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1. 发明授权

US09907336B2 Porous carbon materials and smoking articles and smoke filters therefor incorporating such materials 有权
公开(公告)号：US09907336B2
公开(公告)日：2018-03-06
申请号：US11887301
申请日：2006-03-27
申请人： Maria Cashmore , Peter Rex White , Oleksandr Kozynchenko , Andrew Blackburn , Stephen Robert Tennison
发明人： Maria Cashmore , Peter Rex White , Oleksandr Kozynchenko , Andrew Blackburn , Stephen Robert Tennison
IPC分类号： A24B15/28 , A24D3/16 , B01J20/20 , B01J20/28 , C04B38/00 , C04B38/06 , C01B32/30
CPC分类号： A24D3/163 , B01J20/20 , B01J20/28011 , B01J20/28057 , B01J20/28069 , B01J20/28073 , B01J20/28076 , B01J20/2808 , B01J20/28083 , B01J20/28092 , C01B32/30 , C01P2004/51 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , C04B38/009 , C04B38/0615 , C04B35/52 , C04B38/0054 , C04B38/0067
摘要： A porous carbon material suitable for incorporation in smoke filters for cigarettes has a BET surface area of at least 800 m2/g and a pore structure that includes mesopores and micropores. The pore volume (as measured by nitrogen adsorption) is at least 0.9 cm3/g and from 15 to 65% of the pore volume is in mesopores. The pore structure of the material provides a bulk density generally less than 0.5 g/cc. The material may be produced by carbonizing and activating organic resins and may be in the form of beads for ease of handling.

2. 发明申请

US20090038632A1 Porous Carbon Materials and Smoking Articles and Smoke Filters Therefor Incorporating Such Materials 有权
标题翻译：多孔碳材料及其吸烟用品和烟雾过滤器
公开(公告)号：US20090038632A1
公开(公告)日：2009-02-12
申请号：US11887301
申请日：2006-03-27
申请人： Maria Cashmore , Peter Rex White , Oleksandr Kozynchenko , Andrew Blackburn , Stephen Robert Tennison
发明人： Maria Cashmore , Peter Rex White , Oleksandr Kozynchenko , Andrew Blackburn , Stephen Robert Tennison
IPC分类号： A24D3/08 , C08J9/00
CPC分类号： A24D3/163 , B01J20/20 , B01J20/28011 , B01J20/28057 , B01J20/28069 , B01J20/28073 , B01J20/28076 , B01J20/2808 , B01J20/28083 , B01J20/28092 , C01B32/30 , C01P2004/51 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , C04B38/009 , C04B38/0615 , C04B35/52 , C04B38/0054 , C04B38/0067
摘要： A porous carbon material suitable for incorporation in smoke filters for cigarettes has a BET surface area of at least 800 m2/g and a pore structure that includes mesopores and micropores. The pore volume (as measured by nitrogen adsorption) is at least 0.9 cm3/g and from 15 to 65% of the pore volume is in mesopores. The pore structure of the material provides a bulk density generally less than 0.5 g/cc. The material may be produced by carbonising and activating organic resins and may be in the form of beads for ease of handling.
摘要翻译：适用于掺入香烟烟雾过滤器的多孔碳材料具有至少800m 2 / g的BET表面积和包括中孔和微孔的孔结构。孔体积（通过氮吸附测量）为至少0.9cm 3 / g，孔体积的15至65％在中孔中。材料的孔结构提供通常小于0.5g / cc的堆积密度。该材料可以通过碳化和活化有机树脂来生产，并且可以是珠子的形式以便于处理。

