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1. 发明专利

JP2009252641A Method of producing superconducting oxide material 有权
标题翻译：生产超导氧化物材料的方法
公开(公告)号：JP2009252641A
公开(公告)日：2009-10-29
申请号：JP2008101536
申请日：2008-04-09
申请人： Japan Steel Works Ltd:The , National Institute Of Advanced Industrial & Technology , 株式会社日本製鋼所 , 独立行政法人産業技術総合研究所
发明人： NAKAMURA TETSUSHIGE , SATO RYOSUKE , KOYANAGI KUNIHIKO , EBISAWA TAKASHI , OTSU HIDEHIKO , SOMA MITSUGI , TSUCHIYA TETSUO , KUMAGAI TOSHIYA , TSUKADA KENICHI
IPC分类号： H01B13/00 , C01G1/00 , C01G3/00 , H01L39/24
摘要： PROBLEM TO BE SOLVED: To provide a method of producing a superconducting oxide material that achieves the same effect as that obtained by back irradiation even when forming a thinner film by overglazing without limiting laser irradiation conditions and even when forming films on both sides of a substrate.
SOLUTION: The method of producing an epitaxially grown superconducting coating material includes: a process (1) of applying a solution of metallic organic compound having an oxide for forming a superconducting material onto the substrate and drying it; a provisional firing process (2) of pyrolizing an organic matter in the metallic organic compound; and a full-scale firing process (3) of performing conversion into a superconducting material, wherein, when a laser is irradiated between the processes (1) and (2), a scattering mechanism is disposed immediately before a surface coated with the solution of metallic organic compound where the superconducting material is formed, and a laser, after being once scattered, is irradiated to the organic compound solution.
COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种制造超导氧化物材料的方法，即使在不限制激光照射条件的情况下甚至当在两侧形成膜时，通过过度玻璃形成较薄的膜也能获得与通过反向照射获得的效果相同的效果的基底。解决方案：制备外延生长的超导涂层材料的方法包括：将具有用于形成超导材料的氧化物的金属有机化合物溶液施加到基底上并干燥的方法（1）对金属有机化合物中的有机物进行热处理的暂时烧制工序（2）以及进行超导材料的转换的全尺寸焙烧工序（3），其中，当在工序（1）和（2）之间照射激光时，散射机构紧接在被涂覆有其中形成超导材料的金属有机化合物和被一次散射的激光照射到有机化合物溶液上。版权所有（C）2010，JPO＆INPIT

2. 发明专利

JP2008198396A Manufacturing method of superconductive oxide material 有权
标题翻译：超导氧化物材料的制造方法
公开(公告)号：JP2008198396A
公开(公告)日：2008-08-28
申请号：JP2007029775
申请日：2007-02-08
申请人： Japan Steel Works Ltd:The , National Institute Of Advanced Industrial & Technology , 株式会社日本製鋼所 , 独立行政法人産業技術総合研究所
发明人： SOMA MITSUGI , TSUCHIYA TETSUO , KUMAGAI TOSHIYA , TSUKADA KENICHI , KOYANAGI KUNIHIKO , EBISAWA TAKASHI , OTSU HIDEHIKO
IPC分类号： H01B12/06 , C01G1/00 , C01G3/00 , H01B13/00
CPC分类号： H01L39/2425 , C23C18/1216 , C23C18/1245 , C23C18/1295 , C23C18/14 , H01L39/2451
摘要： PROBLEM TO BE SOLVED: To provide a manufacturing method of a large-area superconductive material with improved performance, and efficient without causing ablation, in carrying out thermal decomposition of a metal organic compound and heat treatment formation of a superconductive substance.
SOLUTION: In the manufacturing method of the superconductive oxide material for manufacturing a superconductive coating material epitaxially grown through a process (1) of coating organic compound solution of metal whose oxide forms a superconductive substance on a support body and drying it, a temporary calcination process (2) thermally decomposing organic components in the metal organic compound, and a proper calcination process (3) carrying out conversion into the superconductive substance, laser light is irradiated between the process (1) and the process (2).
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：解决的问题：为了提供一种具有改进的性能，高效率而不引起烧蚀的大面积超导材料的制造方法，在进行金属有机化合物的热分解和热处理形成超导物质时。解决方案：在用于制造超导涂层材料的超导氧化物材料的制造方法中，通过将氧化物形成超导性物质的金属的有机化合物溶液涂覆在载体上并干燥而外延生长，临时煅烧方法（2）将金属有机化合物中的有机成分热分解，进行超导性物质的转化的适当的煅烧工序（3）在工序（1）和工序（2）之间照射激光。版权所有（C）2008，JPO＆INPIT

