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1. 发明授权

US06667382B1 Polyamine 有权
标题翻译：多胺
公开(公告)号：US06667382B1
公开(公告)日：2003-12-23
申请号：US09674410
申请日：2000-11-01
申请人： Kazuo Isobe , Ryoichi Tamaki , Keiichiro Tomioka , Wataru Yoshida , Tetsuaki Fukushima , Uichiro Nishimoto
发明人： Kazuo Isobe , Ryoichi Tamaki , Keiichiro Tomioka , Wataru Yoshida , Tetsuaki Fukushima , Uichiro Nishimoto
IPC分类号： C08G802
CPC分类号： C08L95/005 , C07C211/14 , C08K5/17
摘要： The present invention provides an amine or polyamine, which has a surface activity not inferior to a solid tallow-based amine and an excellent workability. A salt of the amine is suited for emulsifying asphalt and the like, and also provides an asphalt emulsion composition which is obtained by using the salt and which has a quick setting property. Namely, the prevent invention provides a polyamine represented by the formula (1), a process for producing the amine, and an asphalt emulsion composition containing a water-soluble salt of the amine. wherein R is a straight or branched hydrocarbon group having 8 to 22 carbon atoms; x is a number of 1 to 5; and each of y and z is a number of 0 to 5 with the proviso that both of y and z are not 0 at the same time.
摘要翻译：本发明提供一种胺或多胺，其具有不劣于固体牛脂基胺的表面活性和优异的可加工性。胺的盐适于乳化沥青等，并且还提供了通过使用盐获得并且具有快速固化性能的沥青乳液组合物。即，本发明提供由式（1）表示的多胺，胺的制造方法和含有胺的水溶性盐的沥青乳液组合物。其中R为直链或支链的烃基，其具有8〜 22个碳原子; x是1到5的数字; 并且y和z中的每一个是0至5的数，条件是y和z两者同时不为0。

2. 发明授权

US06737050B2 Hair cosmetic compositions 有权
标题翻译：头发化妆品组合物
公开(公告)号：US06737050B2
公开(公告)日：2004-05-18
申请号：US10026641
申请日：2001-12-27
申请人： Yasuhiro Doi , Keiko Hasebe , Hiroyuki Masuda , Tetsuaki Fukushima , Uichiro Nishimoto , Hiroshi Abe
发明人： Yasuhiro Doi , Keiko Hasebe , Hiroyuki Masuda , Tetsuaki Fukushima , Uichiro Nishimoto , Hiroshi Abe
IPC分类号： A61K7075
CPC分类号： A61K8/898 , A61K8/416 , A61K8/44 , A61K8/463 , A61K8/60 , A61K8/73 , A61K8/891 , A61Q5/00 , A61Q5/02 , A61Q5/12
摘要： Provided are a hair cosmetic composition comprising an ether type cationic surfactant represented by the following formula (1): wherein, R1 represents a linear or branched C6-24 alkyl or alkenyl group, R2 and R4 each represents a C1-6 alkyl group or —(AO)nH (A: a C2-4 alkylene group, n: a number of from 1 to 6 with the proviso that n pieces of A may be the same or different and their sequence is optional), R3 represents a C1-6 alkyl group or —(A′O)mH (A′: a C2-4 alkylene group, m: a number of from 1 to 6 with the proviso that m pieces of A may be the same or different and their sequence is optional), and X− represents an anion; a hair cleansing composition containing the cationic surfactant(1); and a method of treating hair with these compositions. The hair cosmetic composition of the present invention can impart good flexibility and smoothness to hair not only when it is wetted but also after drying. When used as a hair cleansing composition, it provides excellent quality of foam and feeling upon use and exhibits good low-temperature stability.
摘要翻译：提供一种包含由下式（1）表示的醚型阳离子表面活性剂的毛发化妆品组合物：其中，R 1表示直链或支链的C 6-24烷基或链烯基，R 2和R 4各自表示C 1-6烷基或 - （AO）n H（A：C 2-4亚烷基，n：1至6的数，条件是n个A可以相同或不同，它们的顺序为可选），R 3表示C 1-6烷基或 - （A'O）m H（A'：C 2-4亚烷基，m：1至6的数，条件是m个A 可以相同或不同，它们的顺序是任选的），而X“表示阴离子; 含有阳离子表面活性剂（1）的毛发清洁组合物; 以及使用这些组合物处理毛发的方法。本发明的毛发化妆品组合物可以赋予头发良好的柔韧性和光滑性，不仅当其被润湿时，而且在干燥之后。当用作头发清洁组合物时，它提供优异的泡沫质量和使用感，并表现出良好的低温稳定性。

