAI TOSHIYAHIKATA TAKESHIOKI YASUTARO
    • C01G1/00B05D5/12H01B13/00
    • PROBLEM TO BE SOLVED: To provide a method for producing an oxide superconductive thin film which forms a calcined film in which roughening generated in the surface is suppressed upon the calcining of a coating film of an MOD (Metal Organic Deposition) solution, and produces an oxide superconductive thin film having sufficiently high Jc and Ic by the subsequent normal firing.SOLUTION: The method for producing an oxide superconductive thin film uses a metal organic compound as raw material to produce an oxide superconductive thin film used for producing a superconductive wire rod, by metal organic deposition. The method includes: a coating film producing step of coating the surface of a substrate with a solution of a metal organic compound to produce a coating film; a calcining heat treatment step of thermally decomposing and removing organic components contained in the metal organic compound of the coating film to produce a calcined film; and a normal firing heat treatment step of crystallizing the calcined film to produce an oxide superconductive thin film. In the calcining heat treatment, temperature rising till a calcining heat treatment temperature is performed under a pressure atmosphere lower than the atmospheric pressure.
    • 要解决的问题:提供一种形成氧化物超导薄膜的方法,该氧化物超导薄膜形成煅烧膜,其中在对MOD(金属有机沉积)溶液的涂膜进行煅烧时,在表面产生粗糙度被抑制, 并通过随后的正常烧制产生具有足够高的Jc和Ic的氧化物超导薄膜。 解决方案:氧化物超导薄膜的制造方法使用金属有机化合物作为原料,通过金属有机沉积来制造用于制造超导线材的氧化物超导薄膜。 该方法包括:涂膜生产步骤,用金属有机化合物的溶液涂覆基材的表面以产生涂膜; 煅烧热处理步骤,热分解和除去涂膜的金属有机化合物中所含的有机组分以产生煅烧膜; 以及将煅烧膜结晶以产生氧化物超导薄膜的正常烧成热处理步骤。 在煅烧热处理中,在低于大气压的压力气氛下进行升温至煅烧热处理温度。 版权所有(C)2012,JPO&INPIT
    • 8. 发明专利
    • Catalyst structure and method for manufacturing carbon nanostructure using the same
    • 使用其制造碳纳米结构的催化剂结构和方法
    • JP2012016707A
    • 2012-01-26
    • JP2011233209
    • 2011-10-24
    • Osaka PrefectureSumitomo Electric Ind Ltd住友電気工業株式会社大阪府
    • HIKATA TAKESHIMIZUKOSHI TOMOYUKI
    • B01J23/89B01J37/34C01B31/02
    • PROBLEM TO BE SOLVED: To provide a catalyst structure that improves deposition efficiency in manufacturing carbon nanostructures consisting of carbon crystals through vapor phase deposition, and to provide a method for manufacturing the carbon nanostructures using the same.SOLUTION: In the catalyst structure to be used for manufacturing carbon nanostructures consisting of carbon crystals through vapor phase deposition, a plate body is penetrated in a thickness direction with a first metal and a second metal. The first metal is formed as a plurality of filaments. The filaments are held at intervals by a substrate with their longitudinal direction aligned with the thickness direction of the plate body. One end of the filament is exposed on a first surface while the other-end is connected to the second metal to expose the second metal on a second surface. The first metal includes a material composed primarily of cobalt or nickel. The second metal includes a material containing palladium. The catalyst structure is used for a method for manufacturing the carbon nanostructures.
    • 要解决的问题:提供一种催化剂结构,其提高通过气相沉积制造由碳晶体组成的碳纳米结构的沉积效率,并提供使用其制造碳纳米结构的方法。 解决方案:在通过气相沉积用于制造由碳晶体构成的碳纳米结构的催化剂结构中,板体在第一金属和第二金属的厚度方向上穿透。 第一金属形成为多根细丝。 长丝被基板保持间隔,其长度方向与板体的厚度方向一致。 灯丝的一端暴露在第一表面上,而另一端连接到第二金属,以暴露第二表面上的第二金属。 第一金属包括主要由钴或镍组成的材料。 第二金属包括含钯的材料。 催化剂结构用于制造碳纳米结构的方法。 版权所有(C)2012,JPO&INPIT
    • 10. 发明专利
    • Method for manufacturing carbon nanostructure, catalyst metal base and catalytic reaction container
    • 制造碳纳米管结构的方法,催化剂金属基和催化反应容器
    • JP2007222959A
    • 2007-09-06
    • JP2006043735
    • 2006-02-21
    • Sumitomo Electric Ind Ltd住友電気工業株式会社
    • HISAGAI YUICHIHIKATA TAKESHI
    • B82B3/00C01B31/02
    • PROBLEM TO BE SOLVED: To provide a method for manufacturing a carbon nanostructure, in which a high purity long-length carbon nanostructure can be stably manufactured. SOLUTION: A catalytic reaction container equipped with: an airtight container; a catalyst metal base partitioning the inner space of the airtight container into a first space and a second space; and a fixing member to fix the catalyst metal base, is used. The catalyst metal base is disposed to have a first surface in contact with the first space and a second surface in contact with the second space, and the base is processed to have a recessed portion and/or a projected portion formed in at least a part of the second surface. A source gas containing at least carbon is supplied to the first space, and the carbon reaching the second surface from the first surface through the inner part of the catalyst metal base is grown into a carbon nanostructure from the recessed portion and/or the projectrd portion as a base point. COPYRIGHT: (C)2007,JPO&INPIT
    • 待解决的问题:提供可以稳定制造高纯度长度碳纳米结构的碳纳米结构体的制造方法。 解决方案:一种装有气密容器的催化反应容器; 将所述气密容器的内部空间分隔成第一空间和第二空间的催化剂金属基体; 和用于固定催化剂金属基底的固定构件。 催化剂金属基底设置成具有与第一空间接触的第一表面和与第二空间接触的第二表面,并且基底被加工成具有形成在至少一部分中的凹部和/或突出部分 的第二个表面。 将含有至少碳的源气体供给到第一空间,从催化剂金属基体的内部到达第一表面的第二表面的碳从凹部和/或突出部分生长成碳纳米结构体 作为基点。 版权所有(C)2007,JPO&INPIT