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1. 发明授权

US4419513A Isocyanato-isocyanurates, and process for the production thereof 失效
标题翻译：异氰酸酯 - 异氰脲酸酯，及其生产方法
公开(公告)号：US4419513A
公开(公告)日：1983-12-06
申请号：US296677
申请日：1981-08-27
申请人： Peter Breidenbach , Manfred Bock , Josef Pedain , Gerhard Mennicken
发明人： Peter Breidenbach , Manfred Bock , Josef Pedain , Gerhard Mennicken
IPC分类号： C07D251/34 , C08G18/00 , C08G18/72 , C08G18/73 , C08G18/75 , C08G18/79 , C09D175/00
CPC分类号： C07D251/34 , C08G18/792 , C08G2150/20
摘要： The present invention relates to a process for the preparation of novel isocyanato-isocyanurates by the catalytic and 1-isocyanato-3,3,5-trimethyl-5-isocyanatomethyl-cyclohexane in a mole ratio of about 1:4 to 4:1, and to the products produced therefrom.The present invention also relates to the use of these products, optionally in blocked form, as the isocyanate component in polyurethane lacquers.
摘要翻译：本发明涉及通过催化和1-异氰酸酯基-3,3,5-三甲基-5-异氰酸甲酯 - 环己烷以约1:4至4:1的摩尔比制备新型异氰酸根合异氰脲酸酯的方法，以及由此产生的产品。本发明还涉及这些产品，任选地以封闭形式用作聚氨酯漆中的异氰酸酯组分的用途。

2. 发明授权

US4373081A Coating compositions and process for the production of polyurethane coatings 失效
标题翻译：涂料组合物和生产聚氨酯涂料的方法
公开(公告)号：US4373081A
公开(公告)日：1983-02-08
申请号：US325242
申请日：1981-11-27
申请人： Klaus Nachtkamp , Manfred Bock , Gerhard Mennicken , Josef Pedain
发明人： Klaus Nachtkamp , Manfred Bock , Gerhard Mennicken , Josef Pedain
IPC分类号： C08G18/00 , C08G18/10 , C08G18/42 , C08G18/80 , C09D175/00 , C09D175/06
CPC分类号： C08G18/8093 , C08G18/10 , Y10T428/31551 , Y10T428/31605
摘要： The present invention relates to thermally cross-linkable coating compositions which are liquid and stable in storage at room temperature and which contain combinations of dialkyl-malonate-blocked polyisocyanates and organic polyhydroxyl compounds as binders and, optionally, auxiliaries and additives, being characterized in that the binder comprises:(a) a polyisocyanate component containing dialkyl-malonate-blocked isocyanate groups and a content of blocked isocyanate groups, expressed as NCO, based on the weight of the polyisocyanate component excluding the weight of the blocking agent, of from about 3 to 33.6% by weight, comprising(aa) at least one dialkyl-malonate-blocked, optionally alkyl-substituted diisocyanato-diphenyl methane and/or(ab) at least one dialkyl-malonate-blocked NCO-prepolymer based on excess quantities of optionally alkyl-substituted diisocyanatodiphenyl methane and organic compounds containing at least two hydroxyl groups and(b) a polyol component having an average hydroxyl functionality of greater than 2 and a content of alcoholic hydroxyl groups of from about 1.5 to 8% by weight, comprising at least one polyester polyol in quantities corresponding to an equivalent ratio of blocked isocyanate groups to hydroxyl groups of from about 0.6:1 to 2:1.The present invention also relates to a process for the production of coatings by coating heat-resistant substrates of any type with these coating compositions and subsequently hardening the coating at about 90.degree. to 220.degree. C.
摘要翻译：本发明涉及在室温下储存的液体和稳定的可热交联的涂料组合物，其含有二烷基 - 丙二酸酯封端的多异氰酸酯和有机多羟基化合物作为粘合剂和任选的助剂和添加剂的组合，其特征在于粘合剂包括：（a）含有二烷基 - 丙二酸酯封端的异氰酸酯基团的多异氰酸酯组分和封端异氰酸酯基团的含量，基于除了封闭剂重量以外的多异氰酸酯组分的重量，表示为NCO，为约3 包含（aa）至少一种二烷基 - 丙二酸酯封端的，任选的烷基取代的二异氰酸根合二苯基甲烷和/或（ab）至少一种二烷基 - 丙二酸酯封闭的NCO-预聚物，烷基取代的二异氰酸二苯二甲烷和含有至少两个羟基的有机化合物和（b）具有av的多元醇组分包括至少一种聚酯多元醇，其数量对应于封端异氰酸酯基与羟基的当量比为约0.6:1，其中羟基官能度大于2，醇羟基含量为约1.5至8重量％至2：1。本发明还涉及通过用这些涂料组合物涂覆任何类型的耐热基材并随后在约90℃至220℃硬化涂层来生产涂料的方法。