3. 发明授权

US06576794B2 Process for production of ether amine 有权
标题翻译：醚胺生产工艺
公开(公告)号：US06576794B2
公开(公告)日：2003-06-10
申请号：US10015657
申请日：2001-12-17
申请人： Tetsuaki Fukushima , Hiroyuki Masuda , Uichiro Nishimoto , Hiroshi Abe
发明人： Tetsuaki Fukushima , Hiroyuki Masuda , Uichiro Nishimoto , Hiroshi Abe
IPC分类号： C07C25330
CPC分类号： C07C253/30 , C07C213/02 , C07C255/13 , C07C217/08
摘要： A process for producing an ether amine (3), which comprises reacting a primary or secondary alcohol (1), ROH, with acrylonitrile in an amount of 0.8 to 1.2 equivalents of the alcohol (1) in the presence of an alkali metal hydroxide in an amount of not less than 0.01 part by weight, but less than 0.05 part by weight per 100 parts by weight of the alcohol (1) to obtain an alkyloxypropionitrile (2), and then adding water to the reaction system without removing the alkali metal hydroxide therefrom and effecting hydrogenation using a hydrogenation catalyst: ROH(1)+CH2=CHCN→ROCH2CH2CN(2)→ROCH2CH2CH2NH2(3) wherein R denotes a linear or branched alkyl or alkenyl group having 6 to 24 carbon atoms. Also disclosed are a process for producing an ether tertiary amine (5), R—O—CH2—CH2—CH2—N(CH2R1)2, which comprises adding an aldehyde to the resulting ether amine (3) in the presence of a metal catalyst or a Raney nickel catalyst, and a process for producing an ether quaternary ammonium salt (6), R—O—CH2—CH2—CH2—N(CH2R1)2(R2), which comprises reacting a quaternizing agent with the ether tertiary amine (5).
摘要翻译：一种制备醚胺（3）的方法，其包括在碱金属氢氧化物存在下，将伯醇或仲醇（1），ROH与丙烯腈的量为0.8至1.2当量的醇（1）相对于每100重量份的醇（1），不少于0.01重量份，但小于0.05重量份，得到烷氧基丙腈（2），然后向反应体系中加入水而不除去碱金属使用氢化催化剂氢化，其中R表示碳原子数为6〜24的直链或支链烷基或链烯基。还公开了制备醚叔胺（5），RO-CH2-CH2-CH2-N（CH2R1）2的方法，其包括在金属催化剂存在下将醛加到得到的醚胺（3）中，或阮内镍催化剂和制备醚季铵盐（6），RO-CH2-CH2-CH2-N（CH2R1）2（R2）的方法，其包括使季铵化剂与醚叔胺（5）反应，。

