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1. 发明申请

US20080103270A1 Core/Shell Type Polyamine Dendrimer Compound 审中-公开
标题翻译：核/壳型聚胺树枝状化合物
公开(公告)号：US20080103270A1
公开(公告)日：2008-05-01
申请号：US10529964
申请日：2003-10-02
申请人： Isao Sato , Toru Inaoka , Seiichi Suzuki , Hayato Itagaki , Yoshiyuki Onda
发明人： Isao Sato , Toru Inaoka , Seiichi Suzuki , Hayato Itagaki , Yoshiyuki Onda
IPC分类号： C08F283/00
CPC分类号： C08G83/003 , C08G73/02
摘要： A core/shell type polyamine dendrimer compound comprising core regions formed of a dendrimer compound and shell regions formed by the reaction of at least one amine compound. A method for the production of the compound is also disclosed.
摘要翻译：核/壳型聚胺树枝状大分子化合物，其包含由树枝状大分子化合物形成的核心区域和通过至少一种胺化合物反应形成的壳体区域。还公开了制备该化合物的方法。

2. 发明授权

US06278007B1 (Poly)alkylene glycol higher alkyl ether derivative composition and detergent, lubricant, and dermatologic medicine for external use containing the composition 失效
标题翻译：（聚）亚烷基二醇高级烷基醚衍生物组合物和洗涤剂，润滑剂和皮肤外用药物，含有组合物
公开(公告)号：US06278007B1
公开(公告)日：2001-08-21
申请号：US09309011
申请日：1999-05-10
申请人： Toru Inaoka , Kenji Rakutani , Yukio Kadono , Yoshiyuki Onda
发明人： Toru Inaoka , Kenji Rakutani , Yukio Kadono , Yoshiyuki Onda
IPC分类号： C07B3508
CPC分类号： C10M105/18 , C07C43/11 , C07C69/003 , C07C69/24 , C08G65/2615 , C08G65/3312 , C10M105/40 , C10M107/34 , C10M2207/04 , C10M2207/289 , C10M2209/104 , C10M2209/105 , C10M2209/106 , C10M2209/109 , C11D1/72 , C11D1/721 , C11D1/74
摘要： A (poly)alkylene glycol higher alkyl ether derivative composition characterized by comprising 30-90 mol. % of (B1) (poly)alkylene glycol higher alkyl ether derivative and 70-10 mol. % of (B2) (poly)alkylene glycol higher alkyl ether derivative, respectively having a methyl group for R1 and an alkyl group of not less than two carbon atoms for R1 in the general formula (1) representing the derivatives: (wherein R1 and R2 represent alkyl groups whose total number of carbon atoms is in the range of 7-29, the number of carbon atoms of R2 is larger than the number of carbon atoms of R1, A represents a lower alkylene group, n represents a real number in the range of 1-300 on average, x represents 0 or 1, y represents a real number in the range of 1-10 on average, and R3 represents an optionally substituted organic residue of 1-60 carbon atoms [excluding the carbon atoms of the substituent]) and a deterging agent, a lubricating agent, or a dermatological medicine for external use containing the (poly)alkylene glycol higher alkyl ether derivative composition. The composition possesses such characteristic features as containing no oil-soluble component of low molecular weight, emitting odor sparingly, exhibiting a low stimulating property, having no foaming property, abounding in penetrating force, allowing thorough separation of the foam from a deterged article, and enjoying such low viscosity as to allow great ease of handling.
摘要翻译：（聚）亚烷基二醇高级烷基醚衍生物组合物，其特征在于包含30-90mol。（B1）（聚）亚烷基二醇高级烷基醚衍生物的百分比和70-10摩尔。％的（B2）（聚）亚烷基二醇高级烷基醚衍生物，在通式（1）中分别具有R1的甲基和不少于2个碳原子的烷基，其中R1和 R2表示碳原子数为7〜29的烷基，R2的碳原子数大于R1的碳原子数，A表示低级亚烷基，n表示实数平均1-300的范围，x表示0或1，y表示平均1-10个范围内的实数，R3表示1-60个碳原子的任选取代的有机残基[不包括取代基]）和含有（聚）亚烷基二醇高级烷基醚衍生物组合物的洗涤剂，润滑剂或外用皮肤病学药剂。该组合物具有如下特征：不含低分子量油溶性成分，少量发臭，表现出低刺激性，无起泡性，渗透力大，允许泡沫与洗涤物品彻底分离，享受这样的低粘度以使得易于处理。