3. 发明授权

US4481345A Process for the production of combinations of organic polyisocyanates and at least partly blocked polyamines, the combinations obtainable by this process and their use for the production of lacquers, coating or sealing compositions 失效
标题翻译：用于生产有机多异氰酸酯和至少部分封闭的多胺的组合的方法，可通过该方法获得的组合及其用于生产漆，涂料或密封组合物的用途
公开(公告)号：US4481345A
公开(公告)日：1984-11-06
申请号：US583918
申请日：1984-02-27
申请人： Klaus Nachtkamp , Manfred Bock , Reinhard Halpaap , Josef Pedain
发明人： Klaus Nachtkamp , Manfred Bock , Reinhard Halpaap , Josef Pedain
IPC分类号： C09K3/10 , C08G18/10 , C08G18/32 , C08G18/65 , C09D175/00 , C09D175/02 , C09D175/04 , C08G18/38
CPC分类号： C08G18/3256 , C08G18/10
摘要： Process for the production of water-hardenable compositions of organic polyisocyanates and polyamines containing at least partly blocked amino groups present as ketimines, the combinations essentially representing mixtures and optionally reaction products containing urea groups by mixing the organic polyisocyanates with the polyamines in such quantities that the equivalent ratio of isocyanate groups to blocked and free amino groups is between about 0.9:1 and 4:1 and reacting any free amino groups present with some of the isocyanate groups in the polyisocyanate to form ureas, characterized in that the polyamines containing at least partly blocked amino groups used are mixtures comprising(a) from about 50 to 95 amine equivalent percent of organic compounds which are free from primary and secondary amino groups and which contain at least two ketimine groups corresponding to the following formula ##STR1## in which R.sup.1 represents an alkyl or cycloalkyl radical and R.sup.2 represents hydrogen or an alkyl or cycloalkyl radical or in which R.sup.1 and R.sup.2 form a cycloaliphatic hydrocarbon radical together with the two carbon atoms of the ketimine group and(b) from about 5 to 40 amine equivalent percent of organic compounds which are free from primary and secondary amino groups and which contain at least two ketimine groups of which one corresponds to the formula ##STR2## in which R.sup.1 and R.sup.2 are as defined above, the other ketimine group(s) present correspond(s) to the formula shown in (a).
摘要翻译：用于生产有机多异氰酸酯和含有至少部分封闭的胺基的多胺的水可硬化组合物作为酮亚胺存在的方法，所述组合基本上代表混合物和任选的含有尿素基团的反应产物，通过将有机多异氰酸酯与多胺混合，异氰酸酯基与封端和游离氨基的当量比为约0.9:1至4:1，并使与多异氰酸酯中存在的一些异氰酸酯基团存在的任何游离氨基反应形成脲，其特征在于，含有至少部分使用的封闭氨基是包含（a）约50至95胺当量百分比的不含伯和仲氨基并且含有至少两个对应于下式的酮亚胺基的有机化合物的混合物：其中R 1表示烷基或环烷基，R 2表示氢或a n烷基或环烷基，或其中R1和R2与酮亚胺基团的两个碳原子一起形成脂环族烃基，和（b）约5至40胺当量百分比的不含伯和仲氨基的有机化合物并且其包含至少两个酮亚胺基，其中一个对应于式（Ia）其中R 1和R 2如上所定义的式“IMAGE”，其它酮亚胺基与（a）所示的式表示。

