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1. 发明申请

US20090292145A1 METHOD OF PRODUCING NITROGEN-CONTAINING COMPOUND 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：US20090292145A1
公开(公告)日：2009-11-26
申请号：US12520739
申请日：2007-10-17
申请人： Tetsuaki Fukushima , Hideki Taniguchi , Michio Terasaka
发明人： Tetsuaki Fukushima , Hideki Taniguchi , Michio Terasaka
IPC分类号： C07C209/50
CPC分类号： C07C209/50 , B01J21/10 , B01J23/002 , B01J23/78 , B01J23/80 , B01J23/8926 , B01J23/8946 , B01J29/06 , B01J29/072 , B01J29/143 , B01J37/03 , B01J2523/00 , C07C211/08 , B01J2523/17 , B01J2523/22 , B01J2523/23 , B01J2523/25 , B01J2523/824 , B01J2523/27
摘要： The present invention provides a process for producing high-purity aliphatic tertiary amines containing a less amount of by-products by using a chromium-free catalyst with a good productivity in an economically advantageous manner. The present invention relates to a process for producing a tertiary amine by reducing an amide compound in the presence of a catalyst containing copper and magnesium at a molar ratio of magnesium to copper (magnesium/copper) of from 0.01 to 20.
摘要翻译：本发明提供一种以经济上有利的方式通过使用无铬催化剂以高生产率生产含少量副产物的高纯度脂族叔胺的方法。本发明涉及一种通过在含有铜与镁（镁/铜）摩尔比为0.01〜20的铜和镁的催化剂存在下还原酰胺化合物来制备叔胺的方法。

2. 发明授权

US07259274B2 Method of producing aliphatic nitrile 失效
标题翻译：生产脂族腈的方法
公开(公告)号：US07259274B2
公开(公告)日：2007-08-21
申请号：US10936745
申请日：2004-09-09
申请人： Michio Terasaka , Tetsuaki Fukushima
发明人： Michio Terasaka , Tetsuaki Fukushima
IPC分类号： C07C253/00 , C07C63/30
CPC分类号： B01J21/08 , B01J35/1019 , B01J37/03 , C07C253/22 , C07C255/03
摘要： An aliphatic nitrile is prepared by a process of reacting an aliphatic carboxylic acid, an aliphatic dicarboxylic acid or an alkyl ester thereof, wherein the alkyl group has 1 to 5 carbon atoms, with ammonia in the presence of a catalyst of titanium oxide supported on solid silica.
摘要翻译：通过使负载在固体上的氧化钛催化剂的存在下使氨基在其中烷基具有1至5个碳原子的脂族羧酸，脂族二羧酸或其烷基酯与氨反应来制备脂族腈二氧化硅。

3. 发明申请

US20070149817A1 PROCESS FOR PRODUCING NITROGEN-CONTAINING COMPOUNDS 失效
标题翻译：生产含氮化合物的方法
公开(公告)号：US20070149817A1
公开(公告)日：2007-06-28
申请号：US11614404
申请日：2006-12-21
申请人： Tetsuaki FUKUSHIMA , Masaharu Jono , Michio Terasaka
发明人： Tetsuaki FUKUSHIMA , Masaharu Jono , Michio Terasaka
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , C07C211/07
摘要： The present invention relates to a process for producing an aliphatic amine, including the step of contacting a linear or branched, or cyclic aliphatic alcohol with ammonia and hydrogen in the presence of a catalyst containing (A) nickel, copper and zirconium components, and (B) at least one metal component selected from the group consisting of elements belonging to Group 3 of the Periodic Table, elements belonging to Group 5 of the Periodic Table and platinum group elements. According to the process of the present invention, an aliphatic primary amine can be produced from an aliphatic alcohol with a high selectivity.
摘要翻译：本发明涉及一种生产脂肪族胺的方法，包括在含有（A）镍，铜和锆组分的催化剂和（A）镍，铜和锆组分的催化剂存在下，使直链或支链或环状脂族醇与氨和氢接触的步骤和（ B）选自元素周期表第3族元素，元素周期表第5族元素和铂族元素中的至少一种金属成分。根据本发明的方法，脂肪族伯胺可以以高选择性由脂族醇生产。