3. 发明授权

US08383703B2 Making discrete solid particles of polymeric material 有权
标题翻译：制成离散固体颗粒的聚合材料
公开(公告)号：US08383703B2
公开(公告)日：2013-02-26
申请号：US12444839
申请日：2007-10-04
申请人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Oleksandr Kozynchenko
发明人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Oleksandr Kozynchenko
IPC分类号： B01F3/00
CPC分类号： C08F2/18 , C01B32/30 , C01B32/336 , C01B32/342
摘要： A process is provided for producing discrete solid beads of polymeric material e.g. phenolic resin having a mesoporous structure, which process may produce resin beads on an industrial scale without aggregates of resin building up speedily and interrupting production. The process comprises the steps of: (a) combining a stream of a polymerizable liquid precursor e.g. a novolac and hexamine as cross-linking agent dissolved in a first polar organic liquid e.g. ethylene glycol with a stream of a liquid suspension medium which is a second non-polar organic liquid with which the liquid precursor is substantially or completely immiscible e.g. transformer oil containing a drying oil; (b) mixing the combined stream to disperse the polymerizable liquid precursor as droplets in the suspension medium e.g. using an in-line static mixer; (c) allowing the droplets to polymerise in a laminar flow of the suspension medium so as to form discrete solid beads that cannot agglomerate; and (d) recovering the beads from the suspension medium. Also provided is an apparatus for forming discrete solid beads of polymeric material. In other embodiments, a method is provided for carbonizing and activating carbonaceous material, and an externally fired rotary kiln for carbonizing and activating carbonaceous material.
摘要翻译：提供了一种制备聚合物材料的离散固体珠粒的方法，例如具有中孔结构的酚醛树脂，该方法可以在工业规模上生产树脂珠而不会迅速地积聚树脂并中断生产。该方法包括以下步骤：（a）将可聚合液体前体物流如作为溶解在第一极性有机液体中的交联剂的酚醛清漆和六胺作为交联剂。乙二醇与液体悬浮介质物流，液体悬浮介质是第二非极性有机液体，液体前体基本上或完全不混溶。变压器油含有干油; （b）混合组合的流以将可聚合液体前体分散在悬浮介质中的液滴，例如使用在线静态混合器; （c）允许液滴在悬浮介质的层流中聚合，以便形成不能聚集的不连续的固体珠粒; 和（d）从悬浮介质中回收珠粒。还提供了一种用于形成聚合材料的离散固体珠的装置。在其它实施方案中，提供碳化和活化碳质材料的方法，以及用于碳化和活化碳质材料的外部烧制的回转窑。

4. 发明申请

US20100086469A1 Making Discrete Solid Particles of Polymeric Material 有权
标题翻译：制作聚合材料的离散固体颗粒
公开(公告)号：US20100086469A1
公开(公告)日：2010-04-08
申请号：US12444839
申请日：2007-10-04
申请人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Oleksandr Kozynchenko
发明人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Oleksandr Kozynchenko
IPC分类号： C08J3/12 , C08J3/16 , C08F6/00 , C08J9/00 , B01J19/18 , C01B31/02
CPC分类号： C08F2/18 , C01B32/30 , C01B32/336 , C01B32/342
摘要： A process is provided for producing discrete solid beads of polymeric material e.g. phenolic resin having a mesoporous structure, which process may produce resin beads on an industrial scale without aggregates of resin building up speedily and interrupting production. The process comprises the steps of: (a) combining a stream of a polymerizable liquid precursor e.g. a novolac and hexamine as cross-linking agent dissolved in a first polar organic liquid e.g. ethylene glycol with a stream of a liquid suspension medium which is a second non-polar organic liquid with which the liquid precursor is substantially or completely immiscible e.g. transformer oil containing a drying oil; (b) mixing the combined stream to disperse the polymerizable liquid precursor as droplets in the suspension medium e.g. using an in-line static mixer; (c) allowing the droplets to polymerise in a laminar flow of the suspension medium so as to form discrete solid beads that cannot agglomerate; and (d) recovering the beads from the suspension medium. Also provided is an apparatus for forming discrete solid beads of polymeric material. In other embodiments, a method is provided for carbonizing and activating carbonaceous material, and an externally fired rotary kiln for carbonizing and activating carbonaceous material.
摘要翻译：提供了一种制备聚合物材料的离散固体珠粒的方法，例如具有中孔结构的酚醛树脂，该方法可以在工业规模上生产树脂珠而不会迅速地积聚树脂并中断生产。该方法包括以下步骤：（a）将可聚合液体前体物流如作为溶解在第一极性有机液体中的交联剂的酚醛清漆和六胺作为交联剂。乙二醇与液体悬浮介质物流，液体悬浮介质是第二非极性有机液体，液体前体基本上或完全不混溶。变压器油含有干油; （b）混合组合的流以将可聚合液体前体分散在悬浮介质中的液滴，例如使用在线静态混合器; （c）允许液滴在悬浮介质的层流中聚合，以便形成不能聚集的不连续的固体珠粒; 和（d）从悬浮介质中回收珠粒。还提供了一种用于形成聚合材料的离散固体珠的装置。在其它实施方案中，提供了碳化和活化碳质材料的方法，以及用于碳化和活化碳质材料的外部烧制的回转窑。

