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1. 发明授权

US4593132A Process for producing a graphite fluoride 失效
标题翻译：石墨氟化物的制造方法
公开(公告)号：US4593132A
公开(公告)日：1986-06-03
申请号：US659049
申请日：1984-12-10
申请人： Yasushi Kita , Hishaji Nakano , Shiro Moroi , Akira Sakanoue
发明人： Yasushi Kita , Hishaji Nakano , Shiro Moroi , Akira Sakanoue
IPC分类号： C01B31/04 , C01B31/00 , D01F11/12 , C07C17/00
CPC分类号： D01F11/129 , C01B31/005
摘要： A graphite fluoride can be produced safely and in high yield on a commercial production scale by a process comprising reacting a carbon material having an average size of 100.mu. to 10 mm with fluorine. Further, when the fluorination reaction is stopped before completion thereof and the graphite fluoride product is subjected to sifting with a sieve to separate a desired graphite fluoride from the raw carbon material remaining unreacted.
摘要翻译：可以通过包括使平均粒度为100〜10mm的碳材料与氟反应的方法以商业生产规模安全地和高收率地生产氟化石墨。此外，当氟化反应在其完成之前停止并且氟化石墨产物用筛子进行筛分以从未还原的原料碳分离所需的氟化石墨。

2. 发明授权

US4590316A Method of safely preparing graphite fluoride 失效
标题翻译：安全地制备氟化石墨的方法
公开(公告)号：US4590316A
公开(公告)日：1986-05-20
申请号：US650986
申请日：1984-09-14
申请人： Yasushi Kita , Hisaji Nakano , Shiro Moroi , Akira Sakanoue
发明人： Yasushi Kita , Hisaji Nakano , Shiro Moroi , Akira Sakanoue
IPC分类号： C01B31/00 , C01B31/04 , C07C17/00
CPC分类号： C01B31/005
摘要： A method of preparing graphite fluoride such as (CF).sub.n or (C.sub.2 F).sub.n by heterogeneous contact reaction between a carbon material such as graphite or petroleum coke and fluorine gas at about 200.degree.-550.degree. C. In the gas phase of the reaction system, the total concentration of higher fluorocarbons having more than four carbon atoms formed by side reactions is controlled so as not to become above 3% by volume by, for example, condensation or catalytic decomposition of at least a portion of the higher fluorocarbons in the gas flowed out of the reaction chamber for recirculation. Such control is highly effective for prevention of rapid and violent decomposition of the graphite fluoride existing in the solid phase of the reaction system induced by sudden decomposition of the higher fluorocarbons in the reaction system to lower fluorocarbons.
摘要翻译：一种在约200〜-550℃之间的碳材料如石墨或石油焦炭与氟气之间的非均相接触反应制备（CF）n或（C 2 F）n的氟化石墨的方法。在反应的气相通过副反应形成的具有多于四个碳原子的高级碳氟化合物的总浓度被控制为通过例如至少一部分较高碳氟化合物的冷凝或催化分解而不会变成高于3体积％气体从反应室流出，用于再循环。这种控制对于防止由反应体系中的较高碳氟化合物突然分解成低碳氟化合物引起的反应体系固相中存在的氟化石墨的快速和剧烈分解是非常有效的。

3. 发明授权

US5147435A Method for suppressing crystallization of fluoride glass articles by treatment with inorganic fluoride 失效
标题翻译：通过无机氟化物处理抑制氟化物玻璃的结晶的方法
公开(公告)号：US5147435A
公开(公告)日：1992-09-15
申请号：US698896
申请日：1991-05-13
申请人： Yoshinori Kubota , Akira Sakanoue , Yasushi Kita
发明人： Yoshinori Kubota , Akira Sakanoue , Yasushi Kita
IPC分类号： C03B37/012 , C03C17/22 , C03C17/28 , C03C23/00
CPC分类号： C03C17/22 , C03C2217/285 , C03C2218/11 , Y10S65/16
摘要： Crystallization of a fluoride glass article is suppressed by treating the surface(s) of the fluoride glass article with a solution of a fluorine-containing alkali metal compound or a fluorine-containing ammonium compound such as, e.g., LiPF.sub.6, NaBF.sub.4 or NH.sub.4 BF.sub.4, in a nonaqueous solvent such as, e.g., ethanol, N,N-dimethylformamide or acetonitrile. The treatment can be made at room temperature.
摘要翻译：通过用含氟碱金属化合物或含氟铵化合物（例如LiPF 6，NaBF 4或NH 4 BF 4）的溶液处理氟化物玻璃制品的表面来抑制氟化物玻璃制品的结晶，非水溶剂，例如乙醇，N，N-二甲基甲酰胺或乙腈。处理可在室温下进行。

