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1. 发明授权

US4207128A Reactive polyurethane coatings 失效
标题翻译：反应性聚氨酯涂料
公开(公告)号：US4207128A
公开(公告)日：1980-06-10
申请号：US734857
申请日：1976-10-22
申请人： Harro Traubel , Klaus Konig , Hans J. Muller , Bruno Zorn
发明人： Harro Traubel , Klaus Konig , Hans J. Muller , Bruno Zorn
IPC分类号： B05D7/12 , B05D7/24 , B05D7/26 , C08G18/08 , C08J9/28 , D06M15/564 , D06N3/14 , B32B31/26
CPC分类号： B05D7/12 , C08G18/0842 , D06M15/564 , D06N3/14
摘要： This invention is concerned with a process for producing microporous coatings comprising (1) mixing an NCO-prepolymer prepared from polyisocyanates with compounds containing at least two isocyanate-reactive hydrogen atoms with about 3 to 40% by weight, based on the NCO-prepolymer, of a substantially inert, non-migrating liquid organic compound miscible with said NCO-prepolymer as a plasticizer; (2) adding about 3 to 300 weight % of water, based on the NCO-prepolymer, into the NCO-prepolymer-plasticizer mixture to form a water-in-oil emulsion; (3) adding a polyamine in a quantity substantially equivalent to the isocyanate groups; (4) applying a coating of the water-in-oil emulsion to a substrate; and (5) hardening the coating by evaporating the chemically unbound water from said coating.
摘要翻译：本发明涉及一种生产微孔涂层的方法，其包括（1）基于NCO-预聚物将由多异氰酸酯制备的NCO-预聚物与含有至少两个异氰酸酯反应性氢原子的化合物混合约3至40重量％与所述NCO预聚物可混溶的基本惰性的非迁移性液体有机化合物作为增塑剂; （2）将约3〜300重量％的水作为NCO-预聚物加入到NCO-预聚物 - 增塑剂混合物中以形成油包水乳液; （3）加入基本上等同于异氰酸酯基团的量的多胺; （4）将油包水乳液的涂层施加到基材上; 和（5）通过蒸发来自所述涂层的化学未结合的水来硬化涂层。

2. 发明授权

US5917083A Process for the manufacture of allophanates having isocyanate groups 失效
标题翻译：制备具有异氰酸酯基团的脲基甲酸酯的方法
公开(公告)号：US5917083A
公开(公告)日：1999-06-29
申请号：US907670
申请日：1997-08-08
申请人： Klaus Konig , Helmut Reiff , Christian Wamprecht , Harro Traubel
发明人： Klaus Konig , Helmut Reiff , Christian Wamprecht , Harro Traubel
IPC分类号： B01J27/232 , B01J31/02 , B01J31/04 , C07B61/00 , C07C273/02 , C07C275/60 , C07D273/04 , C08G18/02 , C08G18/78 , C07C269/00
CPC分类号： C08G18/7887 , C07D273/04 , C08G18/7837
摘要： The present invention relates to a process for preparing an isocyanate group-containing allophanate corresponding to formula (I) ##STR1## wherein R represents the residue obtained by removing the isocyanate groups from a (cyclo)aliphatic or araliphatic diisocyanate,Y represents the represents an m-valent residue obtained by removing the hydroxyl groups from a (poly)hydroxyl compound having m OH groups andn and m are the same or different and have a value of 1 to 5, by reacting an isocyanate group-containing oxadiazinetrione with a primary alcohol in the presence of a basic catalyst having a pKa value of >6.
摘要翻译：本发明涉及一种制备对应于式（I）的异氰酸酯基脲基甲酸酯的方法，其中R表示通过从（环）脂族或芳脂族二异氰酸酯除去异氰酸酯基而获得的残基，Y表示m价通过从具有m个OH基团的（多）羟基化合物除去羟基而得到的残基和n和m相同或不同，通过使含异氰酸酯基的恶二唑啉与伯醇反应而得到的值为1〜5 存在pKa值> 6的碱性催化剂。