4. 发明授权

US06307104B1 Process for producing a primary amine compound 有权
标题翻译：伯胺化合物的制造方法
公开(公告)号：US06307104B1
公开(公告)日：2001-10-23
申请号：US09552659
申请日：2000-04-19
申请人： Wataru Yoshida , Tetsuaki Fukushima
发明人： Wataru Yoshida , Tetsuaki Fukushima
IPC分类号： C07C20948
CPC分类号： C07C209/48
摘要： The present invention relates to a process for producing both of a primary amine compound and an alkylene oxide adduct thereto, given that the both are excellent in color, with high yield. That is, the process comprises hydrogenating a nitrile compound in the presence of a Raney catalyst comprising 90 to 96% by weight of Ni, 3 to 9% by weight of Al and 0.5 to 3% by weight of Mo being based on the total of the atoms of Ni, Al and Mo to obtain the primary amine compound. Further, an alkylene oxide may be added thereto to obtain an alkylene oxide adduct to the primary amine compound.
摘要翻译：本发明涉及一种制备伯胺化合物和其氧化烯加成物的方法，只要它们的颜色都优异，产率高。也就是说，该方法包括在阮内催化剂存在下氢化腈化合物，该催化剂包含90至96重量％的Ni，3至9重量％的Al和0.5至3重量％的Mo，基于 Ni，Al和Mo的原子以获得伯胺化合物。此外，可以向其中加入环氧烷以获得与伯胺化合物的烯化氧加合物。

5. 发明授权

US6117948A Process for producing aliphatic amine derivative 有权
标题翻译：脂肪族胺衍生物的制造方法
公开(公告)号：US6117948A
公开(公告)日：2000-09-12
申请号：US192385
申请日：1998-11-16
申请人： Tetsuaki Fukushima , Wataru Yoshida , Hiroshi Abe
发明人： Tetsuaki Fukushima , Wataru Yoshida , Hiroshi Abe
IPC分类号： C07C213/04 , C07C217/08 , C07C217/50 , C08G65/32 , C08L71/02
CPC分类号： C07C213/04
摘要： The present invention provides a process for easily producing an alkylene oxide adduct to an aliphatic amine compound which has a fully excellent color, is not turbid, and does not deteriorate in color even through long-term storage. That is, the present invention provides a process for producing an alkylene oxide adduct to a primary or secondary amine compound having an aliphatic, saturated or unsaturated, hydrocarbon radical having 8 to 22 carbon atoms, having an excellent color, by reacting an alkyene oxide to the amine compound, characterized by comprising the step of adding a base or an aqueous solution thereof to the amine compound and then heating the mixture.
摘要翻译：本发明提供一种容易地制备脂肪族胺化合物的烯化氧加合物的方法，其具有完全优异的颜色，不混浊，即使长期保存也不会劣化颜色。也就是说，本发明提供了通过使氧化烯与氧化烯反应生成具有碳原子数为8〜22的脂肪族，饱和或不饱和的烃基的伯或仲胺化合物的烯化氧加合物，具有优异的颜色的方法所述胺化合物的特征在于包括将碱或其水溶液加入到所述胺化合物中，然后加热所述混合物的步骤。

6. 发明授权

US5703264A Process for producing aliphatic nitrile 失效
标题翻译：生产脂族腈的方法
公开(公告)号：US5703264A
公开(公告)日：1997-12-30
申请号：US670787
申请日：1996-06-24
申请人： Wataru Yoshida , Tetsuaki Fukushima , Hideki Taniguchi , Hiroshi Abe
发明人： Wataru Yoshida , Tetsuaki Fukushima , Hideki Taniguchi , Hiroshi Abe
IPC分类号： B01J23/89 , C07B61/00 , C07C253/00 , C07C255/03
CPC分类号： B01J23/8933 , B01J23/8926 , C07C253/00
摘要： The process for producing an aliphatic nitrile comprising reacting an aliphatic alcohol having 6 to 40 carbon atoms with ammonia (a) in the presence of a copper/transition metal element in the fourth period other than Cr/platinum group element in the eighth group catalyst, (b) under a reaction system pressure in the range of from atmospheric pressure to 100 atm, (c) at a reaction system temperature in the range of from 100.degree. to 250.degree. C., (d) while introducing at least one gas selected from the group consisting of inert gases and hydrogen gas into the reaction system, (e) removing water formed by the reaction out of the reaction system, and (f) controlling the amount of the ammonia contained in the gas (exclusive of the water formed by the reaction) discharged out of the reaction system to 5 to 50% by volume based on the volume of the gas discharged (exclusive of the water formed by the reaction) makes it possible to produce various kinds of aliphatic nitriles.
摘要翻译：在第八组催化剂中除了Cr /铂族元素以外的第四期间，在铜/过渡金属元素的存在下，使具有6〜40个碳原子的脂肪醇与氨（a）反应的方法，（b）在大气压至100大气压范围内的反应体系压力下，（c）反应体系温度为100-250℃，（d）同时引入至少一种选择的气体从由惰性气体和氢气组成的组中进入反应体系，（e）将由反应形成的水除去反应体系，和（f）控制气体中所含的氨的量（不包括形成的水通过反应）从排出的气体的体积（不包括由反应形成的水）排出反应体系的5〜50体积％使得可以生产各种脂族腈。

