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1. 发明授权

US5488168A Tertiary amino alcohol and method of producing the same 失效
标题翻译：三氨基醇及其制备方法
公开(公告)号：US5488168A
公开(公告)日：1996-01-30
申请号：US46924
申请日：1993-04-14
申请人： Kohshiro Sotoya , Hiroshi Abe , Jun Aikawa , Hideki Taniguchi , Uichiro Nishimoto
发明人： Kohshiro Sotoya , Hiroshi Abe , Jun Aikawa , Hideki Taniguchi , Uichiro Nishimoto
IPC分类号： C07D295/08 , B01F17/00 , B01J23/89 , C07B61/00 , C07C213/00 , C07C215/02 , C07C215/14 , C07C215/20 , C07C217/08 , C07D295/088 , C07D295/13 , C10M133/08 , C10M149/22 , C07C215/08
CPC分类号： C07D295/13 , B01F17/0042 , B01F17/005 , C07C215/14 , C07C217/08 , C07D295/088 , C10M133/08 , C10M149/22 , C10M2215/042
摘要： A tertiary amino alcohol, being useful as an emulsifier, is defined by the formula (1) or (2): ##STR1## where R is a C.sub.2 to C.sub.24 straight-chain or branched alkylene group, an alicyclic alkylene group, an aralkylene group or --CH.sub.2 CH.sub.2 O).sub.p (CH.sub.2 CH.sub.2).sub.q (where p is 0 or a positive integer and q is a positive integer), R' is a C.sub.1 to C.sub.24 straight-chain or branched alkyl group or an aralkyl group and n is a positive integer of 2 to 50.
摘要翻译：用作乳化剂的叔氨基醇由式（1）或（2）定义：其中R是C 2至C 24直链或支链亚烷基，脂环族亚烷基，亚芳基或-CH 2 CH 2 O）p（CH 2 CH 2）q（其中p为0或正整数，q为正整数），R'为C 1至C 24直链或支链烷基或芳烷基，n为2〜50的正整数。

2. 发明授权

US5132425A Quaternary ammonium compounds 失效
标题翻译：季铵化合物
公开(公告)号：US5132425A
公开(公告)日：1992-07-21
申请号：US646314
申请日：1991-01-28
申请人： Kohshiro Sotoya , Uichiro Nishimoto , Hiroshi Abe
发明人： Kohshiro Sotoya , Uichiro Nishimoto , Hiroshi Abe
IPC分类号： A61K8/00 , A61K8/40 , A61Q5/00 , C07C215/40 , C07C215/42 , C07C217/42 , C07C245/04 , C07D295/088 , C11D1/62 , D06M13/02 , D06M13/322 , D06M13/46 , D06M13/467 , D06M13/47 , D06M13/477 , D06M101/12
CPC分类号： C07D295/088 , C07C215/40 , Y10S516/07
摘要： Novel quaternary ammonium compounds of formula (1) and (2): ##STR1## wherein R represents a straight or branched alkylene group containing from 2 to 24 carbon atoms, an alicyclic alkylene group, an aralkylene group or a group of the formula --CH.sub.2 CH.sub.2 O).sub.p (CH.sub.2 CH.sub.2).sub.q (in which p and q each represents a positive integer), R' represents a straight or branched alkyl group containing from 1 to 24 carbon atoms, an alkenyl group or an aralkyl group, R" represents an alkyl group containing 1 to 5 carbon atoms or an aralkyl group, X.sup.- represents an anionic group and n represents a positive integer of from 2 to 50 are disclosed. The quaternary ammonium compounds are useful as surfactants capable of serving as softening agents and antistatic agents for fabrics, hair and the like.

