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1. 发明授权

US07667083B2 Fluorosulfonyl group-containing compound, method for its production and polymer thereof 有权
标题翻译：含氟磺酰基的化合物，其制备方法及其聚合物
公开(公告)号：US07667083B2
公开(公告)日：2010-02-23
申请号：US12410524
申请日：2009-03-25
申请人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
IPC分类号： C07C17/00 , C07C19/00 , C07C21/00 , C07C23/00
CPC分类号： C07C303/22 , C07C309/82 , C07C309/84 , C08F214/18 , C08J5/2237 , C08J2327/18 , H01B1/122 , H01M2008/1095 , H01M2300/0082
摘要： A compound containing two fluorosulfonyl groups which are groups convertible to sulfonic acid groups, an intermediate therefor, and methods for their production with high productivity, are provided. Also provided are a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer.A method for producing a compound of the following formula (m0), such a compound, a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer, provided that RF01 is a single bond or a C1-6 bivalent perfluoro organic group, RF02 is a C1-6 bivalent perfluoro organic group, and n is 0 or 1.
摘要翻译：提供了含有可转化成磺酸基团的两个氟磺酰基的化合物，其中间体，以及高生产率的生产方法。还提供了通过聚合这种化合物获得的含氟磺酰基的聚合物和由这种聚合物获得的含磺酸基的聚合物。制备下式（m0）化合物的方法，该化合物，通过聚合该化合物得到的含氟磺酰基的聚合物和由这种聚合物得到的含磺酸基的聚合物，条件是RF01为单键或C1-6二价全氟有机基团，RF02为C1-6二价全氟有机基团，n为0或1。

2. 发明授权

US07531610B2 Fluorosulfonyl group-containing compound, method for its production and polymer thereof 有权
标题翻译：含氟磺酰基的化合物，其制备方法及其聚合物
公开(公告)号：US07531610B2
公开(公告)日：2009-05-12
申请号：US12010586
申请日：2008-01-28
申请人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
IPC分类号： C08F16/24 , C07C309/00
CPC分类号： C07C303/22 , C07C309/82 , C07C309/84 , C08F214/18 , C08J5/2237 , C08J2327/18 , H01B1/122 , H01M2008/1095 , H01M2300/0082
摘要： A compound containing two fluorosulfonyl groups which are groups convertible to sulfonic acid groups, an intermediate therefor, and methods for their production with high productivity, are provided. Also provided are a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer.A method for producing a compound of the following formula (m0), such a compound, a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer, provided that RF01 is a single bond or a C1-6 bivalent perfluoro organic group, RF02 is a C1-6 bivalent perfluoro organic group, and n is 0 or 1:
摘要翻译：提供了含有可转化成磺酸基团的两个氟磺酰基的化合物，其中间体，以及高生产率的生产方法。还提供了通过聚合这种化合物获得的含氟磺酰基的聚合物和由这种聚合物获得的含磺酸基的聚合物。制备下式（m0）化合物的方法，该化合物，通过聚合该化合物得到的含氟磺酰基的聚合物和由这种聚合物得到的含磺酸基的聚合物，条件是RF01为单键或C1-6二价全氟有机基团，RF02为C1-6二价全氟有机基团，n为0或1：

3. 发明申请

US20080146841A1 Fluorosulfonyl group-containing compound, method for its production and polymer thereof 有权
标题翻译：含氟磺酰基的化合物，其制备方法及其聚合物
公开(公告)号：US20080146841A1
公开(公告)日：2008-06-19
申请号：US12010586
申请日：2008-01-28
申请人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
IPC分类号： C07C309/00
CPC分类号： C07C303/22 , C07C309/82 , C07C309/84 , C08F214/18 , C08J5/2237 , C08J2327/18 , H01B1/122 , H01M2008/1095 , H01M2300/0082
摘要： A compound containing two fluorosulfonyl groups which are groups convertible to sulfonic acid groups, an intermediate therefor, and methods for their production with high productivity, are provided. Also provided are a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer.A method for producing a compound of the following formula (m0), such a compound, a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer, provided that RF01 is a single bond or a C1-6 bivalent perfluoro organic group, RF02 is a C1-6 bivalent perfluoro organic group, and n is 0 or 1:
摘要翻译：提供了含有可转化成磺酸基团的两个氟磺酰基的化合物，其中间体，以及高生产率的生产方法。还提供了通过聚合这种化合物获得的含氟磺酰基的聚合物和由这种聚合物获得的含磺酸基的聚合物。制备下式（m0）化合物的方法，该化合物，通过聚合该化合物得到的含氟磺酰基的聚合物和由这种聚合物得到的含磺酸基的聚合物，条件是R < > F01 是单键或C 1-6 - 二价全氟有机基团，R F02是C 1-6烷基，二价全氟有机基团，n为0或1：