3. 发明授权

US5846383A Process for producing structurally resistant paper 失效
标题翻译：生产结构抗性纸的方法
公开(公告)号：US5846383A
公开(公告)日：1998-12-08
申请号：US945525
申请日：1997-10-27
申请人： Harro Traubel , Klaus Konig
发明人： Harro Traubel , Klaus Konig
IPC分类号： D21H19/24 , C08G18/80 , D21H17/08 , D21H17/46 , D21H21/20
CPC分类号： D21H21/20 , C08G18/8009 , D21H17/08
摘要： Process for the production of structurally strong papers (or paper-like materials) which have a terminable strength by treatment of paper in the pulp or of finished paper in the surface with 0.0001 to 50% by weight, preferably 0.01-25% by weight (based on the pulp), of a mixture of isocyanates which contain on average at least two isocyanate groups and of which at least 20% by weight (preferably at least 50%) are those in which the NCO groups are bonded via an organic radical which contains at least one ester and/or amide group in the main chain.
摘要翻译： PCT No.PCT / EP96 / 01670 Sec。 371日期1997年10月27日第 102（e）1997年10月27日PCT PCT 1996年4月22日PCT公布。第WO96 / 35019号公报日期1996年11月7日生产结构坚固的纸（或纸状材料）的方法，其具有通过在纸浆或表面处理纸中处理纸而具有可终止强度，其具有0.0001至50重量％，优选为0.01- 25重量％（基于纸浆），含有平均至少两个异氰酸酯基的异氰酸酯混合物，其中至少20重量％（优选至少50重量％）为NCO基团键合的异氰酸酯混合物通过在主链中含有至少一个酯和/或酰胺基团的有机基团。

4. 发明授权

US6054528A Aqueous coating adhesive and sealant compositions containing oxadiazolinones and polyamines 失效
标题翻译：水性涂料粘合剂和含有恶二唑啉酮和多胺的密封剂组合物
公开(公告)号：US6054528A
公开(公告)日：2000-04-25
申请号：US118244
申请日：1998-07-17
申请人： Josef Pedain , Klaus Konig , Peter Heitkamper , Manfred Schonfelder
发明人： Josef Pedain , Klaus Konig , Peter Heitkamper , Manfred Schonfelder
IPC分类号： C08K5/17 , C07D271/10 , C07D271/113 , C08G73/02 , C08K5/353 , C08L101/00 , C09D5/00 , C09D7/12 , C09D179/02 , C09J11/06 , C09J179/02 , C08L75/00 , B32B27/08 , B32B27/26 , B32B27/40 , C08G73/00
CPC分类号： C07D271/113 , C08G73/0233 , C09D179/02 , C09J179/02 , Y10T428/31551
摘要： The present invention relates to aqueous compositions containinga) bis(1,3,4-oxadiazolin-5-ones) corresponding to formula (I) ##STR1## wherein R represents a single bond or a divalent aliphatic, araliphatic or aromatic radical having 1 to 18 carbon atoms andb) organic polyamines or polyamine blends having an average of more than 2 NH-- and/or NH.sub.2 -- groups.The present invention also relates to coatings, adhesives or sealants prepared from these aqueous compositions, in particular automotive clear coats.
摘要翻译：本发明涉及含有a）对应于式（I）的双（1,3,4-恶二唑啉-5-酮）的含水组合物，其中R表示单键或具有1至18个碳原子的二价脂族，芳脂族或芳族基团原子和b）平均具有多于2个NH-和/或NH 2 - 基团的有机多胺或多胺共混物。本发明还涉及由这些含水组合物，特别是汽车清漆制备的涂料，粘合剂或密封剂。