4. 发明授权

US4500678A Lubricant comprising a partially defluorinated graphite fluoride 失效
标题翻译：润滑剂包括部分脱氟的氟化石墨
公开(公告)号：US4500678A
公开(公告)日：1985-02-19
申请号：US514792
申请日：1983-07-18
申请人： Yasushi Kita , Shirou Moroi , Akira Sakanoue , Hisaji Nakano
发明人： Yasushi Kita , Shirou Moroi , Akira Sakanoue , Hisaji Nakano
IPC分类号： H01M4/583 , C01B31/00 , C01B31/04 , C10M103/02 , C10M111/04 , C10M125/02 , C10N50/08 , C10N70/00 , C10M7/04 , C10M1/10
CPC分类号： C10M111/04 , C01B31/005 , C10M103/02 , C10M125/02 , C10M2201/00 , C10M2201/041 , C10M2201/0413 , C10M2201/042 , C10M2201/0423 , C10M2201/061 , C10M2201/16 , C10M2201/18 , C10M2205/003 , C10M2205/022 , C10M2205/14 , C10M2209/084 , C10M2209/101 , C10M2211/06 , C10M2211/08 , C10M2213/02 , C10M2213/062 , C10M2217/044 , C10M2217/045 , C10N2250/10
摘要： A lubricant comprising a partially defluorinated graphite fluoride obtained by exposing a dispersion of raw material graphite fluoride to electromagnetic radiation, followed by the separation of the resulting partially degraded graphite fluoride. The partially defluorinated graphite fluoride is not only excellent in lubricating properties but also has excellent compatibilities with resins, greases and oils. The excellent compatibilities of the partially defluorinated graphite fluoride are effective in preventing the unfavorable deposition of the graphite fluoride in a liquid lubricant composition and advantageously lead to improvement in the moldability of any graphite fluoride-resin composition, thereby enabling the ultimate composition to exhibit excellent lubricating properties.
摘要翻译：一种润滑剂，其包含通过将原料石墨氟化物的分散体暴露于电磁辐射而获得的部分脱氟氟化石墨氟化物，然后分离所得部分降解的氟化石墨。部分脱氟石墨氟化物不仅具有优异的润滑性能，而且与树脂，油脂和油具有优异的相容性。部分氟化氟化石墨氟化物的优异相容性对于防止氟化石墨在液体润滑剂组合物中的不利沉积是有效的，并且有利地改善了任何氟化石墨树脂组合物的成型性，从而使最终组合物显示出优异的润滑性属性。

5. 发明授权

US5338607A 1.3 micrometer-band amplifying optical fiber preform 失效
标题翻译： 1.3微米带放大光纤预制棒
公开(公告)号：US5338607A
公开(公告)日：1994-08-16
申请号：US6340
申请日：1993-01-19
申请人： Hiromi Kawamoto , Yoshinori Kubota , Natsuya Nishimura , Akira Sakanoue
发明人： Hiromi Kawamoto , Yoshinori Kubota , Natsuya Nishimura , Akira Sakanoue
IPC分类号： C03B37/012 , C03B37/014 , C03C3/247 , C03C3/32 , C03C13/04 , G02B6/00 , G02F1/35 , H01S3/17 , B32B17/02
CPC分类号： C03C13/042 , C03C13/04 , C03B2201/50 , C03B2201/54 , C03B2201/82 , Y10T428/2929 , Y10T428/2938 , Y10T428/294 , Y10T428/2942 , Y10T428/2949 , Y10T428/2964
摘要： An optical fiber preform includes a core made from a fluoride glass which is doped with a rare earth, and a cladding surrounding the core. The cladding is made from one of an oxide glass and a fluoroxide glass. The core has a characteristic of amplification at 1.3 .mu.m-band. The cladding does not have absorption at 1.3 .mu.m-band. The preform is useful as a material for a fiber optical amplifier in optical communication systems.
摘要翻译：光纤预制件包括由掺杂有稀土的氟化物玻璃制成的芯和围绕芯的包层。包层由氧化物玻璃和氟氧化物玻璃之一制成。核心具有1.3微米波段的放大特性。包层在1.3微米带没有吸收。预成型件可用作光通信系统中的光纤放大器的材料。