3. 发明申请

US20050080298A1 Production processes for alkylene oxide addition product and its derivatives 有权
标题翻译：烯化氧加成产物及其衍生物的生产方法
公开(公告)号：US20050080298A1
公开(公告)日：2005-04-14
申请号：US10500554
申请日：2003-05-02
申请人： Toru Inaoka , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
发明人： Toru Inaoka , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
IPC分类号： C08F299/02 , C08G65/26 , C08G65/28 , C08G65/332 , C07C67/26 , C08G59/14
CPC分类号： C08G65/2609 , C08G65/2696 , C08G65/3322
摘要： The present invention provides: a production process for an alkylene oxide addition product, by which a high-molecular alkylene oxide addition product can be obtained with ordinary production facilities while the formation of by-products is suppressed; and production processes for derivatives from the alkylene oxide addition product. The present invention production process for an alkylene oxide addition product comprises the step of carrying out an addition reaction of an alkylene oxide to a hydroxyl-group-containing saturated compound in order to obtain the alkylene oxide addition product; with the production process being characterized by further comprising: the initial step of causing the alkylene oxide to add to the hydroxyl-group-containing saturated compound in an amount of not larger than 20 mols on average of the alkylene oxide per 1 mol of the hydroxyl-group-containing saturated compound to thereby obtain an alkylene oxide low-mol-addition product; and the molar-degree-of-polyaddition-adjusting step of causing the alkylene oxide to further add to the alkylene oxide low-mol-addition product as obtained in the initial step; wherein a portion of the entirety of the alkylene oxide low-mol-addition product as obtained in the initial step is used in the molar-degree-of-polyaddition-adjusting step.
摘要翻译：本发明提供：一种环氧烷加成物的制造方法，通过该方法可以获得具有普通生产设备的高分子量烯化氧加成产物，同时抑制副产物的形成; 以及来自烯化氧加成产物的衍生物的制备方法。本发明的烯化氧加成产物的制备方法包括进行烯化氧与含羟基的饱和化合物的加成反应以获得环氧烷烃加成产物的步骤; 其制备方法的特征还在于：使每1摩尔羟基的烯化氧的平均相对于含有羟基的饱和化合物不少于20摩尔的环氧烷加成的初始步骤含有饱和化合物，得到环氧烷低摩尔加成产物; 和加成摩尔加聚度调整步骤，使得氧化烯进一步添加到初始步骤中获得的环氧烷低摩尔加成产物; 其中在初始步骤中获得的全部烯化氧低摩尔加成产物的一部分用于加聚度加聚步骤。

4. 发明授权

US06762325B2 Method for production of alkoxylated compound 失效
标题翻译：烷氧基化合物的制造方法
公开(公告)号：US06762325B2
公开(公告)日：2004-07-13
申请号：US10144491
申请日：2002-05-13
申请人： Toru Inaoka , Yasuhiko Sato , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
发明人： Toru Inaoka , Yasuhiko Sato , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
IPC分类号： C07C21300
CPC分类号： C04B24/267 , B01F7/18 , B01J19/006 , B01J19/0066 , B01J19/18 , B01J2219/00063 , B01J2219/00168 , B01J2219/00768 , B01J2219/00779 , C04B24/2647 , C04B2103/408 , C08G65/2609 , C08G65/2696 , C08G65/30
摘要： When the reaction solution formed during the addition of an alkylene oxide to an active hydrogen-containing compound has viscosity of not less than 10 mPa·s, this invention provides a method for stirring the reaction solution by the rotation of a vane or vanes continuously disposed in the vertical direction within an agitating reaction vessel in such a manner that the numerical value C represented by the following formula (1): C=A/(h2−h1) (1) (wherein A denotes the length (m) of the vane or the vanes newly immersed by the supply of alkylene oxide, h1 denotes the height (m) of the liquid level before the supply of alkylene oxide, and h2 denotes the height (m) of the liquid level after the supply of alkylene oxide) may be not less than 0.5. By employing the method of this invention, it is made possible to effect addition of an alkylene oxide to the active hydrogen-containing compound with high efficiency. Further, the use of this method allows repression of the content of a by-product which causes the degradation of the characteristic properties of the alkoxylated compound.
摘要翻译：当在含有活性氢的化合物中加入烯化氧时形成的反应溶液的粘度不低于10mPa.s，本发明提供一种通过连续设置的叶片或叶片的旋转来搅拌反应溶液的方法在搅拌反应容器内沿垂直方向以下式（1）表示的数值C :(其中A表示叶片或通过供给环氧烷而新浸入的叶片的长度（m） h1表示供给环氧烷前的液面的高度（m），h2表示供给环氧烷以后的液面高度（μm））可以为0.5以上。通过采用本发明的方法，可以高效率地向含活性氢的化合物中加入烯化氧。此外，使用该方法可抑制副产物的含量，这导致烷氧基化化合物的特征性质的降解。