3. 发明专利

JP2008037726A Process for producing superconducting oxide material 有权
标题翻译：生产超导氧化物材料的工艺
公开(公告)号：JP2008037726A
公开(公告)日：2008-02-21
申请号：JP2006217678
申请日：2006-08-10
申请人： Japan Steel Works Ltd:The , National Institute Of Advanced Industrial & Technology , 株式会社日本製鋼所 , 独立行政法人産業技術総合研究所
发明人： SOMA MITSUGI , TSUCHIYA TETSUO , KUMAGAI TOSHIYA , TSUKADA KENICHI , KOYANAGI KUNIHIKO , EBISAWA TAKASHI , OTSU HIDEHIKO
IPC分类号： C01G1/00 , C01G3/00 , C30B29/22 , H01B12/06
CPC分类号： C01G1/02 , C01G3/006 , C01P2002/82 , C01P2006/40 , C23C18/1216 , C23C18/1283 , C23C18/1291 , C23C18/14 , C30B7/02 , C30B29/22 , H01L39/2425 , H01L39/2451
摘要： PROBLEM TO BE SOLVED: To provide a process in which a superconducting material of a large area with improved properties is efficiently produced through pyrolysis of a metallic organic compound and thermal treatment formation of a superconducting substance. SOLUTION: The process for producing a superconducting material having undergone epitaxial growth through the steps of (1) coating a support with a solution of an organic compound of a metal whose oxide forms a superconducting substance and drying the same, (2) preliminary firing for pyrolysis of the organic component of the organic compound of the metal and (3) principal firing for conversion to the superconducting substance, characterized in that between the step (1) and (2), at the time of laser beam irradiation, laser beam irradiation is carried out from the side opposite to the side coated with the solution of the organic compound of the metal for formation of the superconducting substance. COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：要解决的问题：提供一种通过金属有机化合物的热分解和超导物质的热处理形成有效地产生具有改进性能的大面积超导材料的方法。（1）用氧化物形成超导物质的金属的有机化合物的溶液涂覆载体并干燥所述超导材料的方法，（2）通过以下步骤进行外延生长的超导材料的制造方法：（1）对金属有机化合物的有机组分进行热解的初步烧制和（3）转换为超导物质的主要烧制，其特征在于，在步骤（1）和（2）之间，在激光束照射时，从与用于形成超导物质的金属的有机化合物的溶液涂覆的一侧相反的一侧进行激光束照射。版权所有（C）2008，JPO＆INPIT