6. 发明授权

US4508761A Method of preparing polymer-coated particulate inorganic material 失效
标题翻译：制备聚合物涂覆颗粒无机材料的方法
公开(公告)号：US4508761A
公开(公告)日：1985-04-02
申请号：US467839
申请日：1983-02-18
申请人： Takao Miyoshi , Akira Sakanoue
发明人： Takao Miyoshi , Akira Sakanoue
IPC分类号： C08K9/04 , B29C33/00 , C08F292/00 , C08J3/20 , C09C1/44 , C09C1/46 , C09C3/10 , C10M103/02 , C10M123/02 , C10M125/02 , C10N20/06 , B05D7/00 , B29J5/00
CPC分类号： C10M103/02 , C08F292/00 , C10M123/02 , C10M125/02 , C10M2201/041 , C10M2201/042 , C10M2209/04 , C10M2209/06 , C10M2209/062 , C10M2209/084 , C10M2211/06 , C10M2213/02 , C10M2213/062 , C10M2217/024 , C10M2217/026 , C10M2217/06 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/402 , C10N2240/403 , C10N2240/404 , C10N2240/405 , C10N2240/406 , C10N2240/407 , C10N2240/408 , C10N2240/409 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： A polymer-coated particulate inorganic material, e.g. graphite, graphite fluoride or molybdenum disulfide, is obtained by preparing a reaction system containing a liquid medium, fine particles of the inorganic material, at least one vinylic monomer which undergoes radical polymerization or copolymerization and a polymerization initiator and allowing the vinylic monomer(s) in the reaction system to undergo polymerization and to bond to the surfaces of the inorganic material particles by graft polymerization. To enhance the efficiency of graft polymerization to thereby realize uniform coating even when the inorganic material is very low in surface energy as typified by graphite fluoride, the pH of the reaction system is adjusted to a value ranging from 5 to 9 by adding alkali to the reaction system soon after the addition of the polymerization initiator or alternatively by treating the inorganic material with alkali in advance of preparation of the reaction system. The polymer-coated inorganic material can easily be shaped into a solid body by compacting, optionally with addition of a synthetic resin.
摘要翻译：聚合物涂覆的颗粒无机材料，例如通过制备含有液体介质的反应体系，无机材料的细颗粒，至少一种进行自由基聚合或共聚的乙烯基单体和聚合引发剂并使乙烯基单体进行反应，得到石墨，氟化石墨或二硫化钼，在反应体系中进行聚合，并通过接枝聚合与无机材料颗粒的表面结合。为了提高接枝聚合的效率，从而即使当无机材料以氟化石墨为代表的非常低的表面能时也能实现均匀涂布，反应体系的pH值通过向反应体系在加入聚合引发剂后不久，或者在制备反应体系之前用碱处理无机材料。聚合物涂覆的无机材料可以容易地通过压实成型为固体，任选地加入合成树脂。

