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    • 1. 发明申请
    • ATOM PROBE COMPONENT TREATMENTS
    • 原子探针组分处理
    • US20090138995A1
    • 2009-05-28
    • US11917672
    • 2006-06-16
    • Thomas F. KellyDavid J. LarsonRichard L. MartensKeith J. ThompsonRobert M. UlfigScott A. Wiener
    • Thomas F. KellyDavid J. LarsonRichard L. MartensKeith J. ThompsonRobert M. UlfigScott A. Wiener
    • G12B21/00
    • H01J37/3056H01J37/32853H01J37/32862
    • The present invention relates to treatments for atom probe components. For example, certain aspects are directed toward processes for treating an atom probe component that includes removing material from a surface of the atom probe component (e.g., using an ion beam, a plasma, a chemical etching process, and/or photonic energy). Another aspect of the invention is directed toward a method for treating an atom probe specimen that includes using a computing device to automatically control a voltage used in an ion sputtering process. Still other aspects of the invention are directed toward methods for treating an atom probe component that includes introducing photonic energy proximate to a surface of the atom probe component, annealing at least a portion of a surface of the atom probe component, coating at least a portion of a surface of the atom probe component, and/or cooling at least a portion of the atom probe component.
    • 本发明涉及原子探针成分的处理。 例如,某些方面涉及用于处理原子探针组分的方法,其包括从原子探针组分的表面除去材料(例如,使用离子束,等离子体,化学蚀刻工艺和/或光能)。 本发明的另一方面涉及一种用于处理原子探针样品的方法,其包括使用计算装置自动控制在离子溅射工艺中使用的电压。 本发明的其它方面涉及用于处理原子探针组分的方法,所述方法包括将光子能引入到原子探针组分的表面附近,退火至少部分原子探针组分的表面,涂覆至少一部分 的原子探针组分的表面,和/或冷却原子探针组分的至少一部分。
    • 6. 发明授权
    • Atom probes, atom probe specimens, and associated methods
    • 原子探针,原子探针标本和相关方法
    • US07884323B2
    • 2011-02-08
    • US12064020
    • 2006-08-15
    • Thomas F. KellyJoseph H. BuntonScott A. Wiener
    • Thomas F. KellyJoseph H. BuntonScott A. Wiener
    • G01N23/00
    • G01N23/22
    • The present invention relates generally to atom probes, atom probe specimens, and associated methods. For example, certain aspects are directed toward methods for analyzing a portion of a specimen that includes selecting a region of interest and moving a portion of material in a border region proximate to the region of interest so that at least a portion of the region of interest protrudes relative to at least a portion of the border region. The method further includes analyzing a portion of the region of interest. Other aspects of the invention are directed toward a method for applying photonic energy in an atom probe process by passing photonic energy through a lens system separated from a photonic device and spaced apart from the photonic device. Yet other aspects of the invention are directed toward a method for reflecting photonic energy off an outer surface of an electrode onto a specimen.
    • 本发明一般涉及原子探针,原子探针试样和相关方法。 例如,某些方面涉及用于分析样本的一部分的方法,所述方法包括选择感兴趣区域并移动靠近感兴趣区域的边界区域中的材料的一部分,使得感兴趣区域的至少一部分 相对于边界区域的至少一部分突出。 该方法还包括分析感兴趣区域的一部分。 本发明的其它方面涉及通过使光子能量通过从光子器件分离并与光子器件间隔开的透镜系统来在原子探测过程中施加光子能量的方法。 本发明的其它方面涉及将光子能量从电极的外表面反射到样本上的方法。
    • 7. 发明申请
    • Atom Probes, Atom Probe Specimens, and Associated Methods
    • 原子探针,原子探针样品和相关方法
    • US20080308728A1
    • 2008-12-18
    • US12064020
    • 2006-08-15
    • Thomas F. KellyJoseph H. BuntonScott A. Wiener
    • Thomas F. KellyJoseph H. BuntonScott A. Wiener
    • G01N23/00
    • G01N23/22
    • The present invention relates generally to atom probes, atom probe specimens, and associated methods. For example, certain aspects are directed toward methods for analyzing a portion of a specimen that includes selecting a region of interest and moving a portion of material in a border region proximate to the region of interest so that at least a portion of the region of interest protrudes relative to at least a portion of the border region. The method further includes analyzing a portion of the region of interest. Other aspects of the invention are directed toward a method for applying photonic energy in an atom probe process by passing photonic energy through a lens system separated from a photonic device and spaced apart from the photonic device. Yet other aspects of the invention are directed toward a method for reflecting photonic energy off an outer surface of an electrode onto a specimen.
