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    • 1. 发明公开
    • METHOD AND SYSTEM FOR PRODUCING A MICRONUTRIENT FERTILIZER
    • EP4335835A1
    • 2024-03-13
    • EP23461648.0
    • 2023-09-07
    • Politechnika WroclawskaEkoplon spolka z ograniczona odpowiedzialnosci sp.k.
    • Chojnacka, KatarzynaWitek-Krowiak, AnnaSkrzypczak, DawidMikula, KatarzynaIzydorczyk, Grzegorz
    • C05D9/02C05F5/00
    • The invention relates to a method for producing a micronutrient fertiliser, whereby biomass selected from a group consisting of currant seeds, press cakes, rapeseed meal, soybean meal or waste after supercritical CO 2 extraction of alfalfa and goldenrod, and combinations thereof, is intensively sprayed with an aerosol of a solution of sulphate salts of trace elements, containing Cu(II) ions at a concentration of 500 to 30,000 mg/L, Mn(II) at a concentration of 500 to 30,000 mg/L and Zn(II) at a concentration of 500 to 30,000 mg/L, with a pH in the range from 3.0 to 6.0, preferably generated at a pressure of 0.5 to 5 bar. The biomass is possibly enriched in Fe(II) ions, by spraying with an aerosol of a solution of iron sulphate salt, containing Fe(II) ions at a concentration of 500 to 30,000 mg/L.
      The subject of the invention is also a system for producing the micronutrient fertiliser, which is equipped with devices for dosing and feeding of biosorption substrates, cooperating with an aerosol generating module. Wherein the module for dosing and feeding of the micronutrient solution comprises a tank ( RZ ), connected to the module generating aerosol from the micronutrient solution, pumped using a pump ( RW ), and a module for dosing and feeding of the biomass comprises a weigher ( BW ), from which the biomass is introduced to a ribbon conveyor ( BP ), above which spraying nozzles ( BD ) are located, to which the micronutrient solution is fed simultaneously with compressed air pumped in a spray module from a compressor ( NS ).
      In a variant of the invention, the system for producing micronutrient fertilizer comprises a fluidized bed column to which the module for dosing and feeding of the micronutrient solution and the aerosol generating module are connected. Wherein the column is provided with an opening for biomass loading and a biomass fluidization assembly, which is equipped with a fan, connected to a heater, from which air is introduced into the fluidized bed column. The module for dosing and feeding of the micronutrient solution comprises a tank from which the micronutrient solution is supplied to a spray nozzle located in the fluidized bed column, the aerosol generating module comprises a compressor from which compressed air is pumped to the spray nozzle located in the fluidized bed column.
    • 2. 发明公开
    • Combined directional electron detector
    • 组合的定向电子探测器
    • EP2672504A2
    • 2013-12-11
    • EP13460034.5
    • 2013-05-27
    • POLITECHNIKA WROCLAWSKA
    • Slówko, Witold
    • H01J37/244
    • H01J37/20H01J37/244H01J37/28H01J2237/2003H01J2237/24465H01J2237/2608
    • The combined directional electron detector, intended particularly for environmental scanning electron microscopes with variable gas pressure in the sample chamber, also dedicated to the multidetector three-dimensional imaging of surface topographies, has an intermediate chamber (16) situated on the path of the electron beam (EB) to the sample stage (2), filled with gas with an intermediate pressure (P 2 ) lower than the working gas pressure (P 1 ) in the sample chamber where the place of emission of the electrons subject to detection is located, is equipped with a lower aperture (1) throttling the flow of the gas to the intermediate chamber (16) and in the space between the intermediate chamber (16) and the sample stage (2) it has four anodes (3) in the form of four electrodes identical in shape, arranged in pairs symmetrically around the electron beam (EB) axis, equipped with separate electrical leads and positively biased relative to the wall of the intermediate chamber (16). In the space between the anodes (3) and the sample stage (2) there is an external screening cathode (6) with a hole, delimiting from the sample stage (2) side the maximal backscattered electron (BSE 2 ) detection angle (β 2 ) at which the electrons enter the electric discharge area around the anodes (3). Inside the intermediate chamber (16) there is a quadrant semiconductor BSE 1 detector (13) with four identical sectors active for electrons, arranged symmetrically relative to the electron beam (EB) axis, with their active surfaces facing the lower throttling aperture (1).
    • 10. 发明公开
    • Combined directional electron detector
    • 电影制作人Elektronendetektor
    • EP2672504A3
    • 2015-04-15
    • EP13460034.5
    • 2013-05-27
    • POLITECHNIKA WROCLAWSKA
    • Slówko, Witold
    • H01J37/244H01J37/20H01J37/28
    • H01J37/20H01J37/244H01J37/28H01J2237/2003H01J2237/24465H01J2237/2608
    • The combined directional electron detector, intended particularly for environmental scanning electron microscopes with variable gas pressure in the sample chamber, also dedicated to the multidetector three-dimensional imaging of surface topographies, has an intermediate chamber (16) situated on the path of the electron beam (EB) to the sample stage (2), filled with gas with an intermediate pressure (P 2 ) lower than the working gas pressure (P 1 ) in the sample chamber where the place of emission of the electrons subject to detection is located, is equipped with a lower aperture (1) throttling the flow of the gas to the intermediate chamber (16) and in the space between the intermediate chamber (16) and the sample stage (2) it has four anodes (3) in the form of four electrodes identical in shape, arranged in pairs symmetrically around the electron beam (EB) axis, equipped with separate electrical leads and positively biased relative to the wall of the intermediate chamber (16). In the space between the anodes (3) and the sample stage (2) there is an external screening cathode (6) with a hole, delimiting from the sample stage (2) side the maximal backscattered electron (BSE 2 ) detection angle (β 2 ) at which the electrons enter the electric discharge area around the anodes (3). Inside the intermediate chamber (16) there is a quadrant semiconductor BSE 1 detector (13) with four identical sectors active for electrons, arranged symmetrically relative to the electron beam (EB) axis, with their active surfaces facing the lower throttling aperture (1).
    • 专门用于样品室中具有可变气体压力的环境扫描电子显微镜的组合定向电子检测器也专用于表面形貌的多检测器三维成像,具有位于电子束路径上的中间室(16) (EB)到样品台(2),填充有中间压力(P 2)低于被检测电子发射位置的样品室中的工作气体压力(P 1)的气体, 配备有将气体流动到中间室(16)并在中间室(16)和样品台(2)之间的空间中的下孔(1),其具有四个阳极(3),形式为 四个电极形状相同,以电子束(EB)轴对对称地配置,配备有单独的电引线并相对于中间室(16)的壁被正偏置。 在阳极(3)和样品台(2)之间的空间中,存在具有孔的外部屏蔽阴极(6),其从样品台(2)侧限定最大背散射电子(BSE 2)检测角度(² 2),电子进入阳极周围的放电区域(3)。 在中间室(16)的内部有一个象限半导体BSE 1检测器(13),其四个相同的扇区对电子有活动,相对于电子束(EB)轴对称布置,其有效表面面向下节流孔(1) 。