4. 发明专利

JP2010275119A Method and apparatus for producing superconductive oxide material 有权
标题翻译：用于生产超导氧化物材料的方法和装置
公开(公告)号：JP2010275119A
公开(公告)日：2010-12-09
申请号：JP2009126121
申请日：2009-05-26
申请人： Japan Steel Works Ltd:The , National Institute Of Advanced Industrial Science & Technology , 株式会社日本製鋼所 , 独立行政法人産業技術総合研究所
发明人： KITADA NORITAKA , NAKAMURA TETSUSHIGE , SATO RYOSUKE , KOYANAGI KUNIHIKO , SOMA MITSUGI , TSUKADA KENICHI , TSUCHIYA TETSUO , YAMAGUCHI IWAO , MANABE TAKAAKI , KUMAGAI TOSHIYA
IPC分类号： C01G1/00 , C01G3/00 , H01B12/06 , H01B13/00
CPC分类号： Y02E40/642
摘要： PROBLEM TO BE SOLVED: To provide a method for producing a superconductive oxide material by which a superconductive oxide film of good quality is obtained in a large area on a substrate and easy control is achieved. SOLUTION: In the method for producing a superconductive oxide material, at the time of producing a superconductive coating material epitaxially grown through a step (A) wherein an organic compound solution of a metal whose oxide forms a superconductive substance is applied onto a substrate and dried, a laser irradiation step (B) wherein the organic component of the organic compound of the metal is photodegraded with laser, a temporary firing step (C) wherein the organic component in the organic compound of the metal is thermally decomposed, and a concluding firing step (C) wherein conversion to a superconductive substance is performed, the laser irradiation of the step (B) is performed under substrate cooling by cooling the substrate (4) by surface contact of a cooling body with the substrate (4). COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：解决的问题：提供一种用于制造超导氧化物材料的方法，通过该方法可以在基板上大面积地获得质量好的超导氧化物膜，并且实现了容易的控制。解决方案：在制造超导氧化物材料的方法中，在制造通过其中将氧化物形成超导性物质的金属的有机化合物溶液施加到其上的步骤（A）外延生长的超导涂层材料时，基板并干燥，其中金属的有机化合物的有机组分用激光光降解的激光照射步骤（B），金属有机化合物中的有机组分被热分解的临时烧制步骤（C），以及执行转换为超导物质的结束烧制步骤（C），通过冷却体与基板（4）的表面接触来冷却基板（4），在基板冷却下进行步骤（B）的激光照射，。版权所有（C）2011，JPO＆INPIT

5. 发明专利

JP2010036236A Laser beam irradiation method and apparatus 审中-公开
标题翻译：激光束辐射方法和装置
公开(公告)号：JP2010036236A
公开(公告)日：2010-02-18
申请号：JP2008205098
申请日：2008-08-08
申请人： Japan Steel Works Ltd:The , 株式会社日本製鋼所
发明人： NAKAMURA TETSUSHIGE , SATO RYOSUKE , KOYANAGI KUNIHIKO , TERAO KATSUHIRO , EBISAWA TAKASHI , OTSU HIDEHIKO
IPC分类号： B23K26/00 , B23K26/04 , B23K26/073 , B23K26/08 , H01L21/268 , H01L21/31
摘要： PROBLEM TO BE SOLVED: To provide a laser beam irradiation method and apparatus, which can perform uniform machining by eliminating adverse effects of heat when a photolytic reaction is caused on a substrate by laser beam irradiation. SOLUTION: In the laser beam irradiation method, the photolytic reaction is caused by irradiating a raw film precursor formed on the substrate with a laser beam in producing a thin film on the substrate. The laser beam is radiated while the substrate is rotated in the planar direction and is moved along the planar direction relative to a position to be irradiated with the laser beam. The irradiation apparatus includes a supporting section which supports the substrate on which the raw film is formed, a rotating mechanism which rotates the substrate, a moving mechanism which moves the substrate along the planar direction, a laser beam irradiation means which irradiates the substrate with the laser beam, and a controlling section which causes the photolytic reaction on the raw film by irradiating the substrate with the laser beam by the laser beam irradiation means while the substrate is rotated in the planar direction by the rotating mechanism and is moved relatively along the planar direction by the moving mechanism. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：提供一种激光束照射方法和装置，其可以通过在激光束照射下在基板上引起光解反应时消除热的不利影响而进行均匀的加工。解决方案：在激光束照射方法中，通过用激光束照射形成在基板上的原料膜前驱物在基板上产生薄膜而引起光解反应。激光束在基板沿平面方向旋转时被辐射并且相对于要被激光束照射的位置沿平面方向移动。照射装置包括：支撑部，其支撑形成有原料膜的基板;旋转基板的旋转机构;沿着平面方向移动基板的移动机构;激光束照射装置，激光束，以及控制部，其通过激光束照射装置在激光束照射基板的同时通过旋转机构在平面方向上旋转而沿着平面方向相对移动而在原料膜上引起光解反应，方向由移动机构。版权所有（C）2010，JPO＆INPIT