4. 发明授权

US4146559A Cycloaliphatic diamines 失效
标题翻译：循环泵
公开(公告)号：US4146559A
公开(公告)日：1979-03-27
申请号：US827767
申请日：1977-08-25
申请人： Manfred Bock , Rudolf Braden , Josef Pedain
发明人： Manfred Bock , Rudolf Braden , Josef Pedain
IPC分类号： C07C215/14 , C07C67/00 , C07C209/00 , C07C209/26 , C07C209/52 , C07C211/36 , C07C213/00 , C07C217/08 , C07D295/02 , C08G18/10 , C08G18/32 , C07C87/40 , C07C87/28
CPC分类号： C07D295/02 , C08G18/10 , C08G18/3234
摘要： Compounds are disclosed which correspond to the general formula: ##STR1## in which N AND M WHICH ARE THE SAME OR DIFFERENT HAVE THE VALUES 0, 1 OR 2,R, r.sub.1 and R.sub.2 which are the same or different, represent hydrogen or CH.sub.3 -groupsAnd either(a) R.sub.3 and R.sub.5 represent hydrogen and R.sub.4 and R.sub.6 represent hydrogen, a C.sub.1 -C.sub.18 alkyl group, or a cycloalkyl group with 5 to 8 carbon atoms,Or(b) R.sub.3, R.sub.4, R.sub.5 and R.sub.6 independently represent C.sub.1 -C.sub.18 alkyl groups, or cycloalkyl groups containing 5 to 8 carbon atoms,Or(c) R.sub.3 and R.sub.4 together and R.sub.5 and R.sub.6 together, in conjunction with the nitrogen atom, form a heterocyclic C.sub.4 -C.sub.6 ring which may be interrupted by oxygen and/or nitrogen and which may be substituted by alkyl groups and/or hydroxyl alkyl groups with 1 to 4 carbon atoms.These compounds are produced by hydrogenating the corresponding diketones in the presence of ammonia or a primary or secondary aliphatic or cycloaliphatic amine.

5. 发明授权

US4101578A Cycloaliphatic triamines 失效
标题翻译：环脂族三胺
公开(公告)号：US4101578A
公开(公告)日：1978-07-18
申请号：US778632
申请日：1977-03-17
申请人： Manfred Bock , Josef Pedain , Rudolf Braden
发明人： Manfred Bock , Josef Pedain , Rudolf Braden
IPC分类号： C07C265/14 , C07C20060101 , C07C67/00 , C07C209/00 , C07C209/26 , C07C209/48 , C07C211/18 , C07C241/00 , C07C87/02
CPC分类号： C07C405/00
摘要： This invention relates to new cycloaliphatic triamines which are valuable intermediate products for synthetic resins, above all for lightfast and weather resistant polyurethane resins and in particular for solvent-free or low solvent polyurethane lacquers.
摘要翻译：本发明涉及新的脂环族三胺，它们是合成树脂的有价值的中间产物，尤其是耐光和耐候性聚氨酯树脂，特别是无溶剂或低溶剂聚氨酯漆。

6. 发明授权

US4113705A Triisocyanates useful for the production of polyurethane resins 失效
标题翻译：可用于生产聚氨酯树脂的三异氰酸酯
公开(公告)号：US4113705A
公开(公告)日：1978-09-12
申请号：US778631
申请日：1977-03-17
申请人： Manfred Bock , Josef Pedain , Walter Uerdingen
发明人： Manfred Bock , Josef Pedain , Walter Uerdingen
IPC分类号： C08G18/00 , C07C67/00 , C07C241/00 , C07C265/00 , C07C265/14 , C08G18/73 , C08G18/75 , C09D175/00 , C07C119/045
CPC分类号： C08G18/757
摘要： This invention relates to new liquid cycloaliphatic triisocyanates and to their use as isocyanate components for the production of polyurethane resins by the known isocyanate polyaddition process.
摘要翻译：本发明涉及新的液体脂环族三异氰酸酯及其作为通过已知的异氰酸酯加聚方法生产聚氨酯树脂的异氰酸酯组分的用途。