5. 发明授权

US5688843A Oil-absorbent composition, particulate oil absorber, oil-absorbent material, and oil-absorbent pack 失效
标题翻译：吸油组合物，颗粒油吸收剂，吸油材料和吸油性包装
公开(公告)号：US5688843A
公开(公告)日：1997-11-18
申请号：US548527
申请日：1995-10-26
申请人： Toru Inaoka , Tomoki Gomi , Yoshiyuki Onda , Toshio Tamura , Hideyuki Tahara
发明人： Toru Inaoka , Tomoki Gomi , Yoshiyuki Onda , Toshio Tamura , Hideyuki Tahara
IPC分类号： C09K3/32 , C08K9/00
CPC分类号： C09K3/32
摘要： An oil-absorbent composition including 30 to 99.5 parts by weight of (I) an oil-absorbent, cross-linked polymer formed from 96-99.999% by weight of (A) monomer having a polymerizable unsaturated group in the molecule, said monomer (A) containing mainly a monomer having a solubility parameter of not more than 9, and 4-0.001% by weight of (B) a cross-linking monomer having at least two polymerizable unsaturated groups in the molecule, provided the sum of monomer (A) and cross-linking monomer (B) is 100%, and 70 to 0.5 to parts by weight of (IV) at least one compound selected from the group consisting of (II) inorganic compounds having a methanol value of not less than 25% and (III) substantially water insoluble organic acid salts, provided the sum of oil-absorbent, cross-linked polymer (I) and compound (IV) is 100 parts by weight.
摘要翻译：一种吸油性组合物，其包含30〜99.5重量份（I）由分子中具有聚合性不饱和基团的（A）单体的96-99.999重量％形成的吸油性交联聚合物，所述单体（ A），主要含有溶解度参数为9以下的单体和（B）分子中具有至少2个可聚合不饱和基团的交联单体的4-0.001重量％，提供了单体（A ）和交联单体（B）为100％，和70〜0.5重量份的（Ⅳ）至少一种选自（II）甲醇值不小于25重量％的无机化合物的化合物，和（III）基本上不溶于水的有机酸盐，只要吸油剂，交联聚合物（I）和化合物（IV）之和为100重量份即可。

6. 发明授权

US07402644B2 Production processes for alkylene oxide addition product and its derivatives 有权
标题翻译：烯化氧加成产物及其衍生物的生产方法
公开(公告)号：US07402644B2
公开(公告)日：2008-07-22
申请号：US10500554
申请日：2003-05-02
申请人： Toru Inaoka , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
发明人： Toru Inaoka , Yoshiyuki Onda , Hiromichi Tanaka , Tsuyoshi Hirata
IPC分类号： C08F20/26 , C07C69/52 , C07C43/00
CPC分类号： C08G65/2609 , C08G65/2696 , C08G65/3322
摘要： The present invention provides: a production process for an alkylene oxide addition product, by which a high-molecular alkylene oxide addition product can be obtained with ordinary production facilities while the formation of by-products is suppressed; and production processes for derivatives from the alkylene oxide addition product. The present invention production process for an alkylene oxide addition product comprises the step of carrying out an addition reaction of an alkylene oxide to a hydroxyl-group-containing saturated compound in order to obtain the alkylene oxide addition product; with the production process being characterized by further comprising: the initial step of causing the alkylene oxide to add to the hydroxyl-group-containing saturated compound in an amount of not larger than 20 mols on average of the alkylene oxide per 1 mol of the hydroxyl-group-containing saturated compound to thereby obtain an alkylene oxide low-mol-addition product; and the molar-degree-of-polyaddition-adjusting step of causing the alkylene oxide to further add to the alkylene oxide low-mol-addition product as obtained in the initial step; wherein a portion of the entirety of the alkylene oxide low-mol-addition product as obtained in the initial step is used in the molar-degree-of-polyaddition-adjusting step.
摘要翻译：本发明提供：一种环氧烷加成物的制造方法，通过该方法可以获得具有普通生产设备的高分子量烯化氧加成产物，同时抑制副产物的形成; 以及来自烯化氧加成产物的衍生物的制备方法。本发明的烯化氧加成产物的制备方法包括进行烯化氧与含羟基的饱和化合物的加成反应以获得环氧烷烃加成产物的步骤; 其制备方法的特征还在于：使每1摩尔羟基的烯化氧的平均相对于含有羟基的饱和化合物不少于20摩尔的环氧烷加成的初始步骤含有饱和化合物，得到环氧烷低摩尔加成产物; 和加成摩尔加聚度调整步骤，使得氧化烯进一步添加到初始步骤中获得的环氧烷低摩尔加成产物; 其中在初始步骤中获得的全部烯化氧低摩尔加成产物的一部分用于加聚度加聚步骤。

