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1. 发明授权

US06794598B2 Arc electrodes for synthesis of carbon nanostructures 失效
标题翻译：用于合成碳纳米结构的电弧电极
公开(公告)号：US06794598B2
公开(公告)日：2004-09-21
申请号：US10433028
申请日：2003-07-25
申请人： Houjin Huang , Hisashi Kajiura , Mitsuaki Miyakoshi , Atsuo Yamada , Masashi Shiraishi
发明人： Houjin Huang , Hisashi Kajiura , Mitsuaki Miyakoshi , Atsuo Yamada , Masashi Shiraishi
IPC分类号： B23K1500
CPC分类号： B82Y30/00 , B82Y10/00 , H01J37/32055 , H01J37/32532 , H01J37/32541 , H01J37/3255 , Y10S977/843 , Y10S977/844 , Y10S977/896
摘要： An arc electrode structure, for producing carbon nanostructures, which includes a first electrode and two or more second electrodes disposed within a chamber is provided. The electrodes are connected to a voltage potential to produce an arc-plasma region. The first electrode has a sloped surface with a plurality of holes therein for holding catalyst. The first electrode's sloped surface, and the positioning of the plurality of second electrodes allows control of the direction and region of arc-plasma. Further, the first electrode has a central bore which may be either a blind bore, or a through bore. The blind bore collects unwanted deposits that slide off of the sloped surface of the first electrode. The throughbore either allows soot and carbon nanostructures to be removed from the chamber, or allows organic vapor to be introduced into the chamber. When the throughbore is used to introduce organic vapor into the chamber, the vapor is directed through the arc-plasma region so that carbon nanostructures are built up by a CVD process rather than being broken off of carbon electrodes.
摘要翻译：提供了一种用于制造碳纳米结构的电弧电极结构，其包括第一电极和设置在室内的两个或更多个第二电极。电极连接到电压电位以产生电弧等离子体区域。第一电极具有倾斜表面，其中具有多个孔用于保持催化剂。第一电极的倾斜表面和多个第二电极的定位允许控制电弧等离子体的方向和区域。此外，第一电极具有可以是盲孔或通孔的中心孔。盲孔收集从第一电极的倾斜表面滑出的不需要的沉积物。通孔可以允许煤烟和碳纳米结构从室中移出，或允许有机蒸汽被引入室中。当通孔用于将有机蒸汽引入室中时，蒸汽被引导通过电弧等离子体区域，使得碳纳米结构由CVD工艺构成，而不是被碳电极断开。

2. 发明授权

US06855231B2 Method and system for production fullerene 失效
标题翻译：生产富勒烯的方法和系统
公开(公告)号：US06855231B2
公开(公告)日：2005-02-15
申请号：US10018717
申请日：2001-04-18
申请人： Hisashi Kajiura , Mitsuaki Miyakoshi , Masashi Shiraishi , Masafumi Ata , Atsuo Yamada
发明人： Hisashi Kajiura , Mitsuaki Miyakoshi , Masashi Shiraishi , Masafumi Ata , Atsuo Yamada
IPC分类号： B01J19/08 , C01B31/02 , C07C6/00 , D01F9/12
CPC分类号： B82Y30/00 , B01J19/088 , B01J2219/0809 , B01J2219/082 , B01J2219/083 , B01J2219/0839 , B01J2219/0847 , B01J2219/0875 , B82Y40/00 , C01B32/15 , C01B32/152 , Y10S977/842
摘要： Methods and devices for producing fullerene are provided. The present invention includes a pair of electrodes spaced apart to define a region wherein an arc discharge can be conducted between the electrode pair and a gas containing carbon can be supplied to the region such that fullerene can be easily and readily produced.
摘要翻译：提供了制备富勒烯的方法和装置。本发明包括一对间隔开的电极，以限定能够在电极对和含有气体的气体之间传导电弧放电的区域，从而可以容易且容易地产生富勒烯。