5. 发明授权

US5612408A Polyurethane-based thickeners for aqueous compositions 失效
标题翻译：用于水性组合物的聚氨酯类增稠剂
公开(公告)号：US5612408A
公开(公告)日：1997-03-18
申请号：US593036
申请日：1996-01-29
申请人： Klaus Konig , Jurgen Schwindt , Jan Mazanek , Josef Pedain , Manfred Dietrich , Gerhard Klein , Karl-Roland Jerg
发明人： Klaus Konig , Jurgen Schwindt , Jan Mazanek , Josef Pedain , Manfred Dietrich , Gerhard Klein , Karl-Roland Jerg
IPC分类号： C09K3/00 , C08G18/28 , C08G18/48 , C08G65/28 , C08L75/00 , C08L75/08 , C09D7/00 , C09D175/00 , C09D175/04 , C08G18/12 , C08G18/42
CPC分类号： C08G18/4833 , C08G18/283 , C09D7/002 , C08L75/04
摘要： The present invention relates to a process for the preparation of polyurethanes suitable for use as thickeners for aqueous compositions by reacting at an NCO/OH equivalent ratio of 0.9:1 to 1.2:1a) a polyether component having an OH number of 10 to 30 mg KOH/g and obtained by the alkoxylation of a mixture ofa1) 30 to 80 mole % of a monofunctional alcohol or alkylphenol having 8 to 30 carbon atoms,a2) 2 to 10 mole % of sodium hydroxide or potassium hydroxide,a3) 10 to 60 mole % of water anda4) 0 to 10 mole % of a trihydric to hexahydric alcohol having a molecular weight of 92 to 600, with ethylene oxide or a mixture of ethylene oxide with up to 20 mole %, based on the total moles of alkylene oxides, of propylene oxide, in which the percentages of a1) to a4) add up to 100,withb) a polyisocyanate component containing at least one organic diisocyanate, optionally in admixture with up to 20 mole %, based on the total moles of component b), of higher than difunctional polyisocyanates.The invention also relates to the polyurethanes obtainable by this method and their use, optionally in combination with other thickeners, for the thickening of aqueous systems.
摘要翻译：本发明涉及一种制备适合用作水性组合物增稠剂的聚氨酯的方法，其通过以0.9:1至1.2:1的NCO / OH当量比反应a）OH数为10至30的聚醚组分 mg KOH / g，通过a1）30〜80摩尔％的单官能醇或碳原子数为8〜30的烷基酚的混合物的烷氧基化得到，a2）2〜10摩尔％的氢氧化钠或氢氧化钾，a3）10 至60摩尔％的水和a4）0至10摩尔％的分子量为92至600的三元至六元醇与环氧乙烷或环氧乙烷的混合物至多20摩尔％，基于总摩尔数的环氧丙烷，其中a1）至a4）的百分比加到100，其中b）含有至少一种有机二异氰酸酯的多异氰酸酯组分，任选地与至多20摩尔％的混合物，基于总计组分b）的摩尔数高于双官能多异氰酸酯。本发明还涉及通过该方法获得的聚氨酯，以及它们用于任选与其它增稠剂组合的用于增稠水性体系的用途。

6. 发明授权

US5286761A Process for the production of low-fog flexible polyester polyurethane foams and their use in vehicles 失效
标题翻译：生产低雾柔性聚酯聚氨酯泡沫的方法及其在车辆中的应用
公开(公告)号：US5286761A
公开(公告)日：1994-02-15
申请号：US86489
申请日：1993-07-01
申请人： Manfred Naujoks , Klaus Konig , Manfred Schmidt , Hans-Walter Illger , Gunter Baatz , Hansjurgen Rabe
发明人： Manfred Naujoks , Klaus Konig , Manfred Schmidt , Hans-Walter Illger , Gunter Baatz , Hansjurgen Rabe
IPC分类号： C08G18/42 , C08G18/65 , C08G18/66 , C08G63/88 , C08G63/90 , C08G101/00 , C08G18/14
CPC分类号： C08G63/90 , C08G18/4241 , C08G18/425 , C08G2101/0008 , C08G2101/0033 , C08G2101/0083 , C08G2290/00
摘要： Low-fog flexible polyester polyurethane foams are produced by reactinga) polyisocyanates, withb) polyesters containing at least two hydroxyl groups and having a molecular weight in the range from 400 to 10,000, in the presence ofc) water and/or readily volatile organic compounds as blowing agentswherein prior to reacting, the polyesters have been subjected to continuous distillation over an average holding time of 2 to 600 s, at a temperature of 160.degree. to 250.degree. C., and under a pressure of 0.05 to 10 mbar.The reaction mixture may optionally contain d) compounds containing at least two active hydrogen atoms and having a molecular weight in the range from 32 to 400 as chain-extending and crosslinking agents, and/ore) auxiliaries and additives known per se.These low-fogging polyester polyurethane foams are extremely suitable for use in vehicles, preferably automobiles.
摘要翻译： a）多异氰酸酯，其具有b）分子量为400至10,000的聚酯，其含有至少两个羟基，并且在制备之后以2至600秒的平均停留时间进行连续蒸馏，以及在c）水和/或易挥发的有机化合物的存在下，温度为160-250℃，优选180-230℃，压力为0.05-10mbar，优选0.1-3mbar，如发泡剂和任选地存在d）分子量为32-400的化合物，其含有最少两个活性氢原子作为扩链剂和交联剂，以及任选地在e）本身已知的助剂和添加剂的存在下，以及用于运输工具（运输），最好是汽车（汽车）。

