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71. 发明专利

JPS5725408A Production of cellulose acetate fiber 失效
标题翻译：乙酸纤维素纤维的生产
公开(公告)号：JPS5725408A
公开(公告)日：1982-02-10
申请号：JP10180880
申请日：1980-07-24
申请人： Mitsubishi Rayon Co Ltd
发明人： SHINKAI YUKIO , OOTANI TAKEJI , AOKI KUNIHIRO , KOBAYASHI TADAO
IPC分类号： D01F2/28
摘要： PURPOSE: When cellulose acetate fiber is produced by the wet method, the yarn, after spun and rinsed, is dried under no tension in the fiber-length direction, whereby the titled fiber with high tranparency and mechanical properties is produced.
CONSTITUTION: Cellulose acetate, preferably of more than 58% acetylation degree, is dissolved in, e.g., dimethylacetamide and treated in usual manners to form a spinning dope. The resultant dope is subjected to wet spinning using a dimethylacetamide aqueous solution as a coagulation both, preferably at a temperature lower than 30°C. The resultant yarn is washed, e.g., with boiling water, finishing oil is applied, the yarn is swung on the stainless steel net conveyor and dried in the hot air, preferably at 80W160°C under substantially no tension in the yarn-length direction.
COPYRIGHT: (C)1982,JPO&Japio
摘要翻译：目的：通过湿式制造醋酸纤维素时，纺丝和漂洗后的纱线在纤维长度方向上无张力干燥，由此产生具有高透明性和机械性能的标题纤维。构成：乙酸纤维素，优选超过58％的乙酰化程度，溶解在例如二甲基乙酰胺中，并以常规方式处理以形成纺丝原液。使用二甲基乙酰胺水溶液作为凝结物，将所得的涂料进行湿法纺丝，优选在低于30℃的温度下进行。所得到的纱线被洗涤，例如用沸水，涂上整理油，纱线在不锈钢网状输送机上摆动，在热空气中干燥，优选在80-160℃，基本上没有张力，长度方向。

72. 发明专利

JPS5685414A WET MOLDING METHOD FOR MOLDED CELLULOSE ACETATE ARTICLE 失效
公开(公告)号：JPS5685414A
公开(公告)日：1981-07-11
申请号：JP15998979
申请日：1979-12-10
申请人： MITSUBISHI RAYON CO
发明人： SHINKAI YUKIO , OOTANI TAKEJI , AOKI KUNIHIRO , KOBAYASHI TADAO
IPC分类号： D01F2/28 , C08J5/00
摘要： PURPOSE:To obtain a cellulose acetate fiber, etc. having improve transparency and strength, by wet molding a solution of a cellulose acetate of high combined acetic acid content in a coagulation bath kept at a specific temperature or below. CONSTITUTION:A cellulose acetate of combined acetic acid content 56% or more, preferably cellulose triacetate having a polymerization degree of 150-400, is dissolved in dimethylacetamide at a temperature of preferably 90-120 deg.C to give a uniform solution containing no microgel. The solution thus obtained is then filtered and deaerated to obtain a spinning solution of polymer concentration 15-25wt%. The resultant spinning solution is molded in a coagulation bath of aqueous dimethylacetamide kept at a temperature of 25 deg.C or below, preferably -10-5 deg.C by the wet or dry-jet wet method.

73. 发明专利

JPS5512869A PRODUCTION OF SUEDE LIKE SHEET ARTICLE 失效
公开(公告)号：JPS5512869A
公开(公告)日：1980-01-29
申请号：JP8494878
申请日：1978-07-12
申请人： MITSUBISHI RAYON CO
发明人： MIMURA KOUJI , FUSHIIE TAKASHI , AOKI KUNIHIRO
IPC分类号： D03D15/00 , D04H1/492

74. 发明专利

JPS5419919A NOVEL PHOSPHORIC ACID AMIDE* ITS PREPARATION* AND FLAMEERETARDANTS CONSISTING OF THE COMPOUND 失效
公开(公告)号：JPS5419919A
公开(公告)日：1979-02-15
申请号：JP8451977
申请日：1977-07-14
申请人： NITTO CHEMICAL INDUSTRY CO LTD , MITSUBISHI RAYON CO
发明人： AOKI KUNIHIRO , NAKAHAMA TETSUROU , MIMURA KOUJI
IPC分类号： C08K5/00 , C07F9/24 , C07F9/6509 , C07F9/6512 , C07F9/6574 , C08K5/51 , C08L1/00 , C08L1/12 , C08L67/00 , C08L67/02
摘要： PURPOSE:A phosphoric acid amide expressed by formula I: (R1 and R2 are aryl, halogenated aryl, 1 - 6C alkyl groups, etc., two R1's and two R2's may form alkylene groups respectively; R3 is arylene, halogenated arylene, or 1 - 6C alkylene group; R4 and R5 are H, 1 - 6C alkyl or aryl groups, and may form an alkylene group; halogen is Cl or Br; X is O or S; n is 0 or 1).

