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1. 发明授权

US08383703B2 Making discrete solid particles of polymeric material 有权
标题翻译：制成离散固体颗粒的聚合材料
公开(公告)号：US08383703B2
公开(公告)日：2013-02-26
申请号：US12444839
申请日：2007-10-04
申请人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Oleksandr Kozynchenko
发明人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Oleksandr Kozynchenko
IPC分类号： B01F3/00
CPC分类号： C08F2/18 , C01B32/30 , C01B32/336 , C01B32/342
摘要： A process is provided for producing discrete solid beads of polymeric material e.g. phenolic resin having a mesoporous structure, which process may produce resin beads on an industrial scale without aggregates of resin building up speedily and interrupting production. The process comprises the steps of: (a) combining a stream of a polymerizable liquid precursor e.g. a novolac and hexamine as cross-linking agent dissolved in a first polar organic liquid e.g. ethylene glycol with a stream of a liquid suspension medium which is a second non-polar organic liquid with which the liquid precursor is substantially or completely immiscible e.g. transformer oil containing a drying oil; (b) mixing the combined stream to disperse the polymerizable liquid precursor as droplets in the suspension medium e.g. using an in-line static mixer; (c) allowing the droplets to polymerise in a laminar flow of the suspension medium so as to form discrete solid beads that cannot agglomerate; and (d) recovering the beads from the suspension medium. Also provided is an apparatus for forming discrete solid beads of polymeric material. In other embodiments, a method is provided for carbonizing and activating carbonaceous material, and an externally fired rotary kiln for carbonizing and activating carbonaceous material.
摘要翻译：提供了一种制备聚合物材料的离散固体珠粒的方法，例如具有中孔结构的酚醛树脂，该方法可以在工业规模上生产树脂珠而不会迅速地积聚树脂并中断生产。该方法包括以下步骤：（a）将可聚合液体前体物流如作为溶解在第一极性有机液体中的交联剂的酚醛清漆和六胺作为交联剂。乙二醇与液体悬浮介质物流，液体悬浮介质是第二非极性有机液体，液体前体基本上或完全不混溶。变压器油含有干油; （b）混合组合的流以将可聚合液体前体分散在悬浮介质中的液滴，例如使用在线静态混合器; （c）允许液滴在悬浮介质的层流中聚合，以便形成不能聚集的不连续的固体珠粒; 和（d）从悬浮介质中回收珠粒。还提供了一种用于形成聚合材料的离散固体珠的装置。在其它实施方案中，提供碳化和活化碳质材料的方法，以及用于碳化和活化碳质材料的外部烧制的回转窑。

2. 发明申请

US20100086469A1 Making Discrete Solid Particles of Polymeric Material 有权
标题翻译：制作聚合材料的离散固体颗粒
公开(公告)号：US20100086469A1
公开(公告)日：2010-04-08
申请号：US12444839
申请日：2007-10-04
申请人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Oleksandr Kozynchenko
发明人： Stephen Robert Tennison , Jonathan Robert Tunbridge , Roger Nicholas Place , Oleksandr Kozynchenko
IPC分类号： C08J3/12 , C08J3/16 , C08F6/00 , C08J9/00 , B01J19/18 , C01B31/02
CPC分类号： C08F2/18 , C01B32/30 , C01B32/336 , C01B32/342
摘要： A process is provided for producing discrete solid beads of polymeric material e.g. phenolic resin having a mesoporous structure, which process may produce resin beads on an industrial scale without aggregates of resin building up speedily and interrupting production. The process comprises the steps of: (a) combining a stream of a polymerizable liquid precursor e.g. a novolac and hexamine as cross-linking agent dissolved in a first polar organic liquid e.g. ethylene glycol with a stream of a liquid suspension medium which is a second non-polar organic liquid with which the liquid precursor is substantially or completely immiscible e.g. transformer oil containing a drying oil; (b) mixing the combined stream to disperse the polymerizable liquid precursor as droplets in the suspension medium e.g. using an in-line static mixer; (c) allowing the droplets to polymerise in a laminar flow of the suspension medium so as to form discrete solid beads that cannot agglomerate; and (d) recovering the beads from the suspension medium. Also provided is an apparatus for forming discrete solid beads of polymeric material. In other embodiments, a method is provided for carbonizing and activating carbonaceous material, and an externally fired rotary kiln for carbonizing and activating carbonaceous material.
摘要翻译：提供了一种制备聚合物材料的离散固体珠粒的方法，例如具有中孔结构的酚醛树脂，该方法可以在工业规模上生产树脂珠而不会迅速地积聚树脂并中断生产。该方法包括以下步骤：（a）将可聚合液体前体物流如作为溶解在第一极性有机液体中的交联剂的酚醛清漆和六胺作为交联剂。乙二醇与液体悬浮介质物流，液体悬浮介质是第二非极性有机液体，液体前体基本上或完全不混溶。变压器油含有干油; （b）混合组合的流以将可聚合液体前体分散在悬浮介质中的液滴，例如使用在线静态混合器; （c）允许液滴在悬浮介质的层流中聚合，以便形成不能聚集的不连续的固体珠粒; 和（d）从悬浮介质中回收珠粒。还提供了一种用于形成聚合材料的离散固体珠的装置。在其它实施方案中，提供了碳化和活化碳质材料的方法，以及用于碳化和活化碳质材料的外部烧制的回转窑。

