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1. 发明申请

US20130273250A1 (AMIDE AMINO ALKANE) METAL COMPOUND, METHOD OF MANUFACTURING METAL-CONTAINING THIN FILM USING SAID METAL COMPOUND 有权
标题翻译：（AMIDE AMINO ALKANE）金属化合物，使用含金属化合物制造含金属薄膜的方法
公开(公告)号：US20130273250A1
公开(公告)日：2013-10-17
申请号：US13882824
申请日：2011-11-02
申请人： Osamu Fujimura , Hiroki Kanato , Masashi Shirai , Hiroshi Nihei
发明人： Osamu Fujimura , Hiroki Kanato , Masashi Shirai , Hiroshi Nihei
IPC分类号： H01L51/00 , C07F15/06 , C07F5/00 , C07F3/06 , C07F15/02 , C07F15/04 , C07F3/02 , C07F13/00
CPC分类号： H01L51/0083 , C07C211/65 , C07F3/02 , C07F3/06 , C07F5/003 , C07F13/005 , C07F15/025 , C07F15/045 , C07F15/065 , C23C16/18 , C23C16/403 , C23C16/407 , H01L51/0077 , H01L51/0084 , H01L51/0089 , H01L51/0092
摘要： The present invention relates to an (amide amino alkane) metal compound represented by the formula (1): wherein M represents a metal atom; R1 represents a linear, branched or cyclic alkyl group having 1 to 6 carbon atoms; R2 and R3 may be the same as, or different from each other, and each independently represents a linear or branched alkyl group having 1 to 3 carbon atoms, or R2 and R3 may form a substituted or unsubstituted 5- or 6-membered ring together with the nitrogen atom to which they are bound; Z represents a linear or branched alkylene group having 1 to 10 carbon atoms (a part of which may optionally form a ring); and n represents a number of the ligands, which is equal to the valence of the metal (M), and represents an integer of from 1 to 3; with the proviso that the metal compounds in which M is Li (Lithium), Be (Beryllium), Ge (Germanium) or Nd (Neodymium) are excluded; the metal compounds in which M is Mg (Magnesium) and R1 is methyl group are excluded; the metal compounds in which M is Zn (Zinc) and R1 is methyl group are excluded; the metal compounds in which M is Bi (Bismuth) and R1 is t-butyl group are excluded; and in cases where n is two or greater, two or more ligands may be the same as, or different from each other; and a method of producing a metal-containing thin film using the metal compound.
摘要翻译：本发明涉及由式（1）表示的（酰胺氨基烷烃）金属化合物：其中M表示金属原子; R1表示碳原子数为1〜6的直链状，支链状或环状的烷基。 R 2和R 3可以彼此相同或不同，并且各自独立地表示具有1至3个碳原子的直链或支链烷基，或者R 2和R 3可以一起形成取代或未取代的5-或6-元环与它们所结合的氮原子一起; Z表示碳原子数1〜10的直链状或支链状的亚烷基（其一部分可以形成环）。 n表示与金属（M）的化合价相同的配体数，表示1〜3的整数。条件是不包括其中M为Li（锂），Be（铍），Ge（锗）或Nd（钕）的金属化合物; 其中M为Mg（镁）和R1为甲基的金属化合物被排除; 其中M为Zn（锌）和R1为甲基的金属化合物被排除; 其中M为Bi（铋）和R 1为叔丁基的金属化合物被排除; 并且在n为2或更大的情况下，两个或多个配体可以彼此相同或不同; 以及使用该金属化合物制造含金属薄膜的方法。