4. 发明申请

US20090187044A1 FLUOROSULFONYL GROUP-CONTAINING COMPOUND, METHOD FOR ITS PRODUCTION AND POLYMER THEREOF 有权
标题翻译：含氟聚合物的含氟化合物，其生产方法及其聚合物
公开(公告)号：US20090187044A1
公开(公告)日：2009-07-23
申请号：US12410524
申请日：2009-03-25
申请人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Atsushi Watakabe , Jyunichi Tayanagi , Susumu Saito
IPC分类号： C07C309/82
CPC分类号： C07C303/22 , C07C309/82 , C07C309/84 , C08F214/18 , C08J5/2237 , C08J2327/18 , H01B1/122 , H01M2008/1095 , H01M2300/0082
摘要： A compound containing two fluorosulfonyl groups which are groups convertible to sulfonic acid groups, an intermediate therefor, and methods for their production with high productivity, are provided. Also provided are a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer.A method for producing a compound of the following formula (m0), such a compound, a fluorosulfonyl group-containing polymer obtained by polymerizing such a compound, and a sulfonic acid group-containing polymer obtained from such a polymer, provided that RF01 is a single bond or a C1-6 bivalent perfluoro organic group, RF02 is a C1-6 bivalent perfluoro organic group, and n is 0 or 1:
摘要翻译：提供了含有可转化成磺酸基团的两个氟磺酰基的化合物，其中间体，以及高生产率的生产方法。还提供了通过聚合这种化合物获得的含氟磺酰基的聚合物和由这种聚合物获得的含磺酸基的聚合物。制备下式（m0）化合物的方法，该化合物，通过聚合该化合物得到的含氟磺酰基的聚合物和由这种聚合物得到的含磺酸基的聚合物，条件是RF01为单键或C1-6二价全氟有机基团，RF02为C1-6二价全氟有机基团，n为0或1：

5. 发明授权

US08097383B2 Electrolyte material for polymer electrolyte fuel cells, electrolyte membrane and membrane/electrode assembly 有权
标题翻译：用于聚合物电解质燃料电池，电解质膜和膜/电极组件的电解质材料
公开(公告)号：US08097383B2
公开(公告)日：2012-01-17
申请号：US12010589
申请日：2008-01-28
申请人： Isamu Kaneko , Tetsuji Shimohira , Atsushi Watakabe , Seigo Kotera , Satoru Hommura , Koichi Murata , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Tetsuji Shimohira , Atsushi Watakabe , Seigo Kotera , Satoru Hommura , Koichi Murata , Jyunichi Tayanagi , Susumu Saito
IPC分类号： H01M8/10
CPC分类号： C08J5/225 , C08J2327/12 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M2300/0082
摘要： To provide a polymer electrolyte material for polymer electrolyte fuel cells, which is an electrolyte material having a high ion exchange capacity and a low resistance, and which has a higher softening temperature than a conventional electrolyte material.An electrolyte material for polymer electrolyte fuel cells, which is made of a polymer containing repeating units based on a fluoromonomer having a radical polymerization reactivity, wherein the repeating units contain, in their side chains, a structure having ionic groups represented in the following formula (α) (provided that in the formula, each of Q1 and Q2 which are independent of each other, is a single bond or a perfluoroalkylene group that may have an etheric oxygen atom, provided that they are not single bonds at the same time, Rf1 is a perfluoroalkyl group which may have an etheric oxygen atom, and X is an oxygen atom, a nitrogen atom or a carbon atom, provided that when X is an oxygen atom, a=0, when X is a nitrogen atom, a=1, and when X is a carbon atom, a=2, and Y is a fluorine atom or a monovalent perfluoro organic group).
摘要翻译：本发明提供一种高分子电解质燃料电池用聚合物电解质材料，该高分子电解质材料是具有高离子交换能力和低电阻的电解质材料，其软化温度高于常规电解质材料。一种用于聚合物电解质燃料电池的电解质材料，其由含有具有自由基聚合反应性的含氟单体的重复单元的聚合物制成，其中重复单元在其侧链中包含具有下式表示的离子基团的结构（ α）（条件是在式中，Q1和Q2各自独立地为可以具有醚性氧原子的单键或全氟亚烷基，条件是它们不同时为单键，Rf1 是可以具有醚性氧原子的全氟烷基，X是氧原子，氮原子或碳原子，条件是当X是氧原子时a = 0，当X是氮原子时，a = 1 ，当X为碳原子时，a = 2，Y为氟原子或1价全氟有机基团）。