    • 本发明一般涉及原子探针,原子探针试样和相关方法。 例如,某些方面涉及用于分析样本的一部分的方法,所述方法包括选择感兴趣区域并移动靠近感兴趣区域的边界区域中的材料的一部分,使得感兴趣区域的至少一部分 相对于边界区域的至少一部分突出。 该方法还包括分析感兴趣区域的一部分。 本发明的其它方面涉及通过使光子能量通过从光子器件分离并与光子器件间隔开的透镜系统来在原子探测过程中施加光子能量的方法。 本发明的其它方面涉及将光子能量从电极的外表面反射到样本上的方法。
    • 8. 发明授权
    • Methods of sampling specimens for microanalysis
    • 微量分析样品取样方法
    • US06700121B1
    • 2004-03-02
    • US10428372
    • 2003-05-01
    • Thomas F. KellyRichard L. MartensSteven L. Goodman
    • Thomas F. KellyRichard L. MartensSteven L. Goodman
    • G01N132
    • G01N1/32Y10T436/25
    • Methods of sampling specimens for microanalysis, particularly microanalysis by atom probe microscopy, include steps of forming a study specimen in a first study object (as by use of focused ion beam milling); removing the study specimen from the study object; situating the study specimen on a second study object; and microanalyzing the study specimen. Where the first study object is of particular interest for study, the study specimen may be taken from a functional portion of the first study object so that microanalysis will provide information regarding this functional portion. Where the second study object is of particular interest for study, the second study object may be subjected to manufacturing processes (e.g., deposition of layers of materials) after the study specimen is situated thereon so that the study specimen will provide information regarding the results of the manufacturing process. The study specimen may have study regions formed thereon which are particularly suitable for study by atom probes, e.g., regions bearing raised protrusions, at virtually any point during the process, thereby greatly enhancing the speed and efficiency of specimen preparation.
    • 用于微量分析的样品取样方法,特别是通过原子探针显微镜进行微量分析的方法包括在第一研究对象中(如通过使用聚焦离子束研磨)形成研究样品的步骤; 从研究对象中取出研究标本; 将研究样本置于第二个研究对象上; 并微观分析研究样本。 如果第一研究对象对于研究特别感兴趣,则研究样本可以从第一研究对象的功能部分获取,使得微量分析将提供关于该功能部分的信息。 在第二研究对象特别感兴趣的研究中,第二研究对象可以在研究样本位于其上之后进行制造过程(例如,材料层的沉积),使得研究样本将提供关于 制造过程。 研究样本可以具有在其上形成的研究区域,其特别适合于在原子探针(例如,具有凸起突起的区域)的研究中,在该过程中的几乎任何点,从而大大提高了样品制备的速度和效率。
    • 9. 发明授权
    • Methods of sampling specimens for microanalysis
    • 微量分析样品取样方法
    • US06576900B2
    • 2003-06-10
    • US09861405
    • 2001-05-18
    • Thomas F. KellyRichard L. MartensSteven L. Goodman
    • Thomas F. KellyRichard L. MartensSteven L. Goodman
    • G01N132
    • G01N1/32Y10T436/25
    • Methods of sampling specimens for microanalysis, particularly microanalysis by atom probe microscopy, include steps of forming a study specimen in a first study object (as by use of focused ion beam milling); removing the study specimen from the study object; situating the study specimen on a second study object; and microanalyzing the study specimen. Where the first study object is of particular interest for study, the study specimen may be taken from a functional portion of the first study object so that microanalysis will provide information regarding this functional portion. Where the second study object is of particular interest for study, the second study object may be subjected to manufacturing processes (e.g., deposition of layers of materials) after the study specimen is situated thereon so that the study specimen will provide information regarding the results of the manufacturing process. The study specimen may have study regions formed thereon which are particularly suitable for study by atom probes, e.g., regions bearing raised protrusions, at virtually any point during the process, thereby greatly enhancing the speed and efficiency of specimen preparation.