4. 发明申请

US20120123170A1 METHOD FOR PRODUCING NONIONIC SURFACTANT 审中-公开
标题翻译：生产非离子表面活性剂的方法
公开(公告)号：US20120123170A1
公开(公告)日：2012-05-17
申请号：US13383418
申请日：2010-08-03
申请人： Keisuke Chiba , Yoshifumi Nishimoto , Tetsuaki Fukushima , Satoru Kijima
发明人： Keisuke Chiba , Yoshifumi Nishimoto , Tetsuaki Fukushima , Satoru Kijima
IPC分类号： C07C41/03
CPC分类号： C08G65/2609 , C08G65/2696
摘要： The present invention relates to the method for producing a nonionic surfactant, including the step (I) of reacting alcohol having a water content of not more than 0.1% by mass with ethylene oxide to obtain ethylene oxide-adduct, the step (II) of reacting the ethylene oxide-adduct with propylene oxide to obtain the alkylene oxide-adduct having a content of remaining propylene oxide of not more than 1000 mg/kg, and the step (III) of reacting the alkylene oxide-adduct with ethylene oxide to obtain the nonionic surfactant having each content of remaining ethylene oxide and remaining propylene oxide of not more than 5 mg/kg.
摘要翻译：本发明涉及非水性表面活性剂的制造方法，其包括将水含量为0.1质量％以下的醇与环氧乙烷反应的工序（I），得到环氧乙烷加合物，步骤（II）使环氧乙烷加成物与环氧丙烷反应，得到残留环氧丙烷含量为1000mg / kg以下的环氧烷 - 加成物，和使烯化氧加成物与环氧乙烷反应的工序（III），得到每个残留环氧乙烷和剩余环氧丙烷含量不大于5mg / kg的非离子表面活性剂。

5. 发明申请

US20110266496A1 SURFACTANT COMPOSITION 审中-公开
标题翻译：表面活性剂组合物
公开(公告)号：US20110266496A1
公开(公告)日：2011-11-03
申请号：US13142063
申请日：2009-12-25
申请人： Yoshinori Mitsuda , Takeshi Tomifuji , Tetsuaki Fukushima
发明人： Yoshinori Mitsuda , Takeshi Tomifuji , Tetsuaki Fukushima
IPC分类号： C09K3/00
CPC分类号： C11D1/29 , A61K8/34 , A61K8/463 , A61Q19/10 , C11D3/044 , C11D3/2006
摘要： The present invention provides a surfactant composition containing (a) 40 to 58% by mass of specific polyoxyalkylene alkyl ether sulfate ester salt having a structure formed by addition of propylene oxide, (b) 13 to 20% by mass of alcohol having 1 to 6 carbon atoms, (c) 0.002 to 0.5% by mass of alkaline agent, and water.
摘要翻译：本发明提供一种表面活性剂组合物，其含有（a）40〜58质量％的具有通过添加环氧丙烷形成的结构的特定的聚氧化烯烷基醚硫酸酯盐，（b）13〜20质量％的具有1〜6个碳原子，（c）0.002〜0.5质量％的碱性试剂和水。