5. 发明授权

US07655210B2 Porous carbons 有权
公开(公告)号：US07655210B2
公开(公告)日：2010-02-02
申请号：US11800805
申请日：2007-05-07
申请人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
发明人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
IPC分类号： C09C1/44
摘要： A method of making mesoporous carbon beads comprises steps of providing a nucleophilic component such as phenolic compound or phenol condensation prepolymer, dissolving the nucleophilic component in a pore former, together with at least one electrophilic cross-linking agent such as formaldehyde, paraformaldehyde, furfural and hexamethylene tetramine, dispersing the resulting solution into a mineral oil to form beads, condensing both the component and the agent in the presence of the pore former to form beads of porous resin, removing the beads from the mineral oil and carbonizing the beads to form mesoporous carbon beads.

6. 发明授权

US07317871B2 Heater for fluids comprising an electrically conductive porous monolith 失效
标题翻译：包括导电多孔整料的流体加热器
公开(公告)号：US07317871B2
公开(公告)日：2008-01-08
申请号：US10557919
申请日：2004-05-19
申请人： Stephen Robert Tennison , Andrew John Blackburn , Tho Truong Huynh , Piers Catton , Vladimir Strelko, Jr. , Jonathan Robert Tunbridge
发明人： Stephen Robert Tennison , Andrew John Blackburn , Tho Truong Huynh , Piers Catton , Vladimir Strelko, Jr. , Jonathan Robert Tunbridge
IPC分类号： A47J31/00
CPC分类号： H05B3/145
摘要： An electrical heater element of controlled resistivity which can be used for a wide range of applications is formed from an electrically conductive synthetic porous carbon monolith.
摘要翻译：可用于广泛应用的受控电阻率的电加热器元件由导电合成多孔碳整料形成。

7. 发明授权

US4122040A Platinum group metal catalyst 失效
标题翻译：铂族金属催化剂
公开(公告)号：US4122040A
公开(公告)日：1978-10-24
申请号：US725587
申请日：1976-09-22
申请人： John James McCarroll , John Trevor Kent Clark , Stephen Robert Tennison
发明人： John James McCarroll , John Trevor Kent Clark , Stephen Robert Tennison
IPC分类号： B01J21/18 , B01J23/38 , B01J23/40 , B01J23/58 , B01J35/10 , C01B31/00
CPC分类号： B01J35/10 , B01J21/18 , B01J23/38 , B01J23/40 , B01J23/58 , C01B31/00 , B01J35/1019 , C07C2101/12 , C07C2521/18 , C07C2523/02 , C07C2523/04 , C07C2523/42 , C07C2523/46 , C07C2523/58
摘要： Hydrogen transfer catalyst comprises (a) as support a graphite containing carbon having (1) a basal plane surface area of at least 100 m.sup.2 /g, (2) a ratio of BET surface area to basal plane surface area of not more than 5:1 and (3) a ratio of basal plane surface area to edge surface area of at least 5:1 and (b) as active component, 0.01 to 10% by weight, of the total weight of catalyst of a platinum group metal disposed thereon. The catalyst is particularly suitable for reforming.
摘要翻译：氢转移催化剂包括（a）作为载体，含有（1）基面平面表面积至少为100m 2 / g的碳的石墨，（2）BET表面积与基面面积之比不大于5： 1和（3）基面平面表面积与边缘表面积的比例至少为5:1，（b）作为活性组分，其中置于其上的铂族金属催化剂的总重量为0.01至10重量％。催化剂特别适用于重整。