3. 发明申请

US20050069480A1 Ultrasonic reflux system for one-step purification of carbon nanostructures 审中-公开
标题翻译：超声回流系统用于碳纳米结构的一步纯化
公开(公告)号：US20050069480A1
公开(公告)日：2005-03-31
申请号：US10433125
申请日：2001-12-07
申请人： Houjin Huang , Masashi Shiraishi , Atsuo Yamada , Hisashi Kajiura , Masafumi Ata
发明人： Houjin Huang , Masashi Shiraishi , Atsuo Yamada , Hisashi Kajiura , Masafumi Ata
IPC分类号： B82B3/00 , B01D11/02 , B01J19/10 , C01B31/02 , D01F9/12 , B01D3/14
CPC分类号： B82Y30/00 , B01D11/0219 , B01D11/0261 , B82Y40/00 , C01B32/17
摘要： Reflux systems and methods for purifying carbon nanostructures using same are provided. The reflux system includes a solvent flask, an extraction tube connected to the solvent flask by a siphon tube and a vapor tube each extending between the extraction tube and the solvent flask, and an energy application disposed around the bottom portion of the extraction tube. The reflux systems can be used in a one-step method of purifying carbon nanostructures that includes placing a soot sample that contains the carbon nanostructures and amorphous carbon in a filter and disposing the filter in the extraction tube.
摘要翻译：提供了使用其来净化碳纳米结构的回流系统和方法。回流系统包括溶剂烧瓶，通过虹吸管连接到溶剂烧瓶的提取管和各自在萃取管和溶剂烧瓶之间延伸的蒸气管，以及设置在提取管的底部周围的能量施加。回流系统可以用于净化碳纳米结构的一步法，其包括将含有碳纳米结构和无定形碳的烟灰样品放置在过滤器中并将过滤器设置在萃取管中。

4. 发明申请

US20090121605A1 METHOD OF MANUFACTURING TUBULAR CARBON MOLECULE AND TUBULAR CARBON MOLECULE, METHOD OF MANUFACTURING RECORDING APPARATUS AND RECORDING APPARATUS, METHOD OF MANUFACUTRING FIELD ELECTRON EMISSION DEVICE AND FIELD ELECTRON EMISSION DEVICE 失效
标题翻译：制造管状碳分子和管状碳分子的方法，制造记录装置和记录装置的方法，制造场致电子发射装置和场电子发射装置的方法
公开(公告)号：US20090121605A1
公开(公告)日：2009-05-14
申请号：US12353610
申请日：2009-01-14
申请人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kodono , Shigeaki Wachi , Masafumi Ata
发明人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kodono , Shigeaki Wachi , Masafumi Ata
IPC分类号： H01J1/02 , H01J9/02
CPC分类号： B82Y30/00 , B82Y10/00 , B82Y40/00 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/00
摘要： A method of manufacturing a tubular carbon molecule capable of regularly aligning a carbon nanotube with a finer spacing is provided. A catalyst is arranged on a material substrate (10) made of a semiconductor such as silicon (Si) and including iron (Fe) as a catalyst through the use of melting according to a modulated heat distribution (11). The heat distribution (11) is formed, for example, through diffracting an energy beam (12) by a diffraction grating (13). As a method of arranging the catalyst, for example, iron may be deposited in a planar shape or a projection shape in a position corresponding to the heat distribution (11), or the deposited iron may be used as a master to be transferred to another substrate. A carbon nanotube is grown through the use of the arranged catalyst. The grown carbon nanotube can be used as a recording apparatus, a field electron emission device, an FED or the like.
摘要翻译：提供了一种制造能够以更细的间隔规则地对准碳纳米管的管状碳分子的方法。通过使用根据调制的热分布（11）的熔化，将催化剂布置在由诸如硅（Si）的半导体和包括铁（Fe））作为催化剂的材料基板（10）上。热分布（11）例如通过衍射光栅（13）衍射能量束（12）而形成。作为布置催化剂的方法，例如，铁可以在对应于热分布（11）的位置中以平面形状或突起形状沉积，或者沉积的铁可以用作主转移到另一个基质。通过使用所配置的催化剂生长碳纳米管。生长的碳纳米管可以用作记录装置，场电子发射装置，FED等。