3. 发明授权

US5296631A Process for producing N-alkyl-N-methylamine or N-alkenyl-N-methylamine 失效
标题翻译：制备N-烷基-N-甲胺或N-链烯基-N-甲胺的方法
公开(公告)号：US5296631A
公开(公告)日：1994-03-22
申请号：US871541
申请日：1992-04-21
申请人： Hiroshi Abe , Hideki Taniguchi , Yoshifumi Nishimoto , Kohshiro Sotoya
发明人： Hiroshi Abe , Hideki Taniguchi , Yoshifumi Nishimoto , Kohshiro Sotoya
IPC分类号： B01J29/068 , C07C209/16
CPC分类号： B01J29/068 , C07C209/16
摘要： A process for producing an N-alkyl-N-methylamine or an N-alkenyl-N-methylamine in a high yield from a higher alcohol and methylamine comprising the step of reacting a higher alcohol with methylamine in the presence of a catalyst comprising copper and a fourth period transition metal of the Periodic Table, except for chromium, or a catalyst comprising copper, a fourth period transition metal of the Periodic Table, except for chromium, and an element of the platinum group VIII of the Periodic Table, at a pressure ranging from atmospheric pressure to 100 atm. G., at a reaction temperature ranging from 100.degree. to 250.degree. C., with hydrogen gas being introduced into the reaction system while water produced in the reaction is removed from the reaction system and the amount of methylamine in the gaseous mixture which contains no matter formed through the reaction and is exhausted from the reaction system is regulated from 5 to 50% by volume.
摘要翻译：一种从高级醇和甲胺以高产率生产N-烷基-N-甲基胺或N-链烯基-N-甲基胺的方法，包括在含有铜的催化剂存在下使高级醇与甲胺反应的步骤，元素周期表的第四周期过渡金属，除了铬，或包含铜的催化剂，除了铬以外的元素周期表的第四周期过渡金属和周期表的第Ⅷ族元素的压力从大气压到100大气压。 G.在100℃至250℃的反应温度下，将氢气引入反应体系中，同时从反应体系中除去反应产生的水和不含有气体混合物的甲胺的量通过反应形成的并从反应体系中排出的物质的量为5〜50体积％。

4. 发明授权

US5266730A Process for preparing N-substituted amine 失效
标题翻译：制备N-取代胺的方法
公开(公告)号：US5266730A
公开(公告)日：1993-11-30
申请号：US529928
申请日：1990-05-29
申请人： Hiroshi Abe , Jun Aikawa , Kazuhiko Okabe , Kohshiro Sotoya
发明人： Hiroshi Abe , Jun Aikawa , Kazuhiko Okabe , Kohshiro Sotoya
IPC分类号： B01J23/76 , B01J23/89 , C07C209/16 , C07C209/26 , C07C209/02 , C07C209/04
CPC分类号： B01J23/8926 , B01J23/76 , B01J23/8933 , B01J23/8946 , B01J23/8986 , B01J23/8993 , C07C209/16 , C07C209/26
摘要： An N-substituted amine is produced by reacting an alcohol or aldehyde with ammonia, a primary amine or a secondary amine in the presence of a catalyst comprising:(a) (1) copper, (2) a metal selected from the group consisting of chromium, manganese, iron and zinc and (3) a metal of the platinum VIII group;(b) (1) copper, (2) cobalt and (3) a metal of the platinum VIII group;(c) (1) copper, (2) a metal selected from the group consisting of chromium, manganese, iron, cobalt, nickel and zinc, (3) a metal of the platinum VIII group and (4) a metal selected from the group consisting of alkali metals and alkaline earth metals; or(d) (1) copper, (2) a metal selected from the group consisting of chromium, manganese, iron, cobalt, nickel and zinc, (3) a metal of the platinum VIII group and (4) a metal selected from the group consisting of aluminum, tungsten and molybdenum.
摘要翻译：通过使醇或醛与氨，伯胺或仲胺在催化剂存在下反应制备N-取代的胺，所述催化剂包含：（a）（1）铜，（2）选自以下的金属：铬，锰，铁和锌和（3）铂VIII族金属; （b）（1）铜，（2）钴和（3）铂VIII族金属; （c）（1）铜，（2）选自铬，锰，铁，钴，镍和锌的金属，（3）铂VIII族金属和（4）由碱金属和碱土金属组成的组; 或（d）（1）铜，（2）选自铬，锰，铁，钴，镍和锌的金属，（3）铂VIII族金属和（4）该组由铝，钨和钼组成。

