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1. 发明授权

US07892063B2 Method of manufacturing tubular carbon molecule and tubular carbon molecule, method of manufacturing recording apparatus and recording apparatus, method of manufacturing field electron emission device and field electron emission device, and method of manufacturing display unit and display unit 失效
标题翻译：制造管状碳分子和管状碳分子的方法，制造记录装置和记录装置的方法，制造场致电子发射装置和场电子发射装置的方法以及制造显示单元和显示单元的方法
公开(公告)号：US07892063B2
公开(公告)日：2011-02-22
申请号：US12353610
申请日：2009-01-14
申请人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
发明人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
IPC分类号： H01J9/00
CPC分类号： B82Y30/00 , B82Y10/00 , B82Y40/00 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/00
摘要： A method of manufacturing a tubular carbon molecule capable of regularly aligning a carbon nanotube with a finer spacing is provided. A catalyst is arranged on a material substrate (10) made of a semiconductor such as silicon (Si) and including iron (Fe) as a catalyst through the use of melting according to a modulated heat distribution (11). The heat distribution (11) is formed, for example, through diffracting an energy beam (12) by a diffraction grating (13). As a method of arranging the catalyst, for example, iron may be deposited in a planar shape or a projection shape in a position corresponding to the heat distribution (11), or the deposited iron may be used as a master to be transferred to another substrate. A carbon nanotube is grown through the use of the arranged catalyst. The grown carbon nanotube can be used as a recording apparatus, a field electron emission device, an FED or the like.
摘要翻译：提供了一种制造能够以更细的间隔规则地对准碳纳米管的管状碳分子的方法。通过使用根据调制的热分布（11）的熔化，将催化剂布置在由诸如硅（Si）的半导体和包括铁（Fe））作为催化剂的材料基板（10）上。热分布（11）例如通过衍射光栅（13）衍射能量束（12）而形成。作为布置催化剂的方法，例如，铁可以在对应于热分布（11）的位置中以平面形状或突起形状沉积，或者沉积的铁可以用作主转移到另一个基质。通过使用所配置的催化剂生长碳纳米管。生长的碳纳米管可以用作记录装置，场电子发射装置，FED等。

2. 发明授权

US07828620B2 Method of manufacturing tubular carbon molecule and tubular carbon molecule, method of manufacturing field electron emission device and field electron emission device, and method of manufacturing display unit and display unit 失效
标题翻译：制造管状碳分子和管状碳分子的方法，制造场致电子发射器件和场电子发射器件的方法以及制造显示单元和显示单元的方法
公开(公告)号：US07828620B2
公开(公告)日：2010-11-09
申请号：US10541936
申请日：2004-01-08
申请人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
发明人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
IPC分类号： H01J9/00
CPC分类号： B82Y30/00 , B82Y10/00 , B82Y40/00 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/00
摘要： A method of manufacturing a tubular carbon molecule capable of regularly aligning a carbon nanotube with a finer spacing is provided. A catalyst is arranged on a material substrate (10) made of a semiconductor such as silicon (Si) and including iron (Fe) as a catalyst through the use of melting according to a modulated heat distribution (11). The heat distribution (11) is formed, for example, through diffracting an energy beam (12) by a diffraction grating (13). As a method of arranging the catalyst, for example, iron may be deposited in a planar shape or a projection shape in a position corresponding to the heat distribution (11), or the deposited iron may be used as a master to be transferred to another substrate. A carbon nanotube is grown through the use of the arranged catalyst. The grown carbon nanotube can be used as a recording apparatus, a field electron emission device, an FED or the like.
摘要翻译：提供了一种制造能够以更细的间隔规则地对准碳纳米管的管状碳分子的方法。通过使用根据调制的热分布（11）的熔化，将催化剂布置在由诸如硅（Si）的半导体和包括铁（Fe））作为催化剂的材料基板（10）上。热分布（11）例如通过衍射光栅（13）衍射能量束（12）而形成。作为布置催化剂的方法，例如，铁可以在对应于热分布（11）的位置中以平面形状或突起形状沉积，或者沉积的铁可以用作主转移到另一个基质。通过使用所配置的催化剂生长碳纳米管。生长的碳纳米管可以用作记录装置，场电子发射装置，FED等。