7. 发明授权

US4870152A Process for the production of compounds containing isocyanurate groups and olefinic double bonds and their use as binders 失效
标题翻译：用于生产含有异氰脲酸酯基和烯属双键的化合物的方法及其作为粘合剂的用途
公开(公告)号：US4870152A
公开(公告)日：1989-09-26
申请号：US262623
申请日：1988-10-26
申请人： Jurgen Meixner , Manfred Bock , Josef Pedain , Manfred Schonfelder
发明人： Jurgen Meixner , Manfred Bock , Josef Pedain , Manfred Schonfelder
IPC分类号： C07D251/34 , C08G18/42 , C08G18/67 , C08G18/72 , C08G18/79 , C08G18/81 , C09D175/00 , C09D175/14
CPC分类号： C08G18/672 , C07D251/34 , C08G18/4216 , C08G18/4238 , C08G18/792 , C08G18/8175
摘要： Binders which are hardenable by radiation or peroxides and are useful in coating compositions are compounds containing isocyanurate groups and olefinic double bonds produced by the reaction of components (a), (b) and (c) wherein(a) is a polyisocyanate component containing isocyanurate polyisocyanates which is(i) N,N',N"-tris-(isocyanatohexyl)-isocyanurate alone or in admixture with its higher homologs containing more than one isocyanurate ring or(ii) mixtures of the polyisocyanates (i) with up to 40 NCO-equivalent-%, based on the total component (a), of other polyisocyanates containing aliphatically or cycloaliphatically bound isocyanate groups;(b) is an olefinically unsaturated alcohol component comprising at least one hydroxyalkyl ester of acrylic acid or methacrylic acid; and(c) is a polyol component consisting essentially of a polyester polyol having an OH value of 80 to 350 based on (i) an acid component, of which at least 80 carboxyl equivalent-% is adipic acid, isophthalic acid or a mixture of both and (ii) a polyhydroxy component of which at least 70 hydroxyl equivalent-% is hexane-1, 6-diol;wherein component (c) amounts to 20 to 150% by weight, based on the weight of component (b), and the reaction is carried out at with an NCO:OH equivalent ratio maintained at 0.9:1 to 1.1:1, and wherein components (b) and (c) are reacted with the polyisocyanate component in any order or in admixture.
摘要翻译：通过辐射或过氧化物可硬化并且可用于涂料组合物的粘合剂是含有通过组分（a），（b）和（c）反应生成的异氰脲酸酯基团和烯属双键的化合物，其中（a）是含有异氰脲酸酯的多异氰酸酯组分多异氰酸酯，其是单独的或与其含有多于一个异氰脲酸酯环的较高同系物混合的（i）N，N'，N“ - 三 - （异氰酸根合己基） - 异氰脲酸酯的多异氰酸酯，或（ii）多异氰酸酯（i）基于总组分（a），含有脂族或环脂族结合的异氰酸酯基团的其它多异氰酸酯的40NCO当量％; （b）是包含至少一种丙烯酸或甲基丙烯酸的羟烷基酯的烯属不饱和醇组分; 和（c）是基于（i）酸组分的羟值为80至350的聚酯多元醇组成的多元醇组分，其中至少80羧基当量 - ％是己二酸，间苯二甲酸或两者和（ii）多羟基组分，其中至少70个羟基当量 - ％是己烷-1,6-二醇; 其中组分（c）基于组分（b）的重量计为20至150重量％，并且以保持在0.9:1至1.1:1的NCO:OH当量比进行反应，其中组分（b）和（c）以多异氰酸酯组分的任何顺序或混合物反应。

8. 发明授权

US4777220A Process for the production of prepolymers containing isocyanate groups, prepolymers produced by this process and their use 失效
标题翻译：用于生产含异氰酸酯基团的预聚物的方法，通过该方法制备的预聚物及其用途
公开(公告)号：US4777220A
公开(公告)日：1988-10-11
申请号：US151866
申请日：1988-02-03
申请人： Reinhard Halpaap , Manfred Bock , Josef Pedain , Gerhard Klein , Dieter Arlt
发明人： Reinhard Halpaap , Manfred Bock , Josef Pedain , Gerhard Klein , Dieter Arlt
IPC分类号： C08G18/10 , C08G18/12 , C08G18/42 , C08G18/65 , C08G18/66 , C08G18/73 , C08G18/75 , C09D175/00 , C09D175/06
CPC分类号： C08G18/756 , C08G18/10 , C08G18/12 , C08G18/42 , C08G18/4202 , C08G18/664 , C08G18/735
摘要： The present invention is directed to a process for the production of prepolymers containing free tertiary isocyanate groups by reacting(a) an organic diisocyanate containing one isocyanate group attached to a primary aliphatic carbon atom and an isocyanate group attached to a tertiary aliphatic or cycloaliphatic carbon atom with(b) a polyester polyol having a molecular weight of 800 to 12,000 and a hydroxyl functionality of 2 to 6 at an NCO/OH equivalent ratio of 1.6:1 to 2:1 to provide prepolymers having a molecular weight of about 1000 to 3000 and an NCO content of about 4 to 12%.The present invention is also directed to the prepolymers containing free isocyanate groups obtained by this process and to their use for the production of polyurethane lacquers and coatings.
摘要翻译：本发明涉及通过使（a）含有连接到伯脂肪族碳原子上的一个异氰酸酯基团和连接到叔脂族或脂环族碳原子上的异氰酸酯基团的有机二异氰酸酯反应生产含游离叔异氰酸酯基团的预聚物的方法与（b）分子量为800〜12000，羟基官能度为2〜6，聚酯多元醇的NCO / OH当量比为1.6:1〜2:1，得到分子量约为1000〜3000的预聚物 NCO含量约为4〜12％。本发明还涉及通过该方法获得的含有游离异氰酸酯基团的预聚物及其用于生产聚氨酯漆和涂料的用途。