7. 发明授权

US5308371A Method of forming fluoride glass fiber preform 失效
标题翻译：形成氟化玻璃纤维预制棒的方法
公开(公告)号：US5308371A
公开(公告)日：1994-05-03
申请号：US047522
申请日：1993-04-19
申请人： Hiromi Kawamoto , Yoshinori Kubota , Natsuya Nishimura , Akira Sakanoue
发明人： Hiromi Kawamoto , Yoshinori Kubota , Natsuya Nishimura , Akira Sakanoue
IPC分类号： C03B17/00 , C03B37/012 , C03B37/014 , C03C3/32 , G02B6/00 , C03B37/023
CPC分类号： C03B37/01274 , C03B37/01268 , C03B2201/82
摘要： A method of forming a fiber glass preform includes the steps of: (a) pouring a cladding glass into a mold; (b) pouring a core glass on a flat horizontal upper surface of the cladding glass so as to form a united glass body having the core glass and the cladding glass under a condition that viscosity of the cladding glass and viscosity of the core glass are adjusted to certain predetermined values respectively so that the core glass is separated from and placed on the cladding glass; (c) cooling the united glass body to solidify the same so that the cladding glass is deformed by contraction thereof so as to produce a depression at a top middle portion thereof and that the core glass is deformed so as to form a projected portion thereof to fill the depression therewith; (d) separating the united glass body into an upper portion and a lower portion comprising the projected portion of the core glass; and (e) extruding the lower portion of the united glass body so as to form the fiber glass preform.
摘要翻译：形成玻璃纤维预制棒的方法包括以下步骤：（a）将包层玻璃倒入模具中; （b）在包层玻璃的平坦的水平上表面上浇注芯玻璃，以在包层玻璃的粘度和芯玻璃的粘度被调节的条件下形成具有芯玻璃和包层玻璃的联合玻璃体分别达到某些预定值，使得芯玻璃与包层玻璃分离并放置在包层玻璃上; （c）冷却联合玻璃体以使其固化，使得包层玻璃通过收缩而变形，从而在其顶部中间部分产生凹陷，并且芯玻璃变形以形成其突出部分填充凹陷; （d）将玻璃体分离成包括芯玻璃的突出部分的上部和下部; 和（e）挤出组合玻璃体的下部以便形成玻璃纤维预制件。

8. 发明授权

US4557974A Graphite fluoride coated with organic polymer and method of preparing same 失效
标题翻译：用有机聚合物涂覆的石墨氟化物及其制备方法
公开(公告)号：US4557974A
公开(公告)日：1985-12-10
申请号：US434902
申请日：1982-10-18
申请人： Hitoshi Tsukuda , Akira Sakanoue
发明人： Hitoshi Tsukuda , Akira Sakanoue
IPC分类号： C08F2/44 , C08F292/00 , C10M103/02 , C10M123/02 , C10M125/02 , C08K3/04
CPC分类号： C08F292/00 , C10M103/02 , C10M123/02 , C10M125/02 , C10M2201/041 , C10M2201/042 , C10M2209/04 , C10M2209/06 , C10M2209/062 , C10M2209/084 , C10M2211/06 , C10M2213/02 , C10M2213/062 , C10M2217/024 , C10M2217/026 , C10M2217/06 , C10N2240/00 , C10N2240/22 , C10N2240/30 , C10N2240/40 , C10N2240/402 , C10N2240/403 , C10N2240/404 , C10N2240/405 , C10N2240/406 , C10N2240/407 , C10N2240/408 , C10N2240/409 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66 , Y10T428/2991 , Y10T428/2998
摘要： Graphite fluoride, such as (CF).sub.n or (C.sub.2 F).sub.n, in powder form coated with a vinylic polymer, e.g. polymethyl methacrylate, which is bonding to the surfaces of the graphite fluoride particles by graft polymerization. The polymer-coated graphite fluoride retains unique properties of graphite fluoride such as high lubricating ability, can readily be dispersed in water and organic liquids, and can readily be press-shaped with or without the addition of a synthetic resin powder. The polymer-coated graphite fluoride is prepared by dispersing graphite fluoride in powder form and at least one vinylic monomer which undergoes radical polymerization in a mixture of water and either a water-soluble organic solvent or a surface-active agent, and then adding a polymerization initiator to the aqueous dispersion. The polymerization reaction takes place even at room temperature and can be promoted by heating up to 70.degree. C.
摘要翻译：石墨氟化物，例如（CF）n或（C2F）n），其以粉末形式涂覆有乙烯基聚合物，例如聚甲基丙烯酸甲酯，其通过接枝聚合与氟化石墨粉末的表面结合。聚合物涂覆的氟化石墨氟化物具有石墨氟化物的独特性能，如高润滑性，可以容易地分散在水和有机液体中，并且可以在加入或不加入合成树脂粉末的情况下容易地成型。聚合物涂覆的氟化石墨是通过以粉末形式分散氟化石墨和至少一种在水和水溶性有机溶剂或表面活性剂的混合物中进行自由基聚合的乙烯基单体制备的，然后加入聚合引发剂到水分散体。即使在室温下也发生聚合反应，可以通过加热至70℃来促进聚合反应。

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