5. 发明授权

US5444099A Tertiary aminoalcohol ane process for producing the same, and, polyurethane and process for producing the same 失效
标题翻译：用于制备其的三氨基醇肛门方法，以及聚氨酯及其制备方法
公开(公告)号：US5444099A
公开(公告)日：1995-08-22
申请号：US123165
申请日：1993-09-20
申请人： Hiroshi Abe , Tetsuaki Fukushima , Kohshiro Sotoya , Shoichiro Harada , Hiroshi Kitagawa , Masayoshi Morii , Yasutoshi Isayama
发明人： Hiroshi Abe , Tetsuaki Fukushima , Kohshiro Sotoya , Shoichiro Harada , Hiroshi Kitagawa , Masayoshi Morii , Yasutoshi Isayama
IPC分类号： C07C215/14 , C07C217/08 , C08G18/32 , C08G18/64 , C08G18/66 , C08G73/02 , C07C215/02 , C08G18/00
CPC分类号： C08G73/024 , C07C215/14 , C07C217/08 , C08G18/3275 , C08G18/6423 , C08G18/6688 , C08G73/02 , C08G73/0206 , C08G2101/00
摘要： A tertiary aminoalcohol having a tert-amino group(s) in the main chain and hydroxyl groups at the terminals. The use of this compound for purposes different from that of ordinary amines and amine derivatives is expected.A process for producing the tertiary aminoalcohol wherein a catalyst comprising copper, a transition metal element of the fourth period and a platinum group element of the group VIII, and further optionally containing an alkali metal or an alkaline earth metal is used.A process for producing polyurethane using the above-mentioned tertiary aminoalcohol which can solve the problems occurring in the production of a polyurethane using a tertiary amine which has a strong irritating odor and is highly irritant to the skin as a catalyst, for example, deteriorations of working atmosphere and sales appeal of the polyurethane.The chemical structure of the above-described tertiary aminoalcohol is as follows: ##STR1##
摘要翻译：在主链中具有叔氨基和末端具有羟基的叔氨基醇。期望使用该化合物用于与普通胺和胺衍生物不同的目的。一种制备叔氨基醇的方法，其中使用包含铜的催化剂，第四阶段的过渡金属元素和VIII族的铂族元素，以及进一步任选含有碱金属或碱土金属的催化剂。使用上述叔氨基醇制造聚氨酯的方法，其可以使用具有强烈刺激性气味并且对皮肤高度刺激性的叔胺作为催化剂来解决在制备聚氨酯中发生的问题，例如，劣化工作气氛和聚氨酯的销售吸引力。上述叔氨基醇的化学结构如下：（I）

6. 发明授权

US5315041A Tertiary aminoalcohol and process for producing the same, and, polyurethane and process for producing the same 失效
标题翻译：三氨基醇及其制备方法，以及聚氨酯及其制备方法
公开(公告)号：US5315041A
公开(公告)日：1994-05-24
申请号：US845594
申请日：1992-03-04
申请人： Hiroshi Abe , Tetsuaki Fukushima , Kohshiro Sotoya , Shoichiro Harada , Hiroshi Kitagawa , Masayoshi Morii , Yasutoshi Isayama
发明人： Hiroshi Abe , Tetsuaki Fukushima , Kohshiro Sotoya , Shoichiro Harada , Hiroshi Kitagawa , Masayoshi Morii , Yasutoshi Isayama
IPC分类号： C07C215/14 , C07C217/08 , C08G18/32 , C08G18/64 , C08G18/66 , C08G73/02 , C07C215/02
CPC分类号： C08G73/024 , C07C215/14 , C07C217/08 , C08G18/3275 , C08G18/6423 , C08G18/6688 , C08G73/02 , C08G73/0206 , C08G2101/00
摘要： A tertiary aminoalcohol having a tert-amino group(s) in the main chain and hydroxyl groups at the terminals. The use of this compound for purposes different from that of ordinary amines and amine derivatives is expected.A process for producing the tertiary aminoalcohol wherein a catalyst comprising copper, a transition metal element of the fourth period and a platinum group element of the group VIII, and further optionally containing an alkali metal or an alkaline earth metal is used.A process for producing polyurethane using the above-mentioned tertiary aminoalcohol which can solve the problems occurring in the production of a polyurethane using a tertiary amine which has a strong irritating odor and is highly irritant to the skin as a catalyst, for example, deteriorations of working atmosphere and sales appeal of the polyurethane.The chemical structure of the above-described tertiary aminoalcohol is as follows: ##STR1##
摘要翻译：在主链中具有叔氨基和末端具有羟基的叔氨基醇。期望使用该化合物用于与普通胺和胺衍生物不同的目的。一种制备叔氨基醇的方法，其中使用包含铜的催化剂，第四阶段的过渡金属元素和VIII族的铂族元素，以及进一步任选含有碱金属或碱土金属的催化剂。使用上述叔氨基醇制造聚氨酯的方法，其可以使用具有强烈刺激性气味并且对皮肤高度刺激性的叔胺作为催化剂来解决在制备聚氨酯中发生的问题，例如，劣化工作气氛和聚氨酯的销售吸引力。上述叔氨基醇的化学结构如下：（I）