3. 发明申请

US20090121605A1 METHOD OF MANUFACTURING TUBULAR CARBON MOLECULE AND TUBULAR CARBON MOLECULE, METHOD OF MANUFACTURING RECORDING APPARATUS AND RECORDING APPARATUS, METHOD OF MANUFACUTRING FIELD ELECTRON EMISSION DEVICE AND FIELD ELECTRON EMISSION DEVICE 失效
标题翻译：制造管状碳分子和管状碳分子的方法，制造记录装置和记录装置的方法，制造场致电子发射装置和场电子发射装置的方法
公开(公告)号：US20090121605A1
公开(公告)日：2009-05-14
申请号：US12353610
申请日：2009-01-14
申请人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kodono , Shigeaki Wachi , Masafumi Ata
发明人： Dharam Pal Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kodono , Shigeaki Wachi , Masafumi Ata
IPC分类号： H01J1/02 , H01J9/02
CPC分类号： B82Y30/00 , B82Y10/00 , B82Y40/00 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/00
摘要： A method of manufacturing a tubular carbon molecule capable of regularly aligning a carbon nanotube with a finer spacing is provided. A catalyst is arranged on a material substrate (10) made of a semiconductor such as silicon (Si) and including iron (Fe) as a catalyst through the use of melting according to a modulated heat distribution (11). The heat distribution (11) is formed, for example, through diffracting an energy beam (12) by a diffraction grating (13). As a method of arranging the catalyst, for example, iron may be deposited in a planar shape or a projection shape in a position corresponding to the heat distribution (11), or the deposited iron may be used as a master to be transferred to another substrate. A carbon nanotube is grown through the use of the arranged catalyst. The grown carbon nanotube can be used as a recording apparatus, a field electron emission device, an FED or the like.
摘要翻译：提供了一种制造能够以更细的间隔规则地对准碳纳米管的管状碳分子的方法。通过使用根据调制的热分布（11）的熔化，将催化剂布置在由诸如硅（Si）的半导体和包括铁（Fe））作为催化剂的材料基板（10）上。热分布（11）例如通过衍射光栅（13）衍射能量束（12）而形成。作为布置催化剂的方法，例如，铁可以在对应于热分布（11）的位置中以平面形状或突起形状沉积，或者沉积的铁可以用作主转移到另一个基质。通过使用所配置的催化剂生长碳纳米管。生长的碳纳米管可以用作记录装置，场电子发射装置，FED等。

4. 发明申请

US20060108906A1 Production method for tubular carbon molecule and tubular carbon molecule, production method for recording device and recording device, production method for field electron emission element and field electron emission element, and production method for display unit and display unit 失效
标题翻译：管状碳分子和管状碳分子的制造方法，记录装置及记录装置的制造方法，场致发射元件和场电子发射元件的制造方法以及显示装置及显示装置的制造方法
公开(公告)号：US20060108906A1
公开(公告)日：2006-05-25
申请号：US10541936
申请日：2004-01-08
申请人： Dharam Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
发明人： Dharam Gosain , Hisashi Kajiura , Ryuichiro Maruyama , Masashi Shiraishi , Houjin Huang , Koji Kadono , Shigeaki Wachi , Masafumi Ata
IPC分类号： H01J1/02
CPC分类号： B82Y30/00 , B82Y10/00 , B82Y40/00 , C01B32/162 , H01J1/304 , H01J9/025 , H01J2201/30469 , H01J2329/00
摘要： A method of manufacturing a tubular carbon molecule capable of regularly aligning a carbon nanotube with a finer spacing is provided. A catalyst is arranged on a material substrate (10) made of a semiconductor such as silicon (Si) and including iron (Fe) as a catalyst through the use of melting according to a modulated heat distribution (11). The heat distribution (11) is formed, for example, through diffracting an energy beam (12) by a diffraction grating (13). As a method of arranging the catalyst, for example, iron may be deposited in a planar shape or a projection shape in a position corresponding to the heat distribution (11), or the deposited iron may be used as a master to be transferred to another substrate. A carbon nanotube is grown through the use of the arranged catalyst. The grown carbon nanotube can be used as a recording apparatus, a field electron emission device, an FED or the like.
摘要翻译：提供了一种制造能够以更细的间隔规则地对准碳纳米管的管状碳分子的方法。通过使用根据调制的热分布（11）的熔化，将催化剂布置在由诸如硅（Si）的半导体和包括铁（Fe））作为催化剂的材料基板（10）上。热分布（11）例如通过衍射光栅（13）衍射能量束（12）而形成。作为布置催化剂的方法，例如，铁可以在对应于热分布（11）的位置中以平面形状或突起形状沉积，或者沉积的铁可以用作母盘以转移到另一个基质。通过使用所配置的催化剂生长碳纳米管。生长的碳纳米管可以用作记录装置，场电子发射装置，FED等。