5. 发明申请

US20060108906A1 Production method for tubular carbon molecule and tubular carbon molecule, production method for recording device and recording device, production method for field electron emission element and field electron emission element, and production method for display unit and display unit 失效
标题翻译：管状碳分子和管状碳分子的制造方法，记录装置及记录装置的制造方法，场致发射元件和场电子发射元件的制造方法以及显示装置及显示装置的制造方法
公开(公告)号：US20060108906A1
公开(公告)日：2006-05-25
申请号：US10541936
申请日：2004-01-08
申请人： Dharam Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
发明人： Dharam Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
IPC分类号： H01J1/02
CPC分类号： B82Y30/00 , B82Y10/00 , B82Y40/00 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/00
摘要： A method of manufacturing a tubular carbon molecule capable of regularly aligning a carbon nanotube with a finer spacing is provided. A catalyst is arranged on a material substrate (10) made of a semiconductor such as silicon (Si) and including iron (Fe) as a catalyst through the use of melting according to a modulated heat distribution (11). The heat distribution (11) is formed, for example, through diffracting an energy beam (12) by a diffraction grating (13). As a method of arranging the catalyst, for example, iron may be deposited in a planar shape or a projection shape in a position corresponding to the heat distribution (11), or the deposited iron may be used as a master to be transferred to another substrate. A carbon nanotube is grown through the use of the arranged catalyst. The grown carbon nanotube can be used as a recording apparatus, a field electron emission device, an FED or the like.
摘要翻译：提供了一种制造能够以更细的间隔规则地对准碳纳米管的管状碳分子的方法。通过使用根据调制的热分布（11）的熔化，将催化剂布置在由诸如硅（Si）的半导体和包括铁（Fe））作为催化剂的材料基板（10）上。热分布（11）例如通过衍射光栅（13）衍射能量束（12）而形成。作为布置催化剂的方法，例如，铁可以在对应于热分布（11）的位置中以平面形状或突起形状沉积，或者沉积的铁可以用作母盘以转移到另一个基质。通过使用所配置的催化剂生长碳纳米管。生长的碳纳米管可以用作记录装置，场电子发射装置，FED等。

6. 发明授权

US07892063B2 Method of manufacturing tubular carbon molecule and tubular carbon molecule, method of manufacturing recording apparatus and recording apparatus, method of manufacturing field electron emission device and field electron emission device, and method of manufacturing display unit and display unit 失效
标题翻译：制造管状碳分子和管状碳分子的方法，制造记录装置和记录装置的方法，制造场致电子发射装置和场电子发射装置的方法以及制造显示单元和显示单元的方法
公开(公告)号：US07892063B2
公开(公告)日：2011-02-22
申请号：US12353610
申请日：2009-01-14
申请人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
发明人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
IPC分类号： H01J9/00
CPC分类号： B82Y30/00 , B82Y10/00 , B82Y40/00 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/00
摘要： A method of manufacturing a tubular carbon molecule capable of regularly aligning a carbon nanotube with a finer spacing is provided. A catalyst is arranged on a material substrate (10) made of a semiconductor such as silicon (Si) and including iron (Fe) as a catalyst through the use of melting according to a modulated heat distribution (11). The heat distribution (11) is formed, for example, through diffracting an energy beam (12) by a diffraction grating (13). As a method of arranging the catalyst, for example, iron may be deposited in a planar shape or a projection shape in a position corresponding to the heat distribution (11), or the deposited iron may be used as a master to be transferred to another substrate. A carbon nanotube is grown through the use of the arranged catalyst. The grown carbon nanotube can be used as a recording apparatus, a field electron emission device, an FED or the like.
摘要翻译：提供了一种制造能够以更细的间隔规则地对准碳纳米管的管状碳分子的方法。通过使用根据调制的热分布（11）的熔化，将催化剂布置在由诸如硅（Si）的半导体和包括铁（Fe））作为催化剂的材料基板（10）上。热分布（11）例如通过衍射光栅（13）衍射能量束（12）而形成。作为布置催化剂的方法，例如，铁可以在对应于热分布（11）的位置中以平面形状或突起形状沉积，或者沉积的铁可以用作主转移到另一个基质。通过使用所配置的催化剂生长碳纳米管。生长的碳纳米管可以用作记录装置，场电子发射装置，FED等。