    • 用于微量分析的样品取样方法,特别是通过原子探针显微镜进行微量分析的方法包括在第一研究对象中(如通过使用聚焦离子束研磨)形成研究样品的步骤; 从研究对象中取出研究标本; 将研究样本置于第二个研究对象上; 并微观分析研究样本。 如果第一研究对象对于研究特别感兴趣,则研究样本可以从第一研究对象的功能部分获取,使得微量分析将提供关于该功能部分的信息。 在第二研究对象特别感兴趣的研究中,第二研究对象可以在研究样本位于其上之后进行制造过程(例如,材料层的沉积),使得研究样本将提供关于 制造过程。 研究样本可以具有在其上形成的研究区域,其特别适合于在原子探针(例如,具有凸起突起的区域)的研究中,在该过程中的几乎任何点,从而大大提高了样品制备的速度和效率。
    • 10. 发明授权
    • High mass resolution local-electrode atom probe
    • 高质量分辨率的局部电极原子探针
    • US5440124A
    • 1995-08-08
    • US272204
    • 1994-07-08
    • Thomas F. KellyPatrick P. CamusDavid J. LarsonLouis M. HolzmanSateeshchandra S. Bajikar
    • Thomas F. KellyPatrick P. CamusDavid J. LarsonLouis M. HolzmanSateeshchandra S. Bajikar
    • G01Q90/00H01J37/285
    • H01J37/285H01J49/0004
    • An atom probe provides rapidly pulsed field evaporation/desorption of ions from a tip utilizing a local extraction electrode positioned closely adjacent to the tip. A bias potential is applied between the tip and the local extraction electrode which provides an electric field at the tip which is less than but near the field intensity required for field evaporation of ions. Additional potential is applied between the tip and the extraction electrode in relatively low over-voltage pulses to obtain field evaporation of ions without substantially accelerating the ions. The ions extracted from the tip by the sharply defined pulses pass through an aperture in the extraction electrode and are accelerated by a large potential difference between the tip and a detector spaced from the tip and the local extraction electrode. An intermediate acceleration electrode may be positioned between the extraction electrode and the detector, with the acceleration electrode having an aperture therein to pass ions therethrough to the detector. The acceleration electrode is maintained at a higher potential with respect to the tip than the extraction electrode, and may be maintained at the same potential as the detector so that ions passed through the acceleration electrode coast to the detector. The use of relatively low voltage pulses to obtain evaporation of ions permits rapid repetition of the pulses, on the order of hundreds of thousands of pulses per second, to allow rapid accumulation of atom probe data.
    • 原子探针使用位于尖端附近定位的局部提取电极,从尖端提供离子的快速脉冲场蒸发/解吸。 在尖端和局部引出电极之间施加偏置电位,该电极提供尖端处的电场,该电场小于但接近于离子的场蒸发所需的场强。 在相对低的过电压脉冲中,在尖端和引出电极之间施加额外的电位,以获得离子的场蒸发而基本不加速离子。 通过尖锐的脉冲从尖端提取的离子通过提取电极中的孔,并通过尖端和与尖端和局部引出电极间隔开的检测器之间的大的电位差加速。 中间加速电极可以位于提取电极和检测器之间,其中加速电极在其中具有孔,以将离子穿过其中到达检测器。 加速电极相对于提取电极保持在比尖端更高的电位,并且可以保持在与检测器相同的电位,使得通过加速电极的离子滑行到检测器。 使用相对较低电压的脉冲来获得离子蒸发允许脉冲的快速重复,每秒数十万个脉冲数量级,以允许原子探针数据的快速累积。