6. 发明申请

US20080138685A1 Electrolyte material for polymer electrolyte fuel cells, electrolyte membrane and membrane/electrode assembly 有权
标题翻译：用于聚合物电解质燃料电池，电解质膜和膜/电极组件的电解质材料
公开(公告)号：US20080138685A1
公开(公告)日：2008-06-12
申请号：US12010589
申请日：2008-01-28
申请人： Isamu Kaneko , Tetsuji Shimohira , Atsushi Watakabe , Seigo Kotera , Satoru Hommura , Koichi Murata , Jyunichi Tayanagi , Susumu Saito
发明人： Isamu Kaneko , Tetsuji Shimohira , Atsushi Watakabe , Seigo Kotera , Satoru Hommura , Koichi Murata , Jyunichi Tayanagi , Susumu Saito
IPC分类号： H01M8/10 , C08J5/20
CPC分类号： C08J5/225 , C08J2327/12 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M2300/0082
摘要： To provide a polymer electrolyte material for polymer electrolyte fuel cells, which is an electrolyte material having a high ion exchange capacity and a low resistance, and which has a higher softening temperature than a conventional electrolyte material.An electrolyte material for polymer electrolyte fuel cells, which is made of a polymer containing repeating units based on a fluoromonomer having a radical polymerization reactivity, wherein the repeating units contain, in their side chains, a structure having ionic groups represented in the following formula (α) (provided that in the formula, each of Q1 and Q2 which are independent of each other, is a single bond or a perfluoroalkylene group that may have an etheric oxygen atom, provided that they are not single bonds at the same time, Rf1 is a perfluoroalkyl group which may have an etheric oxygen atom, and X is an oxygen atom, a nitrogen atom or a carbon atom, provided that when X is an oxygen atom, a=0, when X is a nitrogen atom, a=1, and when X is a carbon atom, a=2, and Y is a fluorine atom or a monovalent perfluoro organic group).
摘要翻译：本发明提供一种高分子电解质燃料电池用聚合物电解质材料，该高分子电解质材料是具有高离子交换能力和低电阻的电解质材料，其软化温度高于常规电解质材料。一种用于聚合物电解质燃料电池的电解质材料，其由含有具有自由基聚合反应性的含氟单体的重复单元的聚合物制成，其中重复单元在其侧链中包含具有下式表示的离子基团的结构（ α）（条件是在该式中，彼此独立的Q 1和Q 2各自是单键或可具有醚的全氟亚烷基氧原子，条件是它们不是同时是单键，R f1是可以具有醚性氧原子的全氟烷基，X是氧原子，氮原子或碳原子条件是当X是氧原子时，a = 0，当X为氮原子时a = 1，当X为碳原子时a = 2，Y为氟原子或1价全氟有机基团）。