7. 发明授权

US07828620B2 Method of manufacturing tubular carbon molecule and tubular carbon molecule, method of manufacturing field electron emission device and field electron emission device, and method of manufacturing display unit and display unit 失效
标题翻译：制造管状碳分子和管状碳分子的方法，制造场致电子发射器件和场电子发射器件的方法以及制造显示单元和显示单元的方法
公开(公告)号：US07828620B2
公开(公告)日：2010-11-09
申请号：US10541936
申请日：2004-01-08
申请人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
发明人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
IPC分类号： H01J9/00
CPC分类号： B82Y30/00 , B82Y10/00 , B82Y40/00 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/00
摘要： A method of manufacturing a tubular carbon molecule capable of regularly aligning a carbon nanotube with a finer spacing is provided. A catalyst is arranged on a material substrate (10) made of a semiconductor such as silicon (Si) and including iron (Fe) as a catalyst through the use of melting according to a modulated heat distribution (11). The heat distribution (11) is formed, for example, through diffracting an energy beam (12) by a diffraction grating (13). As a method of arranging the catalyst, for example, iron may be deposited in a planar shape or a projection shape in a position corresponding to the heat distribution (11), or the deposited iron may be used as a master to be transferred to another substrate. A carbon nanotube is grown through the use of the arranged catalyst. The grown carbon nanotube can be used as a recording apparatus, a field electron emission device, an FED or the like.
摘要翻译：提供了一种制造能够以更细的间隔规则地对准碳纳米管的管状碳分子的方法。通过使用根据调制的热分布（11）的熔化，将催化剂布置在由诸如硅（Si）的半导体和包括铁（Fe））作为催化剂的材料基板（10）上。热分布（11）例如通过衍射光栅（13）衍射能量束（12）而形成。作为布置催化剂的方法，例如，铁可以在对应于热分布（11）的位置中以平面形状或突起形状沉积，或者沉积的铁可以用作主转移到另一个基质。通过使用所配置的催化剂生长碳纳米管。生长的碳纳米管可以用作记录装置，场电子发射装置，FED等。

8. 发明授权

US07045240B2 Power generating apparatus having a proton conductor unit that includes a fullerene derivative 失效
标题翻译：具有包含富勒烯衍生物的质子导体单元的发电装置
公开(公告)号：US07045240B2
公开(公告)日：2006-05-16
申请号：US10466860
申请日：2002-01-09
申请人： Atsuo Yamada , Hisashi Kajiura , Masashi Shiraishi , Ryuichiro Maruyama , Yasuhiro Watanabe , Takahiro Nakamura , Hiroshi Miyazawa
发明人： Atsuo Yamada , Hisashi Kajiura , Masashi Shiraishi , Ryuichiro Maruyama , Yasuhiro Watanabe , Takahiro Nakamura , Hiroshi Miyazawa
IPC分类号： H01M8/10
CPC分类号： B82Y30/00 , H01M4/8605 , H01M4/90 , H01M4/92 , H01M8/04089 , H01M8/065 , H01M8/1004 , H01M8/1007 , H01M8/1016
摘要： A power generating apparatus includes a proton conductor unit, containing a fullerene derivative, a hydrogen electrode bonded to one surface of the proton conductor unit, an oxygen electrode bonded to the other surface of the proton conductor unit, and a hydrogen gas supplying unit for supplying a hydrogen gas at a pressure of approximately 0.2 to approximately 3.5 atm to the hydrogen electrode. The present power generating apparatus effectively suppresses transmission of hydrogen and oxygen gases so that it is possible to prevent the hydrogen gas from being emitted to atmosphere due to transmission as well as to prevent the oxygen gas from reaching the hydrogen electrode on transmission to prevent the hydrogen gas from being consumed without contributing to power generation.
摘要翻译：一种发电装置，包括含有富勒烯衍生物的质子导体单元，与质子导体单元的一个面接合的氢电极，与该质子导体单元的另一个表面接合的氧电极，以及供给压力为氢电极约0.2至约3.5atm的氢气。本发明的发电装置有效地抑制氢气和氧气的传输，从而可以防止氢气由于透过而被排放到大气中，并且防止氧气在透射时到达氢电极，以防止氢消耗的气体无助于发电。