2. 发明授权

US08871304B2 (Amide amino alkane) metal compound, method of manufacturing metal-containing thin film using said metal compound 有权
标题翻译：（酰胺氨基烷烃）金属化合物，使用所述金属化合物制造含金属薄膜的方法
公开(公告)号：US08871304B2
公开(公告)日：2014-10-28
申请号：US13882824
申请日：2011-11-02
申请人： Osamu Fujimura , Hiroki Kanato , Masashi Shirai , Hiroshi Nihei
发明人： Osamu Fujimura , Hiroki Kanato , Masashi Shirai , Hiroshi Nihei
IPC分类号： H01L51/00 , C07F15/00 , C07F13/00 , C07F5/00 , C07F3/00 , C07F15/06 , C07F15/04 , C07F15/02 , C07F3/02 , C07F3/06
CPC分类号： H01L51/0083 , C07C211/65 , C07F3/02 , C07F3/06 , C07F5/003 , C07F13/005 , C07F15/025 , C07F15/045 , C07F15/065 , C23C16/18 , C23C16/403 , C23C16/407 , H01L51/0077 , H01L51/0084 , H01L51/0089 , H01L51/0092
摘要： The present invention relates to an (amide amino alkane) metal compound represented by the formula (1): wherein M represents a metal atom; R1 represents a linear, branched or cyclic alkyl group having 1 to 6 carbon atoms; R2 and R3 may be the same as, or different from each other, and each independently represents a linear or branched alkyl group having 1 to 3 carbon atoms, or R2 and R3 may form a substituted or unsubstituted 5- or 6-membered ring together with the nitrogen atom to which they are bound; Z represents a linear or branched alkylene group having 1 to 10 carbon atoms (a part of which may optionally form a ring); and n represents a number of the ligands, which is equal to the valence of the metal (M), and represents an integer of from 1 to 3; with the proviso that the metal compounds in which M is Li (Lithium), Be (Beryllium), Ge (Germanium) or Nd (Neodymium) are excluded; the metal compounds in which M is Mg (Magnesium) and R1 is methyl group are excluded; the metal compounds in which M is Zn (Zinc) and R1 is methyl group are excluded; the metal compounds in which M is Bi (Bismuth) and R1 is t-butyl group are excluded; and in cases where n is two or greater, two or more ligands may be the same as, or different from each other; and a method of producing a metal-containing thin film using the metal compound.
摘要翻译：本发明涉及由式（1）表示的（酰胺氨基烷烃）金属化合物：其中M表示金属原子; R1表示碳原子数为1〜6的直链状，支链状或环状的烷基。 R 2和R 3可以彼此相同或不同，并且各自独立地表示具有1至3个碳原子的直链或支链烷基，或者R 2和R 3可以一起形成取代或未取代的5-或6-元环与它们所结合的氮原子一起; Z表示碳原子数1〜10的直链状或支链状的亚烷基（其一部分可以形成环）。 n表示与金属（M）的化合价相同的配体数，表示1〜3的整数。条件是不包括其中M为Li（锂），Be（铍），Ge（锗）或Nd（钕）的金属化合物; 其中M为Mg（镁）和R1为甲基的金属化合物被排除; 其中M为Zn（锌）和R1为甲基的金属化合物被排除; 其中M为Bi（铋）和R 1为叔丁基的金属化合物被排除; 并且在n为2或更大的情况下，两个或多个配体可以彼此相同或不同; 以及使用该金属化合物制造含金属薄膜的方法。

3. 发明申请

US20060069273A1 Process for producing 1-acetoxy-3-(substituded phenyl) propenes 有权
标题翻译： 1-乙酰氧基-3-（取代苯基）丙烯的制备方法
公开(公告)号：US20060069273A1
公开(公告)日：2006-03-30
申请号：US10539785
申请日：2003-12-18
申请人： Masashi Shirai , Yoshihiro Yoshida , Shinichiro Sadaike
发明人： Masashi Shirai , Yoshihiro Yoshida , Shinichiro Sadaike
IPC分类号： C07D307/87 , C07C67/02
CPC分类号： C07D317/54 , C07C67/293 , C07C69/007 , C07D319/18 , C07C69/157
摘要： The compounds represented by the formula (I) are produced by reacting benzene compound of the formula (IV) or (V) with alkenylidene diacetate of the formula (VI) in the presence of a catalyst comprising one or more members selected from (a) halogenated boron compounds, (b) triflate compounds of Group 11 elements, (c) halogenated compounds of Group 12 elements, and (d) triflate and halogenated compounds of tin and atomic numbers 58 and 66 to 71 elements. R1, R2=H or C1-C10 alkyl group A=Substituted phenyl group corresponding to a compound of formula (IV) or (V), R3, R4=H or C1-C4 alkyl group, m=0 or 1-4, n=1 to 5, k=1 or 2.
摘要翻译：由式（I）表示的化合物通过使式（Ⅳ）或（Ⅴ）的苯化合物与式（Ⅵ）的亚乙烯基二乙酸酯在含有一种或多种选自（ⅰ）卤代硼化合物，（b）第11族元素的三氟甲磺酸酯化合物，（c）第12族元素的卤代化合物，