7. 发明授权

US4969982A Method for producing an alkali metal hydroxide and electrolytic cell useful for the method 失效
标题翻译：用于该方法的碱金属氢氧化物和电解槽的制造方法
公开(公告)号：US4969982A
公开(公告)日：1990-11-13
申请号：US941831
申请日：1986-12-15
申请人： Haruhisa Miyake , Isamu Kaneko , Atsushi Watakabe
发明人： Haruhisa Miyake , Isamu Kaneko , Atsushi Watakabe
IPC分类号： C25B9/00 , C08J5/22 , C25B1/46 , C25B9/08 , C25B13/08
CPC分类号： C08J5/2281 , C25B1/46
摘要： A method for producing an alkali metal hydroxide by electrolysis in an electrolytic cell comprising an anode compartment and a cathode compartment, which comprises supplying an alkali metal chloride to the anode compartment and water or a dilute alkali metal hydroxide to the cathode compartment, wherein a fluorine-containing cation exchange membrane comprising a first outer layer of a perfluorocarbon polymer having --SO.sub.3 M groups (wherein M is an alkali metal) with a thickness of at least 5 .mu.m, and a second layer of a perfluorocarbon polymer having --CO.sub.2 M groups (wherein M is an alkali metal) and a water content of from 2 to 7% by weight in a 45% wt % NaOH aqueous solution with a thickness of at least 5 .mu.m, the water content of the first layer being higher than that of the second layer, is disposed with the first layer facing the cathode compartment.
摘要翻译：一种在包括阳极室和阴极室的电解池中通过电解生产碱金属氢氧化物的方法，包括向阳极室供应碱金属氯化物，将水或稀碱金属氢氧化物供应至阴极室，其中氟包含阳离子交换膜，其包含具有-SO 3 M基团的全氟化碳聚合物（其中M为碱金属）的第一外层，其厚度为至少5μm，第二层具有-CO 2 M基团的全氟化碳聚合物（其中 M为碱金属），水分含量为2〜7重量％，厚度为5μm以上的45重量％NaOH水溶液中，第1层的含水量高于第二层设置有第一层面向阴极室。

8. 再颁专利

USRE41806E1 Process for producing a fluorine atom-containing sulfonyl fluoride compound 失效
标题翻译：含氟原子的磺酰氟化合物的制造方法
公开(公告)号：USRE41806E1
公开(公告)日：2010-10-05
申请号：US11812533
申请日：2007-06-19
申请人： Masahiro Ito , Kunio Watanabe , Takashi Okazoe , Isamu Kaneko , Daisuke Shirakawa
发明人： Masahiro Ito , Kunio Watanabe , Takashi Okazoe , Isamu Kaneko , Daisuke Shirakawa
IPC分类号： C07C309/00
CPC分类号： C07C309/82 , C07C51/60 , C07C303/22 , C07C59/135
摘要： The present invention provides a process whereby fluorine atom-containing sulfonyl fluoride compound(s) useful as e.g. materials for ion-exchange membranes, can be produced efficiently and at low cost without structural limitations while solving the difficulties in production. Namely, the present invention provides a process which comprises reacting XSO2RA-E1 (1) with RB-E2 (2) to form XSO2R4-E-RB (3), then reacting (3) with fluorine in a liquid phase to form FSO2RAF-EF-RBF (4), and further, decomposing the compound to obtain FSO2RAF-EFl (5), wherein RA is a bivalent organic group, E1 is a monovalent reactive group, RB is a monovalent organic group, E2 is a monovalent reactive group which is reactive with E1, E is a bivalent connecting group formed by the reaction of E1 with E2, RAF is a bivalent organic group formed by the fluorination of RA, etc., RBF is the same group as RB, etc., EF1 is a bivalent connecting group formed by the fluorination of E, etc., EF1 is a monovalent group formed by the decomposition of EF, and X is a halogen atom.
摘要翻译：本发明提供了一种可用于例如氟原子的磺酰氟化合物的方法。用于离子交换膜的材料可以在没有结构限制的情况下有效且低成本地生产，同时解决生产上的困难。即，本发明提供一种方法，其包括使XSO2RA-E1（1）与RB-E2（2）反应形成XSO 2 R 4 -E-RB（3），然后使（3）与氟在液相中反应形成FSO2RAF- EF-RBF（4），进一步分解化合物，得到FSO2RAF-EF1（5），其中RA为二价有机基团，E1为单价反应性基团，RB为一价有机基团，E2为单价反应基团 E与E1反应，E是通过E1与E2的反应形成的二价连接基团，RAF是通过RA的氟化形成的二价有机基团等，RBF与RB等同，EF1是通过E的氟化形成的二价连接基团等，EF1是通过EF的分解形成的一价基团，X是卤素原子。