7. 发明授权

US5097073A Production of aliphatic primary of secondary amine 失效
标题翻译：生产二级胺的主要原料
公开(公告)号：US5097073A
公开(公告)日：1992-03-17
申请号：US713835
申请日：1991-06-12
申请人： Hiroshi Abe , Tohru Katoh , Hisakazu Tajima , Kohshiro Sotoya
发明人： Hiroshi Abe , Tohru Katoh , Hisakazu Tajima , Kohshiro Sotoya
IPC分类号： B01J23/89 , C07C209/48
CPC分类号： B01J23/8926 , B01J23/8933 , C07C209/48
摘要： Disclosed is a process for preparing an unsaturated aliphatic primary or secondary amine from the corresponding unsaturated aliphatic nitrile without hydrogenating an olefinic bond in the molecule. The process employs a catalyst which is a combination of copper and a specific metal.

8. 发明授权

US06737050B2 Hair cosmetic compositions 有权
标题翻译：头发化妆品组合物
公开(公告)号：US06737050B2
公开(公告)日：2004-05-18
申请号：US10026641
申请日：2001-12-27
申请人： Yasuhiro Doi , Keiko Hasebe , Hiroyuki Masuda , Tetsuaki Fukushima , Uichiro Nishimoto , Hiroshi Abe
发明人： Yasuhiro Doi , Keiko Hasebe , Hiroyuki Masuda , Tetsuaki Fukushima , Uichiro Nishimoto , Hiroshi Abe
IPC分类号： A61K7075
CPC分类号： A61K8/898 , A61K8/416 , A61K8/44 , A61K8/463 , A61K8/60 , A61K8/73 , A61K8/891 , A61Q5/00 , A61Q5/02 , A61Q5/12
摘要： Provided are a hair cosmetic composition comprising an ether type cationic surfactant represented by the following formula (1): wherein, R1 represents a linear or branched C6-24 alkyl or alkenyl group, R2 and R4 each represents a C1-6 alkyl group or —(AO)nH (A: a C2-4 alkylene group, n: a number of from 1 to 6 with the proviso that n pieces of A may be the same or different and their sequence is optional), R3 represents a C1-6 alkyl group or —(A′O)mH (A′: a C2-4 alkylene group, m: a number of from 1 to 6 with the proviso that m pieces of A may be the same or different and their sequence is optional), and X− represents an anion; a hair cleansing composition containing the cationic surfactant(1); and a method of treating hair with these compositions. The hair cosmetic composition of the present invention can impart good flexibility and smoothness to hair not only when it is wetted but also after drying. When used as a hair cleansing composition, it provides excellent quality of foam and feeling upon use and exhibits good low-temperature stability.
摘要翻译：提供一种包含由下式（1）表示的醚型阳离子表面活性剂的毛发化妆品组合物：其中，R 1表示直链或支链的C 6-24烷基或链烯基，R 2和R 4各自表示C 1-6烷基或 - （AO）n H（A：C 2-4亚烷基，n：1至6的数，条件是n个A可以相同或不同，它们的顺序为可选），R 3表示C 1-6烷基或 - （A'O）m H（A'：C 2-4亚烷基，m：1至6的数，条件是m个A 可以相同或不同，它们的顺序是任选的），而X“表示阴离子; 含有阳离子表面活性剂（1）的毛发清洁组合物; 以及使用这些组合物处理毛发的方法。本发明的毛发化妆品组合物可以赋予头发良好的柔韧性和光滑性，不仅当其被润湿时，而且在干燥之后。当用作头发清洁组合物时，它提供优异的泡沫质量和使用感，并表现出良好的低温稳定性。