75. 发明专利

JPS5336597A PREPARATION OF FLAMEERETARDANT POLYPHOSPHORIC ACID AMIDE TYPE COMPOSITION 失效
公开(公告)号：JPS5336597A
公开(公告)日：1978-04-04
申请号：JP11099876
申请日：1976-09-16
申请人： NITTO CHEMICAL INDUSTRY CO LTD , MITSUBISHI RAYON CO
发明人： NAKAHAMA TETSUROU , MIMURA KOUJI , AOKI KUNIHIRO
IPC分类号： D01F6/60 , C08G79/00 , C08G79/02 , C08G79/04 , D01F6/90
摘要： PURPOSE:To prepare a flame-retardant polyphosphoric acid amide type composition imparting a long-acting flame-retardant effect to a regenerated cellulose fiber by reacting a phosphoric acid dihalide with a diamine compound.

76. 发明专利

JPH11315215A RESIN COMPOSITION CONTAINING COPPER COMPOUND, RESIN SHEET, AND FRONT PANEL FOR PDP 失效
公开(公告)号：JPH11315215A
公开(公告)日：1999-11-16
申请号：JP4212999
申请日：1999-02-19
申请人： MITSUBISHI RAYON CO
发明人： SAWANO TETSUYA , MARUTANI TAKAO , AOKI KUNIHIRO
IPC分类号： B32B27/28 , C08F2/44 , C08F230/02 , C08F246/00 , C08K3/00 , C08K5/521 , C08L33/06 , C08L101/06 , G02B5/22 , H01J11/44 , H01J17/16 , H01J11/02
摘要： PROBLEM TO BE SOLVED: To obtain a resin composition which can give a resin sheet nonproblematic in brittleness during cutting, excellent in durability under high- temperature high-humidity conditions or under hygroscopic condition, and excellent in the characteristic of absorbing near-infrared rays by mixing a copolymer comprising an unsaturated acid phosphoric ester and another polymerizable monomer with a saturated acid phosphoric ester and a copper compound. SOLUTION: This composition is obtained by reacting saturated and unsaturated acid phosphoric esters with copper hydroxide or a basic copper carbonate in a polymerizable monomer solution to form a copper complex and polymerizing and curing the polymerizable component in the solution. It is desirable to add 0.5-5 wt.% water. The unsaturated phosphoric ester is exemplified by an ester of formula I or II [wherein R and R are each a group of formula III or IV (wherein X and Y are each H or methyl; and m and n are each 1-6)] or a derivative thereof. It is desirable that the content of the copper compound is about 0.1-13 wt.% in terms of the copper atoms. It is desirable that the total content of the acid phosphoric esters is about 0.1-10 mol (in terms of the phosphorus atoms) per mol of the copper atoms.

77. 发明专利

JPH08235470A MULTIPLE CHANNEL MONITORING DEVICE 失效
公开(公告)号：JPH08235470A
公开(公告)日：1996-09-13
申请号：JP3412995
申请日：1995-02-22
申请人： MITSUBISHI RAYON CO
发明人： AOKI KUNIHIRO , YAMAMOTO NOBUYUKI , SUMI TOSHINORI , OKAMOTO MASAJI
IPC分类号： G02B6/04 , G02B27/02 , G08B21/00 , G08B21/08 , H04N7/18
摘要： PURPOSE: To perform centralized monitorings of plural places by a CCD and a monitor by a multiple channels monitoring device having two pairs of the units composed of the image transmitting body composed of an objective lens system and a multi-optical optical fiber or more and further having an eyepiece system, a CCD and a monitor. CONSTITUTION: The image formation at the end face of an image transmitting body 2 is performed for a part to be observed by an objective lens system 1, the formed image is propagated in the image transmitting body 2, the image formation at the end face of a CCD 4 is performed by an eyepiece system 3 at the other end, and the image is projected as an image on the screen of a monitor 5. The eyepiece system 3 and the CCD 4 are installed on a movable stage 6 and moves between each image transmitting body. Therefore, the centralized monitorings of plural places are possible by a CCD and a monitor, and because a multi-optical fiber is used as the image transmitting body, the monitorings of a narrow part and a portion to be easy to be a dead angle are also possible and the fiber is possible to be used in a magnetic field and in water.