9. 发明申请

US20070207409A1 FLUORINATED COMPOUND, AND FLUOROPOLYMER, PROCESS FOR ITS PRODUCTION AND RESIST COMPOSITION CONTAINING IT 失效
标题翻译：氟化合物和氟聚合物，其生产及其组合物的方法
公开(公告)号：US20070207409A1
公开(公告)日：2007-09-06
申请号：US11746316
申请日：2007-05-09
申请人： Yoko TAKEBE , Isamu Kaneko
发明人： Yoko TAKEBE , Isamu Kaneko
IPC分类号： C07C43/16
CPC分类号： G03F7/0046 , C07C69/65 , C08F36/20 , G03F7/0395 , G03F7/0397 , Y10S430/115 , Y10S430/146
摘要： To provide a fluoropolymer having functional groups and having high transparency in a wide wavelength region, and a resist composition comprising the fluoropolymer. A fluoropolymer (A) having monomer units formed by polymerization of a fluorinated diene represented by the following formula (1): CF2═CFCH2CH-Q-CH2CH═CH2 (1) wherein Q is (CH2)aC(CF3)2OR4 (wherein a is an integer of from 0 to 3, R4 is an alkyl group or a fluorinated alkyl group having at most 20 carbon atoms which may have an etheric oxygen atom, an alkoxycarbonyl group having at most 6 carbon atoms, or CH2R5 (wherein R5 is an alkoxycarbonyl group having at most 6 carbon atoms)), or (CH2)dCOOR6 (wherein d is 0 or 1, and R6 is a hydrogen atom, or an alkyl group or a fluorinated alkyl group having at most 20 carbon atoms), a process for its production and a resist composition having the fluoropolymer (A) as a base.
摘要翻译：提供具有官能团并且在宽波长区域具有高透明度的含氟聚合物，以及包含含氟聚合物的抗蚀剂组合物。具有通过由下式（1）表示的氟化二烯的聚合形成的单体单元的含氟聚合物（A）：<？in-line-formula description =“In-line formula”end =“lead”？> CF 2 < - CHCH 2 CH-CH-CH 2 CH-CH 2（1）<β在线公式描述其中Q为（CH 2）2，C（CF 3）3）其中Q为（CH 3） >其中a为0〜3的整数，R 4为烷基或碳原子数为20以下的氟代烷基可以具有醚性氧原子的原子，具有至多6个碳原子的烷氧基羰基或CH 2 R 5（其中R 5）是具有至多6个碳原子的烷氧基羰基））或（CH 2）2 COR 6（其中d为0或1，以及 R 6是氢原子，或者具有至多20个碳原子的烷基或氟化烷基），其制备方法和抗蚀剂组合物将含氟聚合物（A）作为碱。

10. 发明授权

US07026416B2 Fluoropolymer 失效
标题翻译：含氟聚合物
公开(公告)号：US07026416B2
公开(公告)日：2006-04-11
申请号：US11124133
申请日：2005-05-09
申请人： Yasuhide Kawaguchi , Shinji Okada , Yoko Takebe , Osamu Yokokoji , Isamu Kaneko
发明人： Yasuhide Kawaguchi , Shinji Okada , Yoko Takebe , Osamu Yokokoji , Isamu Kaneko
IPC分类号： C08F136/16 , C08F236/16 , C08F36/16 , G03F7/039
CPC分类号： C08F214/18 , C08F36/20 , C08F2/60
摘要： To provide a fluoropolymer suitable for use as a base polymer for resist materials for excimer lasers having a wavelength of 250 nm or shorter.A fluoropolymer having a monomer unit formed by cyclopolymerization of a fluorinated diene compound represented by the following formula (3), CF2═CFCF2—C(CF3)(R5)—CH2CH═CH2 (3) wherein R5 is either a hydroxyl group blocked by —CHR7—O—R8 or an organic group having the hydroxyl group, and R8 is a cyclic saturated hydrocarbon such as a cycloalkyl group which may have a substituent, or an organic group having the cyclic saturated hydrocarbon.
摘要翻译：提供适合作为波长为250nm以下的准分子激光的抗蚀剂材料的基础聚合物的氟聚合物。具有由下式（3）表示的氟化二烯化合物的环化聚合形成的单体单元的含氟聚合物，<？in-line-formula description =“In-Line Formulas”end =“lead”→> CF 2 -CFCF 2 -C（CF 3）（R 5）CH 2 CH- （3）<？in-line-formula description =“In-line Formulas”end =“tail”？>其中R 5是羟基被封闭或具有羟基的有机基团，R 8为环状饱和烃，例如环烷基其可以具有取代基，或具有环状饱和烃的有机基团。

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