9. 发明授权

US06576794B2 Process for production of ether amine 有权
标题翻译：醚胺生产工艺
公开(公告)号：US06576794B2
公开(公告)日：2003-06-10
申请号：US10015657
申请日：2001-12-17
申请人： Tetsuaki Fukushima , Hiroyuki Masuda , Uichiro Nishimoto , Hiroshi Abe
发明人： Tetsuaki Fukushima , Hiroyuki Masuda , Uichiro Nishimoto , Hiroshi Abe
IPC分类号： C07C25330
CPC分类号： C07C253/30 , C07C213/02 , C07C255/13 , C07C217/08
摘要： A process for producing an ether amine (3), which comprises reacting a primary or secondary alcohol (1), ROH, with acrylonitrile in an amount of 0.8 to 1.2 equivalents of the alcohol (1) in the presence of an alkali metal hydroxide in an amount of not less than 0.01 part by weight, but less than 0.05 part by weight per 100 parts by weight of the alcohol (1) to obtain an alkyloxypropionitrile (2), and then adding water to the reaction system without removing the alkali metal hydroxide therefrom and effecting hydrogenation using a hydrogenation catalyst: ROH(1)+CH2=CHCN→ROCH2CH2CN(2)→ROCH2CH2CH2NH2(3) wherein R denotes a linear or branched alkyl or alkenyl group having 6 to 24 carbon atoms. Also disclosed are a process for producing an ether tertiary amine (5), R—O—CH2—CH2—CH2—N(CH2R1)2, which comprises adding an aldehyde to the resulting ether amine (3) in the presence of a metal catalyst or a Raney nickel catalyst, and a process for producing an ether quaternary ammonium salt (6), R—O—CH2—CH2—CH2—N(CH2R1)2(R2), which comprises reacting a quaternizing agent with the ether tertiary amine (5).
摘要翻译：一种制备醚胺（3）的方法，其包括在碱金属氢氧化物存在下，将伯醇或仲醇（1），ROH与丙烯腈的量为0.8至1.2当量的醇（1）相对于每100重量份的醇（1），不少于0.01重量份，但小于0.05重量份，得到烷氧基丙腈（2），然后向反应体系中加入水而不除去碱金属使用氢化催化剂氢化，其中R表示碳原子数为6〜24的直链或支链烷基或链烯基。还公开了制备醚叔胺（5），RO-CH2-CH2-CH2-N（CH2R1）2的方法，其包括在金属催化剂存在下将醛加到得到的醚胺（3）中，或阮内镍催化剂和制备醚季铵盐（6），RO-CH2-CH2-CH2-N（CH2R1）2（R2）的方法，其包括使季铵化剂与醚叔胺（5）反应，。

10. 发明授权

US5703264A Process for producing aliphatic nitrile 失效
标题翻译：生产脂族腈的方法
公开(公告)号：US5703264A
公开(公告)日：1997-12-30
申请号：US670787
申请日：1996-06-24
申请人： Wataru Yoshida , Tetsuaki Fukushima , Hideki Taniguchi , Hiroshi Abe
发明人： Wataru Yoshida , Tetsuaki Fukushima , Hideki Taniguchi , Hiroshi Abe
IPC分类号： B01J23/89 , C07B61/00 , C07C253/00 , C07C255/03
CPC分类号： B01J23/8933 , B01J23/8926 , C07C253/00
摘要： The process for producing an aliphatic nitrile comprising reacting an aliphatic alcohol having 6 to 40 carbon atoms with ammonia (a) in the presence of a copper/transition metal element in the fourth period other than Cr/platinum group element in the eighth group catalyst, (b) under a reaction system pressure in the range of from atmospheric pressure to 100 atm, (c) at a reaction system temperature in the range of from 100.degree. to 250.degree. C., (d) while introducing at least one gas selected from the group consisting of inert gases and hydrogen gas into the reaction system, (e) removing water formed by the reaction out of the reaction system, and (f) controlling the amount of the ammonia contained in the gas (exclusive of the water formed by the reaction) discharged out of the reaction system to 5 to 50% by volume based on the volume of the gas discharged (exclusive of the water formed by the reaction) makes it possible to produce various kinds of aliphatic nitriles.
摘要翻译：在第八组催化剂中除了Cr /铂族元素以外的第四期间，在铜/过渡金属元素的存在下，使具有6〜40个碳原子的脂肪醇与氨（a）反应的方法，（b）在大气压至100大气压范围内的反应体系压力下，（c）反应体系温度为100-250℃，（d）同时引入至少一种选择的气体从由惰性气体和氢气组成的组中进入反应体系，（e）将由反应形成的水除去反应体系，和（f）控制气体中所含的氨的量（不包括形成的水通过反应）从排出的气体的体积（不包括由反应形成的水）排出反应体系的5〜50体积％使得可以生产各种脂族腈。

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