6. 发明申请

US20110207964A1 PROCESS FOR PRODUCING NITROGEN-CONTAINING COMPOUNDS 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：US20110207964A1
公开(公告)日：2011-08-25
申请号：US12672327
申请日：2008-08-07
申请人： Michio Terasaka , Tetsuaki Fukushima , Hideki Taniguchi , Masaharu Jono
发明人： Michio Terasaka , Tetsuaki Fukushima , Hideki Taniguchi , Masaharu Jono
IPC分类号： C07C291/04 , C07C209/50
CPC分类号： C07C209/50 , C07C209/02 , C07C211/08 , C07C291/04
摘要： The present invention relates to a process for producing a tertiary amine in the presence of a catalyst containing copper and at least one element selected from the group consisting of elements belonging to Groups 2, 3, 7 and 12 of the Periodic Table (long form of the periodic table), said process including the steps of (a) reducing an amide compound in a hydrogen atmosphere; and (b) introducing a dialkyl amine containing a linear or branched alkyl group having 1 to 6 carbon atoms into a reaction product obtained in the step (a), and treating the reaction product with the dialkyl amine. The present invention provides a process for producing high-purity aliphatic tertiary amines containing a less amount of by-products by reducing aliphatic acid amides under moderate conditions using a chromium-free catalyst, as well as a process for producing amine derivatives such as amine oxide by using the aliphatic tertiary amines, with a good productivity in an economical manner.
摘要翻译：本发明涉及在含有铜的催化剂和选自元素周期表第2,3,7和12族元素中的至少一种元素的存在下制备叔胺的方法（长形式所述方法包括以下步骤：（a）在氢气氛中还原酰胺化合物; 和（b）将含有具有1至6个碳原子的直链或支链烷基的二烷基胺引入步骤（a）中获得的反应产物中，并用二烷基胺处理反应产物。本发明提供了一种通过使用无铬催化剂在中等条件下还原脂肪酸酰胺以及生产胺衍生物如氧化胺的方法来生产含有少量副产物的高纯度脂族叔胺的方法通过使用脂肪族叔胺，以经济的方式具有良好的生产率。

7. 发明申请

US20100274056A1 PROCESS FOR PRODUCING NITROGEN-CONTAINING COMPOUNDS 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：US20100274056A1
公开(公告)日：2010-10-28
申请号：US12159526
申请日：2006-12-21
申请人： Tetsuaki Fukushima , Masaharu Jono , Michio Terasaka
发明人： Tetsuaki Fukushima , Masaharu Jono , Michio Terasaka
IPC分类号： C07C209/14 , B01J23/46 , B01J23/30 , B01J23/10
CPC分类号： B01J23/462 , B01J23/6527 , B01J23/892 , B01J29/068 , B01J37/033 , B01J37/035 , C07C209/16
摘要： The present invention relates to a process for producing an aliphatic amine, comprising the step of contacting a linear or branched, or cyclic aliphatic alcohol having 6 to 22 carbon atoms with ammonia and hydrogen in the presence of a catalyst formed by supporting at least (A) a ruthenium component produced by hydrolysis of a ruthenium compound on a carrier, or by further supporting, in addition to the component (A), a specific second metal component or a specific third metal component on the carrier. According to the process of the present invention, an aliphatic primary amine can be produced from an aliphatic alcohol with a high catalytic activity and a high selectivity.
摘要翻译：本发明涉及脂肪族胺的制造方法，其特征在于，在使至少含有（A）成分的催化剂存在下，使具有6〜22个碳原子的直链或支链或环状脂肪醇与氨和氢接触的工序）通过在载体上水解钌化合物而制备的钌组分，或者除了组分（A）之外还可以在载体上具有特定的第二金属组分或特定的第三金属组分。根据本发明的方法，脂肪族伯胺可以由具有高催化活性和高选择性的脂族醇生产。