78. 发明专利

JPH04227827A POROUS HOLLOW-FIBER MEMBRANE AND ITS PRODUCTION 失效
公开(公告)号：JPH04227827A
公开(公告)日：1992-08-17
申请号：JP14631788
申请日：1988-06-14
申请人： MITSUBISHI RAYON CO
发明人： AKITA TAKASHI , IWASAKI TADASHI , SUGIMORI MASAHIRO , AOKI KUNIHIRO
IPC分类号： B01D69/08 , B01D71/48 , C08J9/00 , C08L67/00 , D01D5/24 , D01F6/62 , D01F6/86 , D01F6/92
摘要： PURPOSE:To obtain a material for refining and separating liq. and gas having sufficient mechanical properties and heat resistance by melt-spinning a polyalkylene glycol-polyester block copolymer or the blend of the copolymer with a polyester, heat-treating the obtained hollow undrawn fiber at a specified temp. and drawing the treated fiber. CONSTITUTION:The polyalkylene glycol (polyethylene glycol)-polyester copolymer or the blend of the copolymer with a polyester contg. 1-25wt.% polyethylene glycol is melt-spun. The obtained hollow undrawn fiber having =1min at a temp. 2-50 deg.C lower than the m.p. of the composition, and then drawn by 20-400% at a temp. 120 deg.C higher than the primary dispersion loss maximum temp. The porous hollow-fiber membrane thus obtained has sufficient mechanical properties and heat resistance and is appropriately used as the material for refining and separating liq. and gas.

79. 发明专利

JPH04150932A FINE PORE SIZE STRAIGHT PORE MEMBRANE AND PREPARATION THEREOF 失效
公开(公告)号：JPH04150932A
公开(公告)日：1992-05-25
申请号：JP27241690
申请日：1990-10-12
申请人： MITSUBISHI RAYON CO
发明人： TAKEHATA KOJI , TAKAHASHI HIROSHI , AOKI KUNIHIRO
IPC分类号： B01D71/40
摘要： PURPOSE:To obtain a membrane having a good fractionating characteristic and excellent permeability by providing straight porous having a specific mean pore size to the surface of a porous membrane and setting the mean pore size and pressure loss at the time of the transmission of air so as to satisfy a specific formula. CONSTITUTION:At first, a composition containing a (meth)acrylic ester polymer and/or other component is dissolved in its good solvent to prepare a polymer solution which is, in turn, formed into membrane-like matter. Steam with absolute humidity of 1.0X10 -1.0X10 g/cm is brought into contact with the surface of this membrane like matter under such a condition that steam liner velocity is 12-50m/sec and a contact time of 0.1-10sec. Next, steam with absolute humidity of 1.0X10 -1.0-10 g/cm is brought into contact with the surface of the membrane like matter under such a condition that steam linear velocity is 0.1-9.0m/sec and a contact time is 10-600sec to perform two-stage steam contact treatment to obtain a membrane. This membrane has a mean fore size (d) of 1mum or less and the mean pore size (d) and pressure loss P generated when air is transmitted at linear velocity of 5.3cm/sec satisfy d X P

80. 发明专利

JPH03106889A FLUORINE-CONTAINING ORGANOSILICON COMPOUND 失效
公开(公告)号：JPH03106889A
公开(公告)日：1991-05-07
申请号：JP24228489
申请日：1989-09-20
申请人： MITSUBISHI RAYON CO
发明人： ONISHI HIROAKI , MATSUMOTO SHIRUYOSHI , AOKI KUNIHIRO
IPC分类号： C07F7/12 , C07F7/18
摘要： NEW MATERIAL:A compound expressed by formula I or formula II (R is 1-9C alkyl; X is halogen or alkoxyl; m is 0-4; n is 0-2). EXAMPLE:A compound expressed by formula III. USE:A raw material for synthesis of a functional polymer containing F and Si and silane coupling agent. PREPARATION:A fluorine-substituted styrene expressed by the formula CH2= CH-C6HmF5-m is subjected to hydrosilylation with a hydrosilane expressed by the formula RnX3-nSiH in the presence of a platinum based catalyst.

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