3. 发明授权

US09907336B2 Porous carbon materials and smoking articles and smoke filters therefor incorporating such materials 有权
公开(公告)号：US09907336B2
公开(公告)日：2018-03-06
申请号：US11887301
申请日：2006-03-27
申请人： Maria Cashmore , Peter Rex White , Oleksandr Kozynchenko , Andrew Blackburn , Stephen Robert Tennison
发明人： Maria Cashmore , Peter Rex White , Oleksandr Kozynchenko , Andrew Blackburn , Stephen Robert Tennison
IPC分类号： A24B15/28 , A24D3/16 , B01J20/20 , B01J20/28 , C04B38/00 , C04B38/06 , C01B32/30
CPC分类号： A24D3/163 , B01J20/20 , B01J20/28011 , B01J20/28057 , B01J20/28069 , B01J20/28073 , B01J20/28076 , B01J20/2808 , B01J20/28083 , B01J20/28092 , C01B32/30 , C01P2004/51 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , C04B38/009 , C04B38/0615 , C04B35/52 , C04B38/0054 , C04B38/0067
摘要： A porous carbon material suitable for incorporation in smoke filters for cigarettes has a BET surface area of at least 800 m2/g and a pore structure that includes mesopores and micropores. The pore volume (as measured by nitrogen adsorption) is at least 0.9 cm3/g and from 15 to 65% of the pore volume is in mesopores. The pore structure of the material provides a bulk density generally less than 0.5 g/cc. The material may be produced by carbonizing and activating organic resins and may be in the form of beads for ease of handling.

4. 发明申请

US20090038632A1 Porous Carbon Materials and Smoking Articles and Smoke Filters Therefor Incorporating Such Materials 有权
标题翻译：多孔碳材料及其吸烟用品和烟雾过滤器
公开(公告)号：US20090038632A1
公开(公告)日：2009-02-12
申请号：US11887301
申请日：2006-03-27
申请人： Maria Cashmore , Peter Rex White , Oleksandr Kozynchenko , Andrew Blackburn , Stephen Robert Tennison
发明人： Maria Cashmore , Peter Rex White , Oleksandr Kozynchenko , Andrew Blackburn , Stephen Robert Tennison
IPC分类号： A24D3/08 , C08J9/00
CPC分类号： A24D3/163 , B01J20/20 , B01J20/28011 , B01J20/28057 , B01J20/28069 , B01J20/28073 , B01J20/28076 , B01J20/2808 , B01J20/28083 , B01J20/28092 , C01B32/30 , C01P2004/51 , C01P2004/61 , C01P2006/10 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , C04B38/009 , C04B38/0615 , C04B35/52 , C04B38/0054 , C04B38/0067
摘要： A porous carbon material suitable for incorporation in smoke filters for cigarettes has a BET surface area of at least 800 m2/g and a pore structure that includes mesopores and micropores. The pore volume (as measured by nitrogen adsorption) is at least 0.9 cm3/g and from 15 to 65% of the pore volume is in mesopores. The pore structure of the material provides a bulk density generally less than 0.5 g/cc. The material may be produced by carbonising and activating organic resins and may be in the form of beads for ease of handling.
摘要翻译：适用于掺入香烟烟雾过滤器的多孔碳材料具有至少800m 2 / g的BET表面积和包括中孔和微孔的孔结构。孔体积（通过氮吸附测量）为至少0.9cm 3 / g，孔体积的15至65％在中孔中。材料的孔结构提供通常小于0.5g / cc的堆积密度。该材料可以通过碳化和活化有机树脂来生产，并且可以是珠子的形式以便于处理。

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