6. 发明专利

JP2004281235A Reformer 审中-公开
标题翻译：重整
公开(公告)号：JP2004281235A
公开(公告)日：2004-10-07
申请号：JP2003071214
申请日：2003-03-17
申请人： Japan Steel Works Ltd:The , 株式会社日本製鋼所
发明人： KOYANAGI KUNIHIKO , TERAO KATSUHIRO
IPC分类号： C01B3/34 , C01B3/56 , H01M8/06
CPC分类号： Y02E60/50
摘要： PROBLEM TO BE SOLVED: To solve such problems that in a reforming chamber, in order to efficiently raise the temperature of fuel gas to reaction temperature, installation of a heating chamber separately from the reforming chamber to preheat the fuel gas before supplying to the reforming chamber is desired, but this makes system constitution complicated. SOLUTION: A fuel gas passage 10 is divided through a partition wall 9 in at least three sides of surrounding of a square reforming chamber 7, the heating chamber 14 to which combustion heat from a combustion chamber 8 is transmitted is installed, a plurality of fins 15 extending in the front and rear direction are installed in parallel on the inside of the reforming chamber 7 to divide a reaction gas passage 13, the fuel gas 3 is made to flow from an inlet 10a at one end of the heating chamber 14 and to flow through the fuel gas passage 10 while heated, supplied to a rear end part of the reforming chamber 7 through an outlet 10b at the other end of the heating chamber 14, the fuel gas 3 entered in the reforming chamber 7 is guided with fins 15 and advanced through the reaction gas passage 13 to form reformed gas 2, and the reformed gas 2 is made to flow out of a reformed gas outlet 4 at the front end of the reforming chamber 7. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：解决的问题为了解决这样的问题，在重整室中，为了有效地将燃料气体的温度提高到反应温度，与重整室分开设置加热室，以在供给前预热燃料气体需要重整室，但这使得系统结构变得复杂。解决方案：燃料气体通道10在方形重整室7的周围的至少三个侧面中通过分隔壁9分开，来自燃烧室8的燃烧热量被传送到的加热室14被安装，在前后方向上延伸的多个翅片15平行地安装在重整室7的内部，以分隔反应气体通道13，使燃料气体3从加热室一端的入口10a流出并且在加热的同时通过燃料气体通道10通过加热室14的另一端的出口10b供给到重整室7的后端部，进入重整室7的燃料气体3被引导带有翅片15，并通过反应气体通道13前进，形成重整气体2，并使重整气体2从重整室7前端的重整气体出口4流出。版权所有（C））2005年，日本特许厅和NCIPI

7. 发明专利

JPH11279267A Production of polylactic acid 失效
标题翻译：生产聚酸
公开(公告)号：JPH11279267A
公开(公告)日：1999-10-12
申请号：JP8357898
申请日：1998-03-30
申请人： Japan Steel Works Ltd:The , 株式会社日本製鋼所
发明人： SUMIHIRO YUKIHIRO , FUKUSHIMA TAKESHI , KOYANAGI KUNIHIKO , HASHIMOTO NORIAKI
IPC分类号： C08G63/06 , C08G63/78
摘要： PROBLEM TO BE SOLVED: To industrially advantageously obtain a polylactic acid having a high molecular weight, capable of resolving problems such as a limit of stirring viscosity, polymer attachment to a stirring wing and a lowering of molecular weight by re-heating after a solid state polymerization, by stirring the inside of a reaction tank with a twin-screw type stirrer, in a melt polymerization of a lactic acid monomer and a solid state polymerization of the obtained polylactic acid.
SOLUTION: This production of polylactic acid is conducted by charging a lactic acid monomer in a reaction tank, refluxing water, a lactide, a polylactic acid oligomer and occasionally a solvent generated from the reaction tank and performing a melt polymerization while removing water to outside of the reaction system, then subjecting the resultant polylactic acid to a solid polymerization at a temperature lower than its melting point. At this time, the stirring in the reaction tank is performed by using a twin screw-type stirrer. Preferably, the stirrer is provided in a state that the two screws are engaged with each other. Furthermore, the one in which both the two screws are indipendently rotatable is preferable. Otherwise, the screw is preferably are-integratable segment type.
COPYRIGHT: (C)1999,JPO
摘要翻译：待解决的问题：在工业上有利地获得具有高分子量的聚乳酸，能够解决搅拌粘度的极限，聚合物附着在搅拌翼上的问题，以及在固态之后再加热降低分子量通过用双螺杆型搅拌器搅拌反应罐内部，在乳酸单体的熔融聚合和所得聚乳酸的固态聚合中进行聚合。解决方案：聚乳酸的生产是通过在反应槽中加入乳酸单体，回流水，丙交酯，聚乳酸低聚物和有时由反应罐产生的溶剂进行熔融聚合，同时将水除去至反应体系，然后在低于其熔点的温度下使所得聚乳酸进行固体聚合。此时，通过使用双螺杆型搅拌器进行反应罐的搅拌。优选地，在两个螺钉彼此接合的状态下设置搅拌器。此外，优选两个螺钉都是独立旋转的。否则，螺杆优选是可整合的段型。