9. 发明授权

US07037622B2 Carbonaceous material for hydrogen storage and method for preparation thereof, carbonaceous material having hydrogen absorbed therein and method for preparation thereof, cell and fuel cell using carbonaceous material having hydrogen absorbed therein 失效
标题翻译：用于储氢的碳质材料及其制备方法，其中吸收有氢的碳质材料及其制备方法，使用其中吸收有氢的碳质材料的电池和燃料电池
公开(公告)号：US07037622B2
公开(公告)日：2006-05-02
申请号：US10221812
申请日：2001-03-16
申请人： Eisuke Negishi , Masashi Shiraishi , Hisashi Kajiura
发明人： Eisuke Negishi , Masashi Shiraishi , Hisashi Kajiura
IPC分类号： H01M4/58
CPC分类号： B82Y30/00 , B01J20/20 , B01J20/205 , C01B3/0021 , D01F9/127 , H01M4/242 , H01M4/96 , H01M8/06 , H01M8/10 , Y02E60/325
摘要： A hydrogen-storing carbonaceous material is provided. The hydrogen-storing carbonaceous material is obtained by heating a carbonaceous material at lower than about 800° C. before hydrogen is stored under the pressure of hydrogen of about 50 atmospheric pressure or higher. The present invention also provides hydrogen-stored carbonaceous material that is obtained by hydrogen storage in the hydrogen-storing carbonaceous material under the pressure of hydrogen of about 50 atmospheric pressure or higher. This hydrogen-stored carbonaceous material is used for a battery or a fuel cell. The hydrogen-stored carbonaceous material is heated at lower than about 800° C. before the hydrogen is stored under the pressure of hydrogen of about 50 atmospheric pressure or higher, so that the hydrogen-storing carbonaceous material whose hydrogen storage capacity is greatly enhanced can be produced.
摘要翻译：提供了储氢的碳质材料。储氢碳质材料通过在氢气约50大气压或更高的氢气储存之前将碳质材料加热至低于约800℃而得到。本发明还提供了通过在约50大气压或更高的氢气压力下在储氢碳质材料中储氢而获得的储氢碳质材料。该储氢碳质材料用于电池或燃料电池。氢储存的碳质材料在氢气约50个大气压或更高的氢气储存之前加热至低于约800℃，从而可以大大提高储氢容量的储氢碳质材料生产。

10. 发明授权

US07014952B2 Hydrogen-storing carbonaceous material and method for producing the same, hydrogen-stored carbonaceous material and method for producing the same and battery and fuel cell using hydrogen-stored carbonaceous material 失效
标题翻译：储氢碳质材料及其制造方法，储氢碳质材料及其制造方法以及使用储氢碳质材料的电池和燃料电池
公开(公告)号：US07014952B2
公开(公告)日：2006-03-21
申请号：US10221888
申请日：2001-03-16
申请人： Masashi Shiraishi , Hisashi Kajiura , Eisuke Negishi , Masafumi Ata
发明人： Masashi Shiraishi , Hisashi Kajiura , Eisuke Negishi , Masafumi Ata
IPC分类号： H01M4/58
CPC分类号： B82Y30/00 , B01J20/20 , C01B3/0021 , D01F9/127 , H01M4/242 , H01M4/96 , H01M8/06 , H01M8/10 , Y02E60/325
摘要： A hydrogen-storing carbonaceous material is provided. The hydrogen-storing carbonaceous material is obtained by heating a carbonaceous material in a gas atmosphere including hydrogen gas and substantially including no reactive gas as impurity gas to store hydrogen. According to the present invention, since the surface of the carbonaceous material can be cleaned and hydrogen can be stored in the carbonaceous material in the same gas atmosphere and a hydrogen-stored carbonaceous material can be produced by controlling a heating process time in the gas atmosphere including the hydrogen gas and substantially including no reactive gas as the impurity gas. This can facilitate the use of the hydrogen-stored carbonaceous material as applied to devices, systems, processes and/or the like.
摘要翻译：提供了储氢的碳质材料。储氢碳质材料通过在包括氢气的气体气氛中加热含碳材料并且基本上不包含反应性气体作为杂质气体来储存氢气而获得。根据本发明，由于能够清洗碳质材料的表面，并且可以在相同的气体气氛中将碳存储在碳质材料中，并且可以通过控制气体气氛中的加热处理时间来制造氢储存的碳质材料包括氢气并且基本上不包括作为杂质气体的反应气体。这可以有利于将氢储存的碳质材料应用于装置，系统，工艺和/或类似物上。

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