8. 发明授权

US07713341B2 Quaternary ammonium salt compositions 有权
标题翻译：季铵盐组合物
公开(公告)号：US07713341B2
公开(公告)日：2010-05-11
申请号：US12078690
申请日：2008-04-03
申请人： Katsuhisa Inoue , Hidehito Ikebata , Kazuhiko Kurita , Tetsuaki Fukushima , Tadayuki Suzuki
发明人： Katsuhisa Inoue , Hidehito Ikebata , Kazuhiko Kurita , Tetsuaki Fukushima , Tadayuki Suzuki
IPC分类号： A01N33/12 , A01N33/02 , B27K3/34 , B27K3/50 , B27K3/00
CPC分类号： C07C217/08 , A01N33/12 , A01N33/02 , A01N33/04 , A01N37/02 , A01N2300/00
摘要： The present invention relates to a quaternary ammonium salt composition containing (a) a quaternary ammonium salt represented by the following general formula (1), (b) a specific tertiary amine and (c) an organic acid ester in specific mass ratios which is excellent in hue and storage stability, a process for producing the quaternary ammonium salt composition, and a wood preservative containing the quaternary ammonium salt composition. wherein R1 is an alkyl or alkenyl group; R2 is an alkyl, alkenyl or hydroxyalkyl group; R3 is an alkyl or hydroxyalkyl group; R4 is an alkylene group; n is a number of from 1 to 5; and A is a counter ion derived from sulfonic acid, etc.
摘要翻译：本发明涉及一种季铵盐组合物，其含有（a）由以下通式（1）表示的季铵盐，（b）特定的叔胺和（c）特定质量比的有机酸酯，其优异在色调和储存稳定性方面，制备季铵盐组合物的方法和含有季铵盐组合物的木材防腐剂。其中R1是烷基或烯基; R2是烷基，烯基或羟烷基; R3是烷基或羟烷基; R4是亚烷基; n是从1到5的数字; 而A是衍生自磺酸等的抗衡离子

9. 发明授权

US07514585B2 Process for producing nitrogen-containing compounds 失效
标题翻译：含氮化合物的制造方法
公开(公告)号：US07514585B2
公开(公告)日：2009-04-07
申请号：US11614404
申请日：2006-12-21
申请人： Tetsuaki Fukushima , Masaharu Jono , Michio Terasaka
发明人： Tetsuaki Fukushima , Masaharu Jono , Michio Terasaka
IPC分类号： C07C209/16 , B01J21/00
CPC分类号： C07C209/16 , C07C211/07
摘要： The present invention relates to a process for producing an aliphatic amine, including the step of contacting a linear or branched, or cyclic aliphatic alcohol with ammonia and hydrogen in the presence of a catalyst containing (A) nickel, copper and zirconium components, and (B) at least one metal component selected from the group consisting of elements belonging to Group 3 of the Periodic Table, elements belonging to Group 5 of the Periodic Table and platinum group elements. According to the process of the present invention, an aliphatic primary amine can be produced from an aliphatic alcohol with a high selectivity.
摘要翻译：本发明涉及一种生产脂肪族胺的方法，包括在含有（A）镍，铜和锆组分的催化剂和（A）镍，铜和锆组分的催化剂存在下，使直链或支链或环状脂族醇与氨和氢接触的步骤和（ B）选自元素周期表第3族元素，元素周期表第5族元素和铂族元素中的至少一种金属成分。根据本发明的方法，脂肪族伯胺可以以高选择性由脂族醇生产。

10. 发明申请

US20070149818A1 PROCESS FOR PRODUCING NITROGEN-CONTAINING COMPOUNDS 失效
标题翻译：生产含氮化合物的方法
公开(公告)号：US20070149818A1
公开(公告)日：2007-06-28
申请号：US11614428
申请日：2006-12-21
申请人： Tetsuaki FUKUSHIMA , Masaharu Jono , Michio Terasaka
发明人： Tetsuaki FUKUSHIMA , Masaharu Jono , Michio Terasaka
IPC分类号： C07C209/16
CPC分类号： C07C209/16 , C07C211/07
摘要： The present invention relates to a process for producing an aliphatic amine, including the step of contacting a linear or branched, or cyclic aliphatic alcohol with ammonia and hydrogen in the presence of a catalyst containing (A) nickel, copper and zirconium components, and (B) at least one metal component selected from the group consisting of elements belonging to Group 1 of the Periodic Table. According to the process of the present invention, an aliphatic primary amine can be produced from the aliphatic alcohol with a good yield and a high productivity.
摘要翻译：本发明涉及一种生产脂肪族胺的方法，包括在含有（A）镍，铜和锆组分的催化剂和（A）镍，铜和锆组分的催化剂存在下，使直链或支链或环状脂族醇与氨和氢接触的步骤和（ B）选自元素周期表第1族元素中的至少一种金属成分。根据本发明的方法，脂肪族伯胺可以从脂肪醇以良好的收率和高生产率制备。

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