8. 发明专利

JP2007302507A Method for producing superconducting thin film 审中-公开
标题翻译：生产超薄膜的方法
公开(公告)号：JP2007302507A
公开(公告)日：2007-11-22
申请号：JP2006132120
申请日：2006-05-11
申请人： Japan Steel Works Ltd:The , 株式会社日本製鋼所
发明人： KOYANAGI KUNIHIKO , EBISAWA TAKASHI , OTSU HIDEHIKO
IPC分类号： C01G3/00 , C01G1/00 , C30B1/02 , C30B29/22 , H01L39/24
摘要： PROBLEM TO BE SOLVED: To solve the problem that the main burning which is a crystallization step takes a long time in a coating pyrolysis method which is one of the methods for producing a superconducting thin film.
SOLUTION: In the coating pyrolysis method, a coating film 3 containing the constituent element of a superconductor is formed on the upper layer of a substrate 1. Further, a surface side seed material layer 4 is formed on the surface side of the coating film 3 to perform temporary burning and main burning. During the main burning, crystallization is performed towards the surface from the substrate 1 side, and crystallization is also performed towards the substrate side from the surface side seed material layer 4. As a result, the time required for crystallization is shortened by performing crystallization from both directions. Furthermore, it is desirable to form a buffer layer 2 between the substrate 1 and the coating film 3. The buffer layer 2 prevents the chemical reaction of the substrate 1 with the coating film 3 and functions as a seed for crystallization.
COPYRIGHT: (C)2008,JPO&INPIT
摘要翻译：解决的问题为了解决在作为制造超导薄膜的方法之一的涂料热解法中长时间存在结晶步骤的主要燃烧的问题。解决方案：在涂层热解法中，在基材1的上层上形成含有超导体的构成元素的涂膜3.此外，表面侧种子层4形成在基材1的表面侧。涂膜3进行临时燃烧和主燃。在主燃烧期间，从基板1侧向表面进行结晶化，从表面侧种子材料层4向基板侧进行结晶化。其结果是，通过从两个方向。此外，希望在基板1和涂膜3之间形成缓冲层2.缓冲层2防止基板1与涂膜3发生化学反应，起到晶种的作用。版权所有（C）2008，JPO＆INPIT