4. 发明授权

US5332844A Method of producing straight-chain acrylonitrile dimers 失效
标题翻译：制备直链丙烯腈二聚体的方法
公开(公告)号：US5332844A
公开(公告)日：1994-07-26
申请号：US26487
申请日：1993-03-04
申请人： Ryoji Sugise , Kouichi Kashiwagi , Masashi Shirai , Toshihiro Shimakawa
发明人： Ryoji Sugise , Kouichi Kashiwagi , Masashi Shirai , Toshihiro Shimakawa
IPC分类号： C07C253/30
CPC分类号： C07C253/30 , Y02P20/52
摘要： Straight-chain acrylonitrile dimers including 1,4-dicyanobutene, 1,4-dicyanobutadiene and adiponitrile are produced at a high selectivity rate and yield by dimerizing acrylonitrile in the presence of a catalyst comprising at least one ruthenium compound, for example dichloro-tetrakis (dimethylsulfoxide) ruthenium, and in the presence of at least one organic acid, for example, propionic acid, and optionally in the further presence of a basic compound, a reducing compound and/or a sulfoxide compound.
摘要翻译：在包含至少一种钌化合物的催化剂存在下，以高选择率和丙烯腈二聚制备直链丙烯腈二聚体，包括1,4-二氰基丁腈，1,4-二氰基丁二烯和己二腈，例如二氯四（二甲基亚砜）钌，并且在至少一种有机酸例如丙酸存在下，以及任选地在碱性化合物，还原性化合物和/或亚砜化合物的存在下进一步存在。

5. 发明授权

US07173148B2 Process for producing 1-acetoxy-3-(substituted phenyl)propene compound 有权
标题翻译： 1-乙酰氧基-3-（取代苯基）丙烯化合物的制备方法
公开(公告)号：US07173148B2
公开(公告)日：2007-02-06
申请号：US10539785
申请日：2003-12-18
申请人： Masashi Shirai , Yoshihiro Yoshida , Shinichiro Sadaike
发明人： Masashi Shirai , Yoshihiro Yoshida , Shinichiro Sadaike
IPC分类号： C07C67/02
CPC分类号： C07D317/54 , C07C67/293 , C07C69/007 , C07D319/18 , C07C69/157
摘要： The compounds represented by the formula (I) are produced by reacting benzene compound of the formula (IV) or (V) with alkenylidene diacetate of the formula (VI) in the presence of a catalyst comprising one or more members selected from (a) halogenated boron compounds, (b) triflate compounds of Group 11 elements, (c) halogenated compounds of Group 12 elements, and (d) triflate and halogenated compounds of tin and atomic numbers 58 and 66 to 71 elements. R1, R2=H or C1–C10 alkyl group A=Substituted phenyl group corresponding to a compound of formula (IV) or (V), R3, R4=H or C1–C4 alkyl group, m=0 or 1–4, n=1 to 5, k=1 or 2.
摘要翻译：由式（I）表示的化合物通过使式（Ⅳ）或（Ⅴ）的苯化合物与式（Ⅵ）的亚乙烯基二乙酸酯在含有一种或多种选自（ⅰ）卤代硼化合物，（b）第11族元素的三氟甲磺酸酯化合物，（c）第12族元素的卤代化合物，和（d）锡和原子数58和66至71元素的三氟甲磺酸酯和卤代化合物。 R 1，R 2 = H或C 1 -C 10烷基A =对应于式（IV）或（V）化合物的取代的苯基，R“ 3，R 4 = H或C 1 -C 4烷基，m = 0或1-4，n = 1至5，k = 1或2。