9. 发明授权

US4288586A Process for the preparation of polyisocyanates containing isocyanurate groups 失效
标题翻译：制备含有异氰脲酸酯基团的多异氰酸酯的方法
公开(公告)号：US4288586A
公开(公告)日：1981-09-08
申请号：US11465
申请日：1979-02-12
申请人： Manfred Bock , Josef Pedain , Wilhelm Slawyk
发明人： Manfred Bock , Josef Pedain , Wilhelm Slawyk
IPC分类号： B01J31/02 , C07B61/00 , C07D251/34 , C08G18/00 , C08G18/78 , C08G18/79 , C08G18/80 , C08G18/16
CPC分类号： C07D251/34 , C08G18/792 , C08G18/8061 , C08G2150/20
摘要： The present invention relates to a new process for the preparation of polyisocyanates containing isocyanurate groups by the partial trimerization of the isocyanate groups of 1-isocyanato-3,3,5-trimethyl-5-isocyanatomethyl-cyclohexane (also known as isophorone diisocyanate and abbreviated IPDI), using catalysts which accelerate the trimerization of isocyanate groups, characterized in that the catalysts used are quaternary hydroxyalkyl ammonium hydroxides containing at least one hydroxyalkyl group. The present invention also relates to the polyisocyanates containing isocyanurate groups produced according to this process and to their use, optionally in the form of products which are blocked with blocking agents for isocyanate groups, as isocyanate components for polyurethane lacquers.
摘要翻译：本发明涉及通过1-异氰酸酯基-3,3,5-三甲基-5-异氰酸甲酯基环己烷（也称为异佛尔酮二异氰酸酯）和缩写的异氰酸酯二异氰酸酯的异氰酸酯基部分三聚制备含有异氰脲酸酯基团的多异氰酸酯的新方法 IPDI），使用加速异氰酸酯基团三聚的催化剂，其特征在于所用的催化剂是含有至少一个羟烷基的季羟基烷基氢氧化铵。本发明还涉及根据该方法制备的含有异氰脲酸酯基团的多异氰酸酯基团及其用途，任选地以用于异氰酸酯基团的封闭剂封闭的产品形式，作为聚氨酯漆的异氰酸酯组分。

10. 发明授权

US4045462A Bicyclic triisocyanates 失效
标题翻译：双环三异氰酸酯
公开(公告)号：US4045462A
公开(公告)日：1977-08-30
申请号：US674014
申请日：1976-04-05
申请人： Manfred Bock , Walter Uerdingen , Josef Pedain
发明人： Manfred Bock , Walter Uerdingen , Josef Pedain
IPC分类号： C08G18/00 , C07C67/00 , C07C241/00 , C07C255/45 , C07C263/10 , C07C265/00 , C07C265/08 , C07C265/10 , C07C265/14 , C08G18/72 , C08G18/73 , C08G18/75 , C08L75/04 , C09D175/00 , C07C119/045
CPC分类号： C07C265/00 , C08G18/758
摘要： The instant invention is directed to new liquid bicycloaliphatic triisocyanates and to the use thereof as the isocyanate component in the production of polyurethane plastics by the known isocyanate-polyaddition process. The new triisocyanates are particularly suitable for use as the isocyanate component in low-solvent, light-stable two-component polyurethane lacquers.
摘要翻译：本发明涉及新的液体双环脂族三异氰酸酯，以及通过已知的异氰酸酯加聚方法在聚氨酯塑料生产中作为异氰酸酯组分的用途。新的三异氰酸酯特别适合用作低溶剂，轻质双组分聚氨酯漆中的异氰酸酯组分。

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