7. 发明申请

US20090292145A1 METHOD OF PRODUCING NITROGEN-CONTAINING COMPOUND 有权
标题翻译：生产含氮化合物的方法
公开(公告)号：US20090292145A1
公开(公告)日：2009-11-26
申请号：US12520739
申请日：2007-10-17
申请人： Tetsuaki Fukushima , Hideki Taniguchi , Michio Terasaka
发明人： Tetsuaki Fukushima , Hideki Taniguchi , Michio Terasaka
IPC分类号： C07C209/50
CPC分类号： C07C209/50 , B01J21/10 , B01J23/002 , B01J23/78 , B01J23/80 , B01J23/8926 , B01J23/8946 , B01J29/06 , B01J29/072 , B01J29/143 , B01J37/03 , B01J2523/00 , C07C211/08 , B01J2523/17 , B01J2523/22 , B01J2523/23 , B01J2523/25 , B01J2523/824 , B01J2523/27
摘要： The present invention provides a process for producing high-purity aliphatic tertiary amines containing a less amount of by-products by using a chromium-free catalyst with a good productivity in an economically advantageous manner. The present invention relates to a process for producing a tertiary amine by reducing an amide compound in the presence of a catalyst containing copper and magnesium at a molar ratio of magnesium to copper (magnesium/copper) of from 0.01 to 20.
摘要翻译：本发明提供一种以经济上有利的方式通过使用无铬催化剂以高生产率生产含少量副产物的高纯度脂族叔胺的方法。本发明涉及一种通过在含有铜与镁（镁/铜）摩尔比为0.01〜20的铜和镁的催化剂存在下还原酰胺化合物来制备叔胺的方法。

8. 发明授权

US07259274B2 Method of producing aliphatic nitrile 失效
标题翻译：生产脂族腈的方法
公开(公告)号：US07259274B2
公开(公告)日：2007-08-21
申请号：US10936745
申请日：2004-09-09
申请人： Michio Terasaka , Tetsuaki Fukushima
发明人： Michio Terasaka , Tetsuaki Fukushima
IPC分类号： C07C253/00 , C07C63/30
CPC分类号： B01J21/08 , B01J35/1019 , B01J37/03 , C07C253/22 , C07C255/03
摘要： An aliphatic nitrile is prepared by a process of reacting an aliphatic carboxylic acid, an aliphatic dicarboxylic acid or an alkyl ester thereof, wherein the alkyl group has 1 to 5 carbon atoms, with ammonia in the presence of a catalyst of titanium oxide supported on solid silica.
摘要翻译：通过使负载在固体上的氧化钛催化剂的存在下使氨基在其中烷基具有1至5个碳原子的脂族羧酸，脂族二羧酸或其烷基酯与氨反应来制备脂族腈二氧化硅。