8. 发明授权

US08318373B2 Fuel cell assembly 有权
标题翻译：燃料电池组件
公开(公告)号：US08318373B2
公开(公告)日：2012-11-27
申请号：US12440691
申请日：2007-09-11
申请人： Hanna Katariina Rajantie , Jonathan David Brereton Sharman , David Thompsett , David Emmerson Brown , Stephen Robert Tennison , Beverley Sowerby , Vlad Strelko
发明人： Hanna Katariina Rajantie , Jonathan David Brereton Sharman , David Thompsett , David Emmerson Brown , Stephen Robert Tennison , Beverley Sowerby , Vlad Strelko
IPC分类号： H01M8/10
CPC分类号： H01M8/065 , H01M4/8605 , H01M8/0232 , H01M8/0234 , H01M8/0252 , H01M8/026 , H01M8/0289 , H01M8/1004 , H01M8/1011 , H01M2008/1095 , Y02E60/523
摘要： An MEA comprising: (i) a central first conductive gas diffusion substrate having a first face and a second face; (ii) first and second catalyst layers each having a first and second face and wherein the first face of the first catalyst layer is in contact with the first face of the gas diffusion substrate and the first face of the second catalyst layer is in contact with the second face of the gas diffusion substrate; (iii) first and second electrolyte layers each having a first and second face and wherein the first face of the first electrolyte layer is in contact with the second face of the first catalyst layer and the first face of the second electrolyte layer is in contact with the second face of the second catalyst layer; (iv) third and fourth catalyst layers each having a first and second face and wherein the first face of the third catalyst layer is in contact with the second face of the first electrolyte layer and the first face of the fourth catalyst layer is in contact with the second face of the second electrolyte layer; and (v) first and second porous current collecting means each having a thickness of less than 400 m, and each having a first and second face and wherein the first face of the first current collecting means is in contact with the second face of the third catalyst layer and the first face of the second current collecting means is in contact with the second face of the fourth catalyst layer is disclosed and a fuel cell comprising such an MEA.
摘要翻译：一种MEA，包括：（i）具有第一面和第二面的中心第一导电气体扩散基板; （ii）第一和第二催化剂层，其各自具有第一和第二表面，并且其中第一催化剂层的第一面与气体扩散基板的第一面接触，并且第二催化剂层的第一面与气体扩散基板的第二面; （iii）第一和第二电解质层，每个第一和第二电解质层具有第一和第二表面，并且其中第一电解质层的第一面与第一催化剂层的第二面接触，并且第二电解质层的第一面与第二催化剂层的第二面; （iv）第三和第四催化剂层，其各自具有第一和第二表面，并且其中第三催化剂层的第一面与第一电解质层的第二面接触，并且第四催化剂层的第一面与第二电解质层的第二面; 和（v）第一和第二多孔电流收集装置，每个具有小于400μm的厚度，并且各自具有第一和第二面，并且其中第一集电装置的第一面与第三面的第二面接触催化剂层和第二集电装置的第一面与第四催化剂层的第二面接触，并且包括这样的MEA的燃料电池。