7. 发明授权

US06451961B2 Ethylenimine polymer, aqueous solution of ethylenimine polymer, production process for the same and purifying process therefor 失效
标题翻译：乙烯亚胺聚合物，乙烯亚胺聚合物的水溶液，生产方法相同，并进行净化处理
公开(公告)号：US06451961B2
公开(公告)日：2002-09-17
申请号：US09771704
申请日：2001-01-30
申请人： Seiichi Suzuki , Yoshiyuki Onda , Isao Satoh
发明人： Seiichi Suzuki , Yoshiyuki Onda , Isao Satoh
IPC分类号： G08G7304
CPC分类号： C08G73/0213
摘要： Provided are processes by which an ethylenimine polymer and an aqueous solution thereof can advantageously be produced at low costs in an industrial scale. The ethylenimine polymer can be produced by polymerizing crude ethylenimine obtained by a simple distilling operation from an ethylenimine-containing reaction mixture produced by subjecting ethanolamine to intermolecular dehydration reaction, preferably crude ethylenimine having impurity contents which are controlled in the specific ranges. When the above crude ethylenimine is polymerized in an aqueous medium, capable of being obtained is an aqueous solution of an ethylenimine polymer having a higher molecular weight than that produced by non-solvent polymerization. The ethylenimine polymer can be purified by, for example, adding water thereto, mixing them and then vaporizing and removing water under heating. The aqueous solution of an ethylenimine polymer can be purified by heating and condensing it.
摘要翻译：提供了以工业规模低成本有利地生产乙烯亚胺聚合物及其水溶液的方法。乙烯亚胺聚合物可以通过将通过使乙醇胺进行分子间脱水反应制备的含乙烯亚胺的反应混合物通过简单蒸馏操作获得的粗制乙烯亚胺进行聚合来制备，优选将杂质含量控制在特定范围内的粗制乙烯亚胺。当上述粗制亚乙基亚胺在水性介质中聚合时，能得到的分子量高于通过非溶剂聚合制得的乙烯亚胺聚合物的水溶液。乙烯亚胺聚合物可以通过例如向其中加水，混合，然后在加热下汽化和除去水来纯化。乙烯亚胺聚合物的水溶液可以通过加热和冷凝来纯化。

8. 发明授权

US06444769B2 Production process for ethylenimine polymer aqueous solution 有权
标题翻译：乙烯亚胺聚合物水溶液的生产工艺
公开(公告)号：US06444769B2
公开(公告)日：2002-09-03
申请号：US09810568
申请日：2001-03-19
申请人： Seiichi Suzuki , Yoshiyuki Onda , Isao Satoh
发明人： Seiichi Suzuki , Yoshiyuki Onda , Isao Satoh
IPC分类号： C08F12608
CPC分类号： C08J3/03 , C08G73/0213 , C08J2379/02
摘要： Provided is a process for producing an ethylenimine polymer aqueous solution which has a high concentration (high resin content) and is less changeable with the passage of time, that is, has a stabilized quality. The above process comprises polymerizing ethylenimine in a water based medium at a temperature of 80° C. or lower and then ripening it at a temperature of 100 to 150° C.
摘要翻译：提供了具有高浓度（高树脂含量）并且随时间流逝变化不大，即具有稳定质量的乙烯亚胺聚合物水溶液的制备方法。上述方法包括在80℃或更低的温度下在水性介质中聚合乙烯亚胺，然后在100至150℃的温度下熟化。