9. 发明专利

JP2006124233A Reforming reactor 审中-公开
标题翻译：改性反应器
公开(公告)号：JP2006124233A
公开(公告)日：2006-05-18
申请号：JP2004315100
申请日：2004-10-29
申请人： Japan Steel Works Ltd:The , 株式会社日本製鋼所
发明人： KOYANAGI KUNIHIKO , MASHITA TORU , NAKAMURA TETSUSHIGE
IPC分类号： C01B3/38 , B01D53/22 , B01J19/24
CPC分类号： Y02P20/52
摘要： PROBLEM TO BE SOLVED: To use a compact reforming reactor excellent in durability so as to efficiently perform a reforming reaction accompanied with endothermic action for obtaining a hydrogen-containing gas by using a hydrocarbon or an oxygen-containing hydrocarbon as a raw material. SOLUTION: Flow passages 2 for a raw material gas are formed through a catalyst carrier block 1, then a catalyst is supported on the inner surface of each flow passage 2 for the raw material gas, and a cylindrical gas separation membrane 20 having an interval between the inner surface of the flow passage 2 for the raw material gas and itself is arranged in each flow passage 2 for the raw material gas. Ventilation passages 21, 22 for taking out the permeated gas to the outside of the catalyst carrier block 1 are connected to the gas separation membrane 20. The temperature of the catalyst carrier block 1 is raised by providing a heating means 3 for heating the catalyst carrier block 1 or by the motion of other functions. Thereby, the reforming reaction is stabilized, and it becomes possible to perform the reaction at a higher conversion rate than the equilibrium conversion rate. The apparatus is easily made compact, and the restriction is also small when a reformer is installed in a desired site. COPYRIGHT: (C)2006,JPO&NCIPI
摘要翻译：要解决的问题：使用耐久性优异的紧凑型重整反应器，以便通过使用烃或含氧烃作为原料有效地进行伴随吸热作用的重整反应，以获得含氢气体。解决方案：通过催化剂载体块1形成用于原料气体的流动通道2，然后将催化剂负载在用于原料气体的每个流动通道2的内表面上，并且具有圆柱形气体分离膜20，其具有在原料气体的流路2中配置有用于原料气体的流路2的内表面与其自身之间的间隔。用于将渗透气体排出到催化剂载体块1的外部的通风通道21,22与气体分离膜20相连。催化剂载体块1的温度通过设置加热装置3而升高，催化剂载体块1或其他功能的动作。由此，重整反应稳定，可以以比平衡转化率更高的转化率进行反应。该装置容易制造，并且当将重整器安装在所需位置时，该限制也很小。版权所有（C）2006，JPO＆NCIPI

10. 发明专利

JP2003299947A Hydrogenation apparatus and method using the same 审中-公开
标题翻译：氢化装置及其使用方法
公开(公告)号：JP2003299947A
公开(公告)日：2003-10-21
申请号：JP2002104612
申请日：2002-04-08
申请人： Japan Steel Works Ltd:The , 株式会社日本製鋼所
发明人： KOYANAGI KUNIHIKO , ICHIKAWA MASARU
IPC分类号： B01J19/24 , C07B61/00 , C07C5/10 , C07C13/18
摘要： PROBLEM TO BE SOLVED: To solve the problem that the fluidized state of a hydrogen gas and liquid benzene becomes non-uniform because a reaction pipe is non-uniformly filled with catalyst particles, in a perfusate type fixed bed reactor being one embodiment of a conventional hydrogeneration apparatus and reaction is not performed because the contact of the catalyst with a substrate is not performed at a certain part in the reaction pipe and, therefore, the utilization efficiency of a catalyst is low and, further, the optimum reaction temperature Topt required for achieving a high reaction speed is not prescribed especially.
SOLUTION: In this hydrogenation apparatus, the temperature of a monolithic catalyst is held to the optimum reaction temperature higher than the boiling point of a dehydrogenation reaction product, and the reaction product is uniformly supplied to the upper part of the monolithic catalyst from a despersion device in each of stages. A required amount of a hydrogen gas is uniformly supplied to the upper part of the monolithic catalyst of the first stage from a hydrogen gas supply part, and the supply volume ratio of the hydrogen gas and the reaction product is regulated in each stage to perform hydrogenation reaction.
COPYRIGHT: (C)2004,JPO
摘要翻译：解决的问题为了解决由于反应管不均匀填充有催化剂颗粒而导致氢气和液态苯的流化状态变得不均匀的问题，在作为一个实施方案的灌注型固定床反应器中的常规加氢发生装置，并且不进行反应，因为催化剂与基板的接触不在反应管的某一部分进行，因此催化剂的利用效率低，进一步优选的反应温度没有特别规定达到高反应速度所需的加压。解决方案：在该氢化装置中，将整体式催化剂的温度保持在高于脱氢反应产物的沸点的最佳反应温度，并将反应产物从均匀地供给到整体式催化剂的上部，在每个阶段中都是一种浸泡装置。从氢气供给部向氢化物的整体式催化剂的上部均匀地供给所需量的氢气，在各阶段调节氢气和反应生成物的供给体积比进行氢化反应。版权所有（C）2004，JPO

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