9. 发明授权

US08227518B2 Porous carbons 有权
标题翻译：多孔碳
公开(公告)号：US08227518B2
公开(公告)日：2012-07-24
申请号：US13097819
申请日：2011-04-29
申请人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
发明人： Stephen Robert Tennison , Oleksundr Prokopovych Kozynchenko , Volodymyr Vasyljovych Strelko , Andrew John Blackburn
IPC分类号： C08J9/00 , C08G14/12
CPC分类号： C04B35/524 , C01B32/00 , C01B32/30 , C04B38/0064 , C04B38/009 , C04B2235/77 , Y10T428/24273 , Y10T428/2982 , C04B35/52 , C04B38/0022 , C04B38/0054 , C04B38/062
摘要： A cured porous phenolic resin is provided that can be made by cross-linking a phenol-formaldehyde pre-polymer in the presence of a pore former, preferably ethylene glycol. The resin may be formed in situ by condensing a phenol with or without modifying agents and with cross-linking agent by pouring partially cross-linked resin into hot oil, in which case mesoporous resin beads are obtained. The resulting resin has mesopores observable in carbon derived from said resin by a pore structure of said derived carbon that comprises mesopores of diameter of 20-500 Å, as estimated by nitrogen adsorption porosimentry, the value for the differential of pore volume V with respect to the logarithm of pore radius R (dV/d log R) for the mesopores being greater than 0.2 for at least some values of pore size in the range 20-500 Å. Microporous beads of the resin may be carbonized into mesoporous carbon beads.
摘要翻译：提供了一种固化的多孔酚醛树脂，其可以通过在成孔剂，优选乙二醇的存在下交联苯酚 - 甲醛预聚物来制备。树脂可以通过将苯酚与或不与改性剂和交联剂通过将部分交联的树脂倒入热油中而原位形成，在这种情况下获得介孔树脂珠。所得树脂具有通过所述衍生碳的孔结构可观察到的中孔，所述碳源包括直径为20-500的介孔，如通过氮吸附孔隙度估计的，孔体积V的差异值相对于对于孔径在20-500埃的至少一些值，中孔的孔半径R（dV / d log R）的对数大于0.2。树脂的微孔可以碳化成中孔碳珠。

10. 发明申请

US20100098615A1 Carbonising and/or Activating Carbonaceous Material 有权
公开(公告)号：US20100098615A1
公开(公告)日：2010-04-22
申请号：US12444840
申请日：2007-10-04
申请人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Andrew John Blackburn , Alan Mark Giles
发明人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Andrew John Blackburn , Alan Mark Giles
IPC分类号： C01B31/10 , F27B7/14
CPC分类号： F27B7/167 , C01B32/30 , C01B32/336 , C01B32/342 , C01B32/39 , C08F2/18 , C10B47/30 , C10B53/07 , C10B57/12 , F27B7/162 , Y02P20/143
摘要： A method is provided for carbonizing and activating carbonaceous material, which comprises supplying the material to an externally fired rotary kiln maintained at carbonizing and activating temperatures, the kiln having a downward slope to progress the material as it rotates, the kiln having an atmosphere substantially free of oxygen provided by a counter-current of steam or carbon dioxide, and annular weirs being provided at intervals along the kiln to control progress of the material. There may further be provided an externally fired rotary kiln for carbonizing and activating carbonaceous material having a hollow rotary body that has a downward slope towards a discharge end thereof, and which is provided at intervals along its length with annular weirs for controlling progress of the carbonaceous material. In embodiments, there is also provided a process is for producing discrete solid beads of polymeric material e.g. phenolic resin beads having a mesoporous structure, which may be useful as feedstock for the above mentioned carbonization/activation process or which may have other utility e.g. as ion exchange resins. The process may produce resin beads on an industrial scale without aggregates of resin building up speedily and interrupting production. The process comprises the steps of: (a) combining a stream of a polymerizable liquid precursor e.g. a novolac and hexamine as cross-linking agent dissolved in a first polar organic liquid e.g. ethylene glycol with a stream of a liquid suspension medium which is a second non-polar organic liquid with which the liquid precursor is substantially or completely immiscible e.g. transformer oil containing a drying oil; (b) mixing the combined stream to disperse the polymerizable liquid precursor as droplets in the suspension medium e.g. using an in-line static mixer; (c) allowing the droplets to polymerise in a laminar flow of the suspension medium so as to form discrete solid beads that cannot agglomerate; and (d) recovering the beads from the suspension medium. There is also provided apparatus for forming discrete solid beads of polymeric material, said apparatus comprising: a first line for conveying s stream of a polymerizable liquid precursor; a second line for conveying a stream of a dispersion medium with which the polymerizable liquid precursor is substantially or completely immiscible; an in-line mixer configured to receive a combined flow from the first and second lines and to disperse the polymerizable liquid precursor as droplets in the dispersion medium; a vertical polymerization column configured to receive the dispersion medium with the droplets dispersed therein and to permit the polymerizable liquid precursor polymerize while descending the column in a descending flow of polymerization medium; and a vessel at the base of the column for receiving the descending flow of dispersion medium and collecting polymerized solid beads.

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