6. 发明授权

US5696301A Process for preparing protocatechualdehyde 失效
标题翻译：原儿茶醛的制备方法
公开(公告)号：US5696301A
公开(公告)日：1997-12-09
申请号：US787583
申请日：1997-01-22
申请人： Katsumasa Harada , Masashi Shirai , Toshio Furuya , Nobuyuki Kuroda
发明人： Katsumasa Harada , Masashi Shirai , Toshio Furuya , Nobuyuki Kuroda
IPC分类号： C07C45/43 , C07D317/46 , C07C34/10 , C07D307/00 , C07D317/44
CPC分类号： C07D317/46 , C07C45/43
摘要： Protocatechualdehyde is prepared by the steps of reacting piperonyl dichloride with molecular chlorine in the presence of phosphorus trichloride, phosphorus pentachloride or sulfuryl chloride to prepare dichloropiperonylidene dichloride and hydrolyzing the dichloropiperonylidene dichloride. The piperonyl dichloride can be prepared by the reaction of piperonal with thionyl chloride in the presence of dimethylformamide.
摘要翻译：通过在三氯化磷，五氯化磷或磺酰氯存在下使胡椒基二氯与分子氯反应的步骤制备原儿茶醛，制备二氯哌啶子基二氯化物并水解二氯磷酰二氯。胡椒基二氯化物可以通过胡椒醛与亚硫酰氯在二甲基甲酰胺存在下反应来制备。

7. 发明授权

US06603024B1 Process for the preparation of 3,4-methylenedioxymandelic acid 失效
标题翻译：制备3,4-亚甲二氧基扁桃酸的方法
公开(公告)号：US06603024B1
公开(公告)日：2003-08-05
申请号：US10110263
申请日：2002-04-02
申请人： Katsumasa Harada , Masashi Shirai , Koji Shiba
发明人： Katsumasa Harada , Masashi Shirai , Koji Shiba
IPC分类号： C07D32302
CPC分类号： C07D317/60
摘要： A process for preparing 3,4-methylenedioxymandelic acid by reacting 1,2-methylenedioxybenzene with glyoxylic acid in the presence of a strong acid and of at least one substance selected from the group consisting of an aprotic organic solvent and 100 to 1200 ml of an organic acid per kg of 1,2-methylenedioxybenzene.
摘要翻译：一种通过1,2-亚甲二氧基苯与乙醛酸在强酸和至少一种选自非质子有机溶剂和100至1200ml 有机酸/ kg 1,2-亚甲二氧基苯。

8. 发明授权

US06573397B2 Process for producing 3,4-dihydroxybenzonitrile 失效
标题翻译： 3,4-二羟基苄腈的制备方法
公开(公告)号：US06573397B2
公开(公告)日：2003-06-03
申请号：US10170360
申请日：2002-06-14
申请人： Masashi Shirai , Koji Shiba , Toshio Furuya
发明人： Masashi Shirai , Koji Shiba , Toshio Furuya
IPC分类号： C07C25550
CPC分类号： C07C253/30 , C07C255/53
摘要： 3,4-dihydroxybenzonitrile useful as a starting compound for synthesis of medicines and agricultural chemicals is produced, with a high yield by chlorinating 3,4-methylenedioxybenzonitrile with sulfuryl chloride or a mixture of molecular chlorine with a chlorination-promoter including phosphorus trichloride, phosphorus pentachloride, sulfuryl chloride, thionyl chloride, and/or nitrosyl chloride, to prepare 2-chloro-benzo[1,3]dioxole-5-carbonitrile, and hydrolyzing 2-chloro-benzo[1,3]dioxole-5-carbonitrile by contacting it with water to produce 3,4-dihydroxybenzonitrile.
摘要翻译：制备可用作合成药物和农药的起始化合物的3,4-二羟基苄腈，通过用磺酰氯或分子氯与氯化促进剂的混合物氯化3,4-亚甲二氧基苄腈，产率高，包括三氯化磷，磷五氯化碳，磺酰氯，亚硫酰氯和/或亚硝酰氯，以制备2-氯 - 苯并[1,3]间二氧杂环戊烯-5-甲腈，并通过以下方法水解2-氯 - 苯并[1,3]间二氧杂环戊烯-5-腈：将其与水接触以产生3,4-二羟基苄腈。