5. 发明申请

US20050069480A1 Ultrasonic reflux system for one-step purification of carbon nanostructures 审中-公开
标题翻译：超声回流系统用于碳纳米结构的一步纯化
公开(公告)号：US20050069480A1
公开(公告)日：2005-03-31
申请号：US10433125
申请日：2001-12-07
申请人： Houjin Huang , Masashi Shiraishi , Atsuo Yamada , Hisashi Kajiura , Masafumi Ata
发明人： Houjin Huang , Masashi Shiraishi , Atsuo Yamada , Hisashi Kajiura , Masafumi Ata
IPC分类号： B82B3/00 , B01D11/02 , B01J19/10 , C01B31/02 , D01F9/12 , B01D3/14
CPC分类号： B82Y30/00 , B01D11/0219 , B01D11/0261 , B82Y40/00 , C01B32/17
摘要： Reflux systems and methods for purifying carbon nanostructures using same are provided. The reflux system includes a solvent flask, an extraction tube connected to the solvent flask by a siphon tube and a vapor tube each extending between the extraction tube and the solvent flask, and an energy application disposed around the bottom portion of the extraction tube. The reflux systems can be used in a one-step method of purifying carbon nanostructures that includes placing a soot sample that contains the carbon nanostructures and amorphous carbon in a filter and disposing the filter in the extraction tube.
摘要翻译：提供了使用其来净化碳纳米结构的回流系统和方法。回流系统包括溶剂烧瓶，通过虹吸管连接到溶剂烧瓶的提取管和各自在萃取管和溶剂烧瓶之间延伸的蒸气管，以及设置在提取管的底部周围的能量施加。回流系统可以用于净化碳纳米结构的一步法，其包括将含有碳纳米结构和无定形碳的烟灰样品放置在过滤器中并将过滤器设置在萃取管中。

6. 发明申请

US20080315746A1 Method of Manufacturing Fine Structure, Fine Structure, Display Unit, Method of Manufacturing Recoding Device, and Recoding Device 审中-公开
标题翻译：制造精细结构，精细结构，显示单元，制造再编码装置的方法和重新编码装置的方法
公开(公告)号：US20080315746A1
公开(公告)日：2008-12-25
申请号：US10570077
申请日：2004-08-31
申请人： Dharam Pal Gosain , Hisashi Kajiura , Yosuke Murakami , Masafumi Ata
发明人： Dharam Pal Gosain , Hisashi Kajiura , Yosuke Murakami , Masafumi Ata
IPC分类号： H01J17/04 , B32B3/20 , G11B5/64 , H01L21/306
CPC分类号： H01J9/025 , G11B5/855 , H01J1/3042 , Y10T428/24744
摘要： A method of manufacturing a fine structure capable of accurately controlling formation positions of tubular structures made of carbon or the like is provided. Column-shaped protrusions (11) are formed on a substrate (10). Next, a catalyst material (20) such as iron (Fe) is adhered to the substrate (10). Subsequently, by providing the substrate (10) with heat treatment, the catalyst material (20) is melted and agglomerated on the side faces (11A) of the protrusions (11), and thereby cyclic catalyst patterns made of the catalyst material (20) are formed on the side faces (11A) of the protrusions (11). After that, tubular structures (30) in a state of tube are grown by using the catalyst patterns. The tubular structures (30) become carbon (nano) pipes, which are raised from the side faces (11A) of the protrusions (11) and whose ends (30A) are opened. The tubular structures (30) can be formed correspondingly to the positions of the protrusions (11) accurately.
摘要翻译：提供一种能够精确控制由碳等制成的管状结构的形成位置的精细结构体的制造方法。柱状突起（11）形成在基板（10）上。接下来，将诸如铁（Fe）的催化剂材料（20）粘合到基板（10）上。随后，通过使基板（10）进行热处理，催化剂材料（20）在突起（11）的侧面（11A）上熔化并凝聚，由此由催化剂材料（20）制成的环状催化剂图案，形成在突起（11）的侧面（11A）上。之后，通过使用催化剂图案生长处于管状状的管状结构（30）。管状结构（30）成为从突起（11）的侧面（11A）升起并且其端部（30A）打开的碳（纳米）管。可以精确地对应于突起（11）的位置形成管状结构（30）。

