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    • 4. 发明公开
    • WELL PLATE
    • WANNENPLATTEFÜRRÖNTGENFLUORESZENZMESSUNGEN
    • EP2183644A1
    • 2010-05-12
    • EP08798006.6
    • 2008-08-15
    • Caldera Pharmaceuticals, Inc.
    • BIRNBAUM, Eva, R.WARNER, Benjamin, P.BALDWIN, Sharon, M.BERGER, Jennifer, A.MILLER, Rebecca, L.E.
    • G03B42/02G03C5/16
    • G01N23/2202G01N23/2204G01N23/223G01N2223/074G01N2223/076G01N2223/309G01N2223/64G03B42/02
    • The present invention includes an apparatus for preparing samples for measurement by x-ray fluorescence spectrometry The apparatus comprises a plate having one or more through holes which are less than 500 micrometers across in one dimension where a film covers the holes on one side of the plate The film is translucent to x-rays In another embodiment, the holes are covered on one side of the plate by a detachable cover forming a water-tight seal against the plate The cover is substantially free of the elements osmium, yttrium, Indium, phosphorus, zirconium, platinum, gold, niobium, mercury, thallium, molybdenum, sulfur, lead, bismuth, technetium, ruthenium, chlorine, rhodium, palladium, argon, silver, and thorium The present invention also comprises providing a solution of less than 10 micromolar and a volume between about 2 microliters and about 2 milliliters The solution is concentrated and analyzed using x-ray fluorescence spectrometry
    • 本发明包括通过X射线荧光光谱法制备用于测量的样品的装置。 该装置包括具有穿过板的一个或多个孔的板。 孔被板的一侧的薄膜覆盖。 在膜覆盖孔的一个维度上,孔小于500微米。 这部电影对于x射线是半透明的。 本发明还包括通过X射线荧光光谱法制备用于测量的样品的装置。 该装置包括具有穿过板的一个或多个孔的板。 孔通过可拆卸的盖子覆盖在板的一侧上,该盖子形成对板的防水密封。 盖子基本上不含锇,钇,铱,磷,锆,铂,金,铌,汞,铊,钼,硫,铅,铋,锝,钌,氯,铑,钯,氩, 和钍。 这些孔在一个尺寸上小于约500微米,其中盖覆盖孔。 本发明还包括通过X射线荧光光谱法制备用于测量的样品的方法。 该方法包括提供小于10微摩尔溶质的溶液和约2微升至约2毫升的体积。 使用x射线荧光光谱法浓缩溶液并进行分析。
    • 10. 发明公开
    • ANORDNUNG UND VERFAHREN ZUR HERSTELLUNG VON ANALYSEPROBEN
    • EP2901131A1
    • 2015-08-05
    • EP13762825.1
    • 2013-09-16
    • Fluxana GmbH & Co. Kg
    • SCHRAMM, Rainer
    • G01N1/44
    • G01N1/44F27B14/02F27B14/08F27B17/02F27D2005/0075G01N1/38G01N23/2202G01N23/2204
    • The invention relates to an arrangement for producing analysis samples for X-ray fluorescence analysis, with a crucible arranged in a furnace and receiving sample material to be melted, a crucible mount arranged in the furnace, and a collection dish, dimensioned for receiving the sample material present in the crucible, arranged underneath the crucible. The crucible is arranged in the furnace so as to be movable for mixing, in such a manner that the sample material present in the crucible can be intimately mixed by means of crucible movements. The crucible is arranged in the furnace so as to be movable for tilting, in such a manner that the collection dish can be filled with the sample material present in the crucible by means of the tilting movement of the crucible. According to the invention, the mounting is placed movably in the furnace. A mount suitable for such an arrangement is characterized in that the mount has a tilt bearing receiving the crucible. A crucible suitable for such an arrangement is characterized in that the crucible has two opposing protrusions, which form a tilting axis for the crucible. A furnace suitable for such an arrangement is characterized in that the furnace has a base on which the mount is positioned upright, and that the region of the base receiving the mount is designed as a turntable which is rotationally movable in an oscillating manner. The invention further relates to a procedure which is characterized in that the crucible and the mount are located outside the furnace prior to the beginning of the melting process, and that the mount is loaded with the crucible outside the furnace prior to the beginning of the melting process and is placed in the furnace together with the crucible.
    • 用于生产用于X射线荧光光谱的分析样品的装置,其包括用样品材料支撑坩埚的坩埚保持器和设置在坩埚下方的铸造皿。 坩埚可倾斜地安装在坩埚保持器中,并且坩埚保持器与坩埚保持器一起被安装,并且铸造盘作为用于装载和卸载烤箱的单个单元来处理。 烤箱具有坩埚保持器直立定位的地板,并且接收坩埚保持器的地板的部分被设计为向坩埚托架和坩埚托架施加摆动旋转运动的转台。 该方法需要将具有样品材料的坩埚放置在坩埚保持器中,同时它们在炉外,然后将整个坩埚单元松散地放置在烘箱中。