9. 发明授权

US5466858A Method of producing straight-chain acrylonitrile dimers 失效
标题翻译：制备直链丙烯腈二聚体的方法
公开(公告)号：US5466858A
公开(公告)日：1995-11-14
申请号：US298113
申请日：1994-08-30
申请人： Ryoji Sugise , Kouichi Kashiwagi , Masashi Shirai , Toshihiro Shimakawa
发明人： Ryoji Sugise , Kouichi Kashiwagi , Masashi Shirai , Toshihiro Shimakawa
IPC分类号： C07C63/70 , C07C65/32 , C07C65/34 , C07C253/30
CPC分类号： C07C65/32 , C07C253/30 , C07C65/34 , Y02P20/52
摘要： Straight-chain acrylonitrile dimers including 1,4-dicyanobutene, 1,4-dicyanobutadiene and adiponitrile are produced at a high selectivity by dimerizing acrylonitrile in the presence of a ruthenium catalyst, and in the presence of a straight-chain dimer selectivity-enhancing agent comprising at least one member selected from(A) substituted benzoic acids, except for monoalkylbenzoic acids, having at least one substituent and preferably exhibiting a pKa of 1.50 to 6.0 determined in water at an ionic strength of 0 to 0.1 mole/liter at 25.degree. C.;(B) hetero atom-containing acyclic carboxylic acids having at least one substituent having a sulfur or nitrogen atom attached to a carbon atom located in an .alpha.- on .beta.-position with respect to a carboxyl group in a main hydrocarbon structure; and(C) 5 to 12 membered heterocyclic carboxylic acids having an oxygen, sulfur or nitrogen atom included in a 5 to 12 membered heterocyclic structure and a carboxyl or carboxymethyl group attached to a carbon atom located in an .alpha.-position with respect to the hetero atom.
摘要翻译：通过在钌催化剂的存在下使丙烯腈二聚，并且在直链二聚体选择性增强剂的存在下，以高选择性制备包括1,4-二氰基，1,4-二氰基丁二烯和己二腈的直链丙烯腈二聚体包括至少一种选自（A）取代的苯甲酸，除了单烷基苯甲酸，具有至少一个取代基，并且优选表现出在25℃下在离子强度为0至0.1摩尔/升的水中测定的pKa为1.50至6.0。 C。; （B）具有至少一个具有硫原子或氮原子的取代基的含杂原子的非环状羧酸与位于主烃结构中的羧基上位于β-位上的α-位上的碳原子连接; 和（C）5至12元杂环结构中包含的具有氧，硫或氮原子的5至12元杂环羧酸和连接于位于相对于杂原子的α位的碳原子上的羧基或羧甲基原子。

10. 发明授权

US08633380B2 Photoelectric conversion element comprising binuclear ruthenium complex dye having a substituted bipyridyl group, and photochemical cell 失效
标题翻译：包含具有取代的联吡啶基的双核钌络合物染料和光化学电池的光电转换元件
公开(公告)号：US08633380B2
公开(公告)日：2014-01-21
申请号：US13635226
申请日：2011-03-15
申请人： Kazuaki Kakita , Takafumi Iwasa , Yoshihisa Kakuta , Masashi Shirai , Toshio Furuya , Shigeyoshi Nishino , Hidetaka Shima
发明人： Kazuaki Kakita , Takafumi Iwasa , Yoshihisa Kakuta , Masashi Shirai , Toshio Furuya , Shigeyoshi Nishino , Hidetaka Shima
IPC分类号： H01G9/20 , H01L51/48 , H01L51/46
CPC分类号： H01M14/005 , C07F15/0053 , C09B23/102 , C09B57/10 , H01G9/2031 , H01G9/2059 , H01L51/0086 , H01L51/009 , Y02E10/542 , Y02E10/549 , Y02P70/521
摘要： The present invention relates to a binuclear ruthenium complex dye having a higher absorption coefficient and capable of absorbing light of longer wavelength for realizing a photoelectric conversion element and a photochemical cell which may convert solar light into electricity over a wide wavelength range and exhibit high photoelectric conversion efficiency; and a binuclear ruthenium complex dye for realizing a photoelectric conversion element and a photochemical cell which may have high durability.
摘要翻译：本发明涉及一种具有较高吸收系数并能够吸收较长波长的光的双核钌络合物染料，用于实现光电转换元件和可将太阳光转换成宽波长范围内的电并显示高光电转换的光化学电池效率; 以及用于实现可能具有高耐久性的光电转换元件和光化学电池的双核钌络合物染料。

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