7. 发明申请

US20080124502A1 Carbon Nanotube and Manufacturing Method Thereof, and Carbon Nanotube Manufacturing Equipment 审中-公开
标题翻译：碳纳米管及其制造方法和碳纳米管制造设备
公开(公告)号：US20080124502A1
公开(公告)日：2008-05-29
申请号：US10564565
申请日：2004-07-15
申请人： Houjin Huang , Hisashi Kajiura , Masafumi Ata
发明人： Houjin Huang , Hisashi Kajiura , Masafumi Ata
IPC分类号： D01F9/12 , C01B31/00 , C01B31/02 , B01J8/00
CPC分类号： D01F9/127 , B82Y30/00 , B82Y40/00 , C01B32/162 , C01B32/164 , C01B2202/02 , C01B2202/04 , C01B2202/34 , Y10T428/13
摘要： A manufacturing method of carbon nanotubes capable of mass-producing DWCNT with high throughput and a low defect incidence ratio is provided. In a vacuum chamber (1), a first electrode (2) having a hollow (2a) and a rod-like second electrode (3) are included. Inert gas such as helium gas, nitrogen gas, and argon gas is introduced into the vacuum chamber (1), the atmosphere not containing hydrogen gas and oxygen gas is created, and in this state, arc discharge is generated between the first electrode (2) and the second electrode (3). The heat generated by arc discharge is moderately stored on the surface of the inner side surrounded by the first electrode (2), and temperatures on the surface of the first electrode (2) are maintained at the temperatures suitable for producing the DWCNT (8). Thereby, the thready DWCNT (8) can be continuously produced without pause starting with a catalyst (6).
摘要翻译：提供能够大量生产高产量和低缺陷发生率的DWCNT的碳纳米管的制造方法。在真空室（1）中，包括具有中空部（2a）和棒状第二电极（3）的第一电极（2）。惰性气体如氦气，氮气和氩气被引入真空室（1），不产生氢气和氧气的气氛，在这种状态下，在第一电极（2））和第二电极（3）。由电弧放电产生的热适度地储存在由第一电极（2）包围的内侧的表面上，并且第一电极（2）的表面上的温度保持在适于生产DWCNT（8）的温度下，。因此，可以不间断地从催化剂（6）开始直接制造DWCNT（8）。

8. 发明授权

US06794598B2 Arc electrodes for synthesis of carbon nanostructures 失效
标题翻译：用于合成碳纳米结构的电弧电极
公开(公告)号：US06794598B2
公开(公告)日：2004-09-21
申请号：US10433028
申请日：2003-07-25
申请人： Houjin Huang , Hisashi Kajiura , Mitsuaki Miyakoshi , Atsuo Yamada , Masashi Shiraishi
发明人： Houjin Huang , Hisashi Kajiura , Mitsuaki Miyakoshi , Atsuo Yamada , Masashi Shiraishi
IPC分类号： B23K1500
CPC分类号： B82Y30/00 , B82Y10/00 , H01J37/32055 , H01J37/32532 , H01J37/32541 , H01J37/3255 , Y10S977/843 , Y10S977/844 , Y10S977/896
摘要： An arc electrode structure, for producing carbon nanostructures, which includes a first electrode and two or more second electrodes disposed within a chamber is provided. The electrodes are connected to a voltage potential to produce an arc-plasma region. The first electrode has a sloped surface with a plurality of holes therein for holding catalyst. The first electrode's sloped surface, and the positioning of the plurality of second electrodes allows control of the direction and region of arc-plasma. Further, the first electrode has a central bore which may be either a blind bore, or a through bore. The blind bore collects unwanted deposits that slide off of the sloped surface of the first electrode. The throughbore either allows soot and carbon nanostructures to be removed from the chamber, or allows organic vapor to be introduced into the chamber. When the throughbore is used to introduce organic vapor into the chamber, the vapor is directed through the arc-plasma region so that carbon nanostructures are built up by a CVD process rather than being broken off of carbon electrodes.
摘要翻译：提供了一种用于制造碳纳米结构的电弧电极结构，其包括第一电极和设置在室内的两个或更多个第二电极。电极连接到电压电位以产生电弧等离子体区域。第一电极具有倾斜表面，其中具有多个孔用于保持催化剂。第一电极的倾斜表面和多个第二电极的定位允许控制电弧等离子体的方向和区域。此外，第一电极具有可以是盲孔或通孔的中心孔。盲孔收集从第一电极的倾斜表面滑出的不需要的沉积物。通孔可以允许煤烟和碳纳米结构从室中移出，或允许有机蒸汽被引入室中。当通孔用于将有机蒸汽引入室中时，蒸汽被引导通过电弧等离子体区域，使得碳纳米结构由CVD工艺构成，而不是被碳电极断开。