9. 发明授权

US07405264B2 Polycarboxylic acid copolymer, production method and use thereof 失效
标题翻译：聚羧酸共聚物，其制备方法和用途
公开(公告)号：US07405264B2
公开(公告)日：2008-07-29
申请号：US10921148
申请日：2004-08-19
申请人： Tsutomu Yuasa , Tomotaka Nishikawa , Noboru Sakamoto , Tsuyoshi Hirata , Hiroko Izukashi , Tomiyasu Ueta , Hiromichi Tanaka , Yoshiyuki Onda , Toru Uno
发明人： Tsutomu Yuasa , Tomotaka Nishikawa , Noboru Sakamoto , Tsuyoshi Hirata , Hiroko Izukashi , Tomiyasu Ueta , Hiromichi Tanaka , Yoshiyuki Onda , Toru Uno
IPC分类号： C08F16/12 , C08F20/06
CPC分类号： C04B24/2658 , C04B2103/302 , C08F290/06 , C08F290/065 , C08G65/2624 , C08G2650/24 , C08L51/04 , C08L53/00 , C08L55/02 , C08L71/02 , C08L2666/24 , C08L2666/14 , C08L2666/02 , C08L2666/04
摘要： It is an object of the present invention to provide a polycarboxylic acid polpolymer which improves the water reducing capacity and workability of cement compositions and the like and making them easier to handle when the fluidity and water reducing capacity are at the same levels, a method of producing the copolymer, and a cement additive and a cement composition comprising the copolymer. The present invention is further to provide a polycarboxylic acid copolymer and a cement additive which are capable of improving the strength and durability of hardening products of cement compositions, hence can advantageously be used in ultrahigh strength concrete. The present invention is polycarboxylic acid copolymers having high water reducing capacity, reducing the viscosity of cement compositions and improving the workability in applying cement.The present invention is directed to a polycarboxylic acid copolymer which is obtained by copolymerization of monomer components comprising a polyalkyleneimine unsaturated monomer (A1) and an unsaturated carboxylic acid monomer (B).
摘要翻译：本发明的目的是提供一种改善水泥组合物等的减水能力和加工性的多元羧酸聚合物，并且当流动性和减水能力处于相同水平时使其更容易处理，制备共聚物，以及包含该共聚物的水泥添加剂和水泥组合物。本发明还提供能够提高水泥组合物的硬化物的强度和耐久性的聚羧酸共聚物和水泥添加剂，因此可以有利地用于超高强度混凝土中。本发明是具有高降水能力的聚羧酸共聚物，降低了水泥组合物的粘度并提高了施加水泥的可加工性。本发明涉及通过使包含聚亚烷基亚胺不饱和单体（A1）和不饱和羧酸单体（B）的单体成分共聚获得的多元羧酸共聚物。

10. 发明授权

US5430170A Process for preparing dialkyl carbonates 失效
标题翻译：制备碳酸二烷基酯的方法
公开(公告)号：US5430170A
公开(公告)日：1995-07-04
申请号：US155925
申请日：1993-11-23
申请人： Yoshiaki Urano , Masaru Kirishiki , Yoshiyuki Onda , Hideaki Tsuneki
发明人： Yoshiaki Urano , Masaru Kirishiki , Yoshiyuki Onda , Hideaki Tsuneki
IPC分类号： B01J23/10 , C07C68/06 , C07C69/96
CPC分类号： C07C68/065
摘要： A industrially advantageous process for preparing dialkyl carbonates is provided. The process is characterized in that an alkylene carbonate and an alcohol are subjected to an transesterification in the presence of a catalyst which contains, as the catalytically active component, at least one rare-earth oxide. According to this process, the transesterification progresses rapidly due to the excellent activity of the catalyst, and the catalyst can be readily separated after termination of the reaction, allowing high efficiency isolation and purification of dialkyl carbonate.
摘要翻译：提供了一种工业上有利的制备碳酸二烷基酯的方法。该方法的特征在于，在含有作为催化活性组分的至少一种稀土氧化物的催化剂存在下，将碳酸亚烷基酯和醇进行酯交换反应。根据该方法，由于催化剂的优异活性，酯交换反应迅速进行，催化剂在反应终止后可以容易地分离，能够高效地分离和纯化碳酸二烷基酯。

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