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    • 1. 发明公开
    • Process and apparatus for producing polycrystalline semiconductor ingot
    • Verfahren und Vorrichtung zur Herstellung polykristalliner Halbleiter-blöcke
    • EP0887442A1
    • 1998-12-30
    • EP98111342.6
    • 1998-06-19
    • SHARP KABUSHIKI KAISHA
    • Yamazaki, MotoharuOkuno, Tetsuhiro
    • C30B11/00C30B29/06
    • C30B29/06C30B11/002
    • A silicon semiconductor material (15) is charged in a double-structured crucible of an outer crucible (1) and an inner crucible (2). The crucible is heated from the upper side thereof by the heat radiated from a heating member (8) energized by an induction heating coil (7), so that the silicon raw semiconductor material is melted. The bottom of the crucible (1) is mounted on a supporting bed (4) cooled by cooling water supplied from a cooling medium tank (13). The silicon semiconductor material (15) is melted in the inner crucible (2) and starts solidifying from the bottom portion thereof. The silicon semiconductor material (15) expands in volume at the time of solidification. Since a gap is formed between the inner crucible (2) and the outer crucible (1), however, the outward extension of the inner crucible (1) with the silicon semiconductor material (15) alleviates a strain generated at the time of solidification, thereby producing an excellent polycrystalline semiconductor ingot. As a result, the strain in the polycrystalline semiconductor ingot produced by the unidirectional solidification process is reduced to improve the quality.
    • 将硅半导体材料(15)装入外坩埚(1)和内坩埚(2)的双结构坩埚中。 通过从由感应加热线圈(7)激励的加热部件(8)辐射的热量从其上侧加热坩埚,使得硅原料半导体材料熔化。 坩埚(1)的底部安装在由冷却介质罐(13)供应的冷却水冷却的支撑床(4)上。 硅半导体材料(15)在内坩埚(2)中熔化,并从其底部开始凝固。 在固化时,硅半导体材料(15)的体积膨胀。 然而,由于内坩埚(2)和外坩埚(1)之间形成间隙,所以内部坩埚(1)与硅半导体材料(15)的向外延伸减轻了凝固时产生的应变, 从而生产出优异的多晶半导体锭。 结果,通过单向凝固工艺生产的多晶半导体锭中的应变被降低以提高质量。
    • 8. 发明公开
    • Process and apparatus for producing polycrystalline semiconductor
    • 生产多晶半导体的工艺和设备
    • EP0889148A1
    • 1999-01-07
    • EP98111872.2
    • 1998-06-26
    • SHARP KABUSHIKI KAISHA
    • Okuno, Tetsuhiro
    • C30B11/00C30B29/06
    • C30B29/06C30B11/003Y10T83/448Y10T83/4493
    • A process and apparatus for producing a high-quality polycrystalline semiconductor ingot with excellent crystallographic properties are disclosed. The interior of an airtight vessel (1) is kept in an inert atmosphere for semiconductors. A raw semiconductor material (17) is charged in a crucible (9), and the raw semiconductor material (17) is heated by an induction heating coil (5) so as to be melted. Then the bottom of the crucible is deprived of heat for causing the raw semiconductor material (17) to solidify, thereby producing a polycrystalline semiconductor. The semiconductor crystal grows in one direction from the bottom to the top of the crucible while the heat emission is changed in accordance with a predetermined relationship for keeping the solidification rate of the raw semiconductor material (17) constant.
    • 公开了用于制造具有优异晶体学性质的高质量多晶半导体晶锭的方法和设备。 密封容器(1)的内部保持在半导体的惰性气氛中。 将原料半导体材料(17)装入坩埚(9)中,并通过感应加热线圈(5)加热原料半导体材料(17)以使其熔化。 然后,坩埚的底部被剥夺热量,以使原料半导体材料(17)凝固,由此产生多晶半导体。 半导体晶体从坩埚的底部到顶部在一个方向上生长,同时根据预定关系改变放热量,以保持半导体材料(17)的凝固速度恒定。
    • 10. 发明公开
    • Process and apparatus for producing polycrystalline semiconductors
    • Verfahren und Vorrichtung zur Herstellung polykristalliner Halbleiter
    • EP0748884A1
    • 1996-12-18
    • EP96109528.8
    • 1996-06-13
    • SHARP KABUSHIKI KAISHA
    • Okuno, Tetsuhiro
    • C30B11/00
    • C30B29/06C30B11/002C30B11/003
    • For the highly repeatable growth of high-quality semiconductor polycrystals with excellent crystallographic properties, at a low cost, there are provided a process for producing a polycrystalline semiconductor including charging a raw semiconductor material into a crucible (9) with semiconductor seed crystals placed on its bottom in an atmosphere inert to the semiconductor, heating to melt the raw semiconductor material in the crucible (9) by heating means (5) while depriving the bottom of the crucible (9) of heat to maintain the underside temperature T1 of the bottom below the melting point of the raw semiconductor material, and then cooling the crucible (9) to solidify the melted material, wherein the underside temperature T1 of the bottom of the crucible under heating is measured, and the heating by the heating means (5) is suspended when the rate Δt of time-dependent change of the temperature increases over a predetermined value, to thereby melt only the raw semiconductor material, substantially without melting the seed crystals, and the melted raw material is then solidified to grow a polycrystal from the seed crystals, as well as a manufacturing apparatus therefor.
    • 对于具有优异的晶体学特性的高质量半导体多晶体的高度可重复的生长,以低成本提供了一种制造多晶半导体的方法,其包括将原料半导体材料装入坩埚(9)中,半导体晶种放置在其上 底部处于对半导体惰性的气氛中,加热以通过加热装置(5)熔化坩埚(9)中的原料半导体材料,同时剥离坩埚(9)的底部加热,以将底部的下侧温度T1保持在下方 原料半导体材料的熔点,然后冷却坩埚(9)以固化熔融材料,其中测量加热坩埚底部的下侧温度T1,并且加热装置(5)的加热为 当温度的时间依赖性变化的速率DELTA t超过预定值时暂停,从而仅熔化原料半导体配合物 实质上不熔化晶种,然后将熔融的原料固化,从晶种生长多晶,以及其制造装置。