9. 发明授权

US07045240B2 Power generating apparatus having a proton conductor unit that includes a fullerene derivative 失效
标题翻译：具有包含富勒烯衍生物的质子导体单元的发电装置
公开(公告)号：US07045240B2
公开(公告)日：2006-05-16
申请号：US10466860
申请日：2002-01-09
申请人： Atsuo Yamada , Hisashi Kajiura , Masashi Shiraishi , Ryuichiro Maruyama , Yasuhiro Watanabe , Takahiro Nakamura , Hiroshi Miyazawa
发明人： Atsuo Yamada , Hisashi Kajiura , Masashi Shiraishi , Ryuichiro Maruyama , Yasuhiro Watanabe , Takahiro Nakamura , Hiroshi Miyazawa
IPC分类号： H01M8/10
CPC分类号： B82Y30/00 , H01M4/8605 , H01M4/90 , H01M4/92 , H01M8/04089 , H01M8/065 , H01M8/1004 , H01M8/1007 , H01M8/1016
摘要： A power generating apparatus includes a proton conductor unit, containing a fullerene derivative, a hydrogen electrode bonded to one surface of the proton conductor unit, an oxygen electrode bonded to the other surface of the proton conductor unit, and a hydrogen gas supplying unit for supplying a hydrogen gas at a pressure of approximately 0.2 to approximately 3.5 atm to the hydrogen electrode. The present power generating apparatus effectively suppresses transmission of hydrogen and oxygen gases so that it is possible to prevent the hydrogen gas from being emitted to atmosphere due to transmission as well as to prevent the oxygen gas from reaching the hydrogen electrode on transmission to prevent the hydrogen gas from being consumed without contributing to power generation.
摘要翻译：一种发电装置，包括含有富勒烯衍生物的质子导体单元，与质子导体单元的一个面接合的氢电极，与该质子导体单元的另一个表面接合的氧电极，以及供给压力为氢电极约0.2至约3.5atm的氢气。本发明的发电装置有效地抑制氢气和氧气的传输，从而可以防止氢气由于透过而被排放到大气中，并且防止氧气在透射时到达氢电极，以防止氢消耗的气体无助于发电。

10. 发明授权

US06855231B2 Method and system for production fullerene 失效
标题翻译：生产富勒烯的方法和系统
公开(公告)号：US06855231B2
公开(公告)日：2005-02-15
申请号：US10018717
申请日：2001-04-18
申请人： Hisashi Kajiura , Mitsuaki Miyakoshi , Masashi Shiraishi , Masafumi Ata , Atsuo Yamada
发明人： Hisashi Kajiura , Mitsuaki Miyakoshi , Masashi Shiraishi , Masafumi Ata , Atsuo Yamada
IPC分类号： B01J19/08 , C01B31/02 , C07C6/00 , D01F9/12
CPC分类号： B82Y30/00 , B01J19/088 , B01J2219/0809 , B01J2219/082 , B01J2219/083 , B01J2219/0839 , B01J2219/0847 , B01J2219/0875 , B82Y40/00 , C01B32/15 , C01B32/152 , Y10S977/842
摘要： Methods and devices for producing fullerene are provided. The present invention includes a pair of electrodes spaced apart to define a region wherein an arc discharge can be conducted between the electrode pair and a gas containing carbon can be supplied to the region such that fullerene can be easily and readily produced.
摘要翻译：提供了制备富勒烯的方法和装置。本发明包括一对间隔开的电极，以限定能够在电极对和含有气体的气体之间传导电弧放电的区域，从而可以容易且容易地产生富勒烯。

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