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    • 5. 发明授权
    • Method and apparatus in gas chromatography for introducing a sample
    • 用于引入样品的气相色谱法的方法和装置
    • US06062065A
    • 2000-05-16
    • US80818
    • 1998-05-18
    • Kiyoshi SugimotoHaruhiko MiyagawaKatsuhiro Nakagawa
    • Kiyoshi SugimotoHaruhiko MiyagawaKatsuhiro Nakagawa
    • G01N30/10G01N30/12G01N30/16G01N30/04
    • G01N30/12G01N2030/122
    • A tubular insert with a small internal volume is disposed inside the vaporization chamber at the inlet of a capillary column of a gas chromatograph such that the sample with a solvent injected into the vaporization chamber is carried by a carrier gas through the insert into the column. The internal volume of the insert is such that the retention time of the carrier gas through the insert is less than 4 seconds. A heater is controlled to maintain the temperature inside the vaporization chamber within a specified range above the boiling point of the solvent as the sample is injected into the vaporization chamber, and this temperature is subsequently raised to a final temperature above the boiling points of the components to be analyzed. The carrier gas pressure is temporarily increased for better efficiency as the sample is injected.
    • 在气相色谱仪的毛细管柱的入口处,在蒸发室内设置具有小的内部体积的管状插入物,使得注入到蒸发室中的溶剂的样品由载气通过插入件载入柱中。 插入件的内部容积使得载气通过插入件的保留时间小于4秒。 控制加热器以将样品注入蒸发室内,将蒸发室内的温度保持在高于溶剂沸点的规定范围内,然后将该温度升至高于组分沸点的最终温度 待分析。 当样品被注入时,载气压力暂时增加以获得更好的效率。
    • 9. 发明授权
    • Control in mass analyzer
    • 质量分析仪控制
    • US4812649A
    • 1989-03-14
    • US105251
    • 1987-10-07
    • Katsuhiro Nakagawa
    • Katsuhiro Nakagawa
    • G01N27/62H01J49/02H01J49/32B01D59/44
    • H01J49/022
    • In a mass analyzer, an acceleration voltage is applied to an ionization chamber in which a voltage to be applied to repeller electrodes to repel ions is generated with reference to the acceleration voltage and a repeller voltage source is linked with a controller by use of a photocoupler or the like such that the repeller voltage is adjusted with the repeller voltage source electrically insulated from the controller. The repeller voltage can be easily and automatically adjusted by use of a low-voltage control signal so as to obtain a sensitivity developing the maximum value of the quantity of detected ions and hence a qualitative or quantitative analysis of a sample can be achieved with a high sensitivity. The controller processes digital signals and appropriate parameters are stored in a memory. Each parameter is changed with the center of change set to an appropriate parameter previously used and consequently the automatic control is simplified.
    • 在质量分析装置中,向电离室施加加速电压,在该离子化室中,参照加速电压产生施加到排斥电极的电压以排斥离子,并且使用光电耦合器将调制器电压源与控制器连接 使得排斥电压通过与控制器电绝缘的推斥极电压源来调节。 可以通过使用低电压控制信号容易且自动地调节推斥极电压,以获得显影检测离子量的最大值的灵敏度,因此可以以高的方式实现样品的定性或定量分析 灵敏度。 控制器处理数字信号,并将适当的参数存储在存储器中。 每个参数都会随着变化中心的变化而被改变为先前使用的适当参数,因此简化了自动控制。
    • 10. 发明授权
    • Engine with breather apparatus
    • 发动机带呼吸器
    • US07537000B2
    • 2009-05-26
    • US11702518
    • 2007-02-06
    • Takahiro IdeguchiKoichi AsaiToshikazu NakamuraRyo SaitoKatsuhiro NakagawaYasushi Fujita
    • Takahiro IdeguchiKoichi AsaiToshikazu NakamuraRyo SaitoKatsuhiro NakagawaYasushi Fujita
    • F02G5/00F02B25/06
    • F01M13/04F01M2013/0455
    • In order to suppress freezing of a water content within a breather tube, a heater (13) is arranged within a breather tube (11) joining a cylinder head cover (10) and an air cleaner (8). A main body of the breather tube (11) is constituted by a joint tube (18) arranged in a middle, and partial tubes (22, 23) connected to both ends thereof. The heater (13) has a heating element (14) corresponding to a heating element, and has a heater case (21) accommodating the heating element (14) in a state of being pinched by electrodes (15), and is arranged in a center portion of the joint 18. A slot (18a) for inserting the heater (13) is formed in the joint tube 18. A heat radiating body (20) extended along the breather tube (11) is joined to the heater case (21). An outer peripheral portion of the breather tube (11) is covered by an insulative outer tube (24).
    • 为了抑制通气管内的水分冻结,加热器(13)设置在连接气缸盖罩(10)和空气滤清器(8)的通气管(11)内。 通气管(11)的主体由设置在中间的接合管(18)和与其两端连接的部分管(22,23)构成。 加热器(13)具有与加热元件相对应的加热元件(14),并且在被电极(15)夹持的状态下具有容纳加热元件(14)的加热器壳体(21) 在接头管18中形成用于插入加热器(13)的槽(18a)。沿着通气管(11)延伸的散热体(20)与加热器壳体(21) )。 通气管(11)的外周部分由绝缘外管(24)覆盖。