9. 发明授权

US08278488B2 Process for producing nitrogen-containing compounds 有权
标题翻译：含氮化合物的制造方法
公开(公告)号：US08278488B2
公开(公告)日：2012-10-02
申请号：US12672327
申请日：2008-08-07
申请人： Michio Terasaka , Tetsuaki Fukushima , Hideki Taniguchi , Masaharu Jono
发明人： Michio Terasaka , Tetsuaki Fukushima , Hideki Taniguchi , Masaharu Jono
IPC分类号： C07C209/00 , C07C291/04
CPC分类号： C07C209/50 , C07C209/02 , C07C211/08 , C07C291/04
摘要： The present invention relates to a process for producing a tertiary amine in the presence of a catalyst containing copper and at least one element selected from the group consisting of elements belonging to Groups 2, 3, 7 and 12 of the Periodic Table (long form of the periodic table), said process including the steps of (a) reducing an amide compound in a hydrogen atmosphere; and (b) introducing a dialkyl amine containing a linear or branched alkyl group having 1 to 6 carbon atoms into a reaction product obtained in the step (a), and treating the reaction product with the dialkyl amine. The present invention provides a process for producing high-purity aliphatic tertiary amines containing a less amount of by-products by reducing aliphatic acid amides under moderate conditions using a chromium-free catalyst, as well as a process for producing amine derivatives such as amine oxide by using the aliphatic tertiary amines, with a good productivity in an economical manner.
摘要翻译：本发明涉及在含有铜的催化剂和选自元素周期表第2,3,7和12族元素中的至少一种元素的存在下制备叔胺的方法（长形式所述方法包括以下步骤：（a）在氢气氛中还原酰胺化合物; 和（b）将含有具有1至6个碳原子的直链或支链烷基的二烷基胺引入步骤（a）中获得的反应产物中，并用二烷基胺处理反应产物。本发明提供了一种通过使用无铬催化剂在中等条件下还原脂肪酸酰胺以及生产胺衍生物如氧化胺的方法来生产含有少量副产物的高纯度脂族叔胺的方法通过使用脂肪族叔胺，以经济的方式具有良好的生产率。

10. 发明申请

US20120208738A1 NONIONIC SURFACTANT AND SURFACTANT COMPOSITION COMPRISING THE SAME 有权
标题翻译：非离子表面活性剂和包含其的表面活性剂组合物
公开(公告)号：US20120208738A1
公开(公告)日：2012-08-16
申请号：US13502859
申请日：2010-10-18
申请人： Masato Nomura , Satoru Kijima , Katsuhisa Inoue , Tetsuaki Fukushima , Tomoya Sato
发明人： Masato Nomura , Satoru Kijima , Katsuhisa Inoue , Tetsuaki Fukushima , Tomoya Sato
IPC分类号： C11D17/00 , C07C43/11 , C07C43/13
CPC分类号： C11D1/722
摘要： The present invention provides the nonionic surfactant represented by the formula (1): R—O-(PO)m-(EO)n-H (1) wherein, R represents a saturated linear-chain hydrocarbon group having 8 to 18 carbon atoms, and n-octyl groups are 20 to 80% by mole of the saturated linear-chain hydrocarbon groups, n-decyl groups are 0 to 10% by mole of the saturated linear-chain hydrocarbon groups, and saturated linear-chain hydrocarbon groups having 12 to 18 carbon atoms are 20 to 80% by mole of the saturated linear-chain hydrocarbon groups; PO represents a propyleneoxy group; EO represents an ethyleneoxy group; m represents an average addition mole number of propyleneoxy groups ranging from 0.1 to 5; n represents an average addition mole number of ethyleneoxy groups ranging from 0.5 to 20; and (PO)m and (EO)n are bonded as blocks in this order.
摘要翻译：本发明提供由式（1）表示的非离子型表面活性剂：R-O-（PO）m-（EO）nH（1）其中，R表示碳原子数8〜18的饱和直链烃基，正辛基的饱和直链烃基为20〜80摩尔％，正癸基为饱和直链烃基为0〜10摩尔％，饱和直链烃基为12〜 18个碳原子为饱和直链烃基的20〜80摩尔％ PO表示丙烯氧基; EO表示乙烯氧基; m表示丙烯氧基的平均加成摩尔数为0.1〜5; n表示0.5〜20的乙烯氧基的平均加成摩尔数; 和（PO）m和（EO）n以该顺序键合。

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