7. 发明授权

US5220032A Herbicidal substituted 4,5-diamino-1,2,4-triazol-3-(thi)ones 失效
标题翻译：除草剂取代的4,5-二氨基-1,2,4-三唑-3-（thi）
公开(公告)号：US5220032A
公开(公告)日：1993-06-15
申请号：US764437
申请日：1991-09-23
申请人： Klaus-Helmut Muller , Kurt Findelsen , Michael Haug , Ulrich Heinemann , Joachim Kluth , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
发明人： Klaus-Helmut Muller , Kurt Findelsen , Michael Haug , Ulrich Heinemann , Joachim Kluth , Klaus Konig , Hans-Joachim Santel , Klaus Lurssen , Robert R. Schmidt
IPC分类号： A01N47/38 , C07C281/06 , C07D249/12 , C07D249/14 , C07D405/12
CPC分类号： C07D405/12 , A01N47/38 , C07C281/06 , C07D249/14 , C07C2101/02
摘要： Herbecidal substituted 4,5-diamino-1,2,4-triazol-3-(thi)ones of the formula ##STR1## in which R.sup.1, R.sup.2, R.sup.3, R.sup.4 and R.sup.5 each independently is hydrogen or and organic radical,X is O or S, andY is O or S.There are also provided novel intermediates of the formula ##STR2##
摘要翻译：其中R 1，R 2，R 3，R 4和R 5各自独立地是氢或者有机基团，其中R 1，R 2，R 3，R 4和R 5各自独立地是氢，取代的4,5-二氨基-1,2,4-三唑-3-（thi）另外，还提供了新颖的式（IIa）（IVa）（XXI）（XXIII））的新型中间体。

8. 发明授权

US5089627A Herbicidal substituted 4-sulphonylamino-2-azinyl-2,4-triazol-3-ones 失效
标题翻译：除草剂取代的4-磺酰基氨基-2-亚氨基-2,4-三唑-3-酮
公开(公告)号：US5089627A
公开(公告)日：1992-02-18
申请号：US583883
申请日：1990-09-17
申请人： Klaus-Helmut Muller , Rolf Kirsten , Joachim Kluth , Klaus Konig , Hans-Jochem Riebel , Peter Babczinski , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang
发明人： Klaus-Helmut Muller , Rolf Kirsten , Joachim Kluth , Klaus Konig , Hans-Jochem Riebel , Peter Babczinski , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang
IPC分类号： A01N43/64 , A01N43/653 , A01N43/66 , A01N43/707 , A01N43/713 , C07D401/14 , C07D403/00 , C07D403/04 , C07D403/14 , C07D405/14 , C07D409/14 , C07D417/14
CPC分类号： C07D401/14 , A01N43/653 , A01N43/66 , C07D403/04 , C07D403/14 , C07D409/14 , C07D417/14
摘要： Herbicidal substituted sulphonylaminotriazolinones of the formula ##STR1## in which R.sup.1 represents an optionally substituted radical from the group consisting of alkyl, aralkyl, aryl and heteroaryl,R.sup.2 represents hydrogen or the group --SO.sub.2 --R.sup.1 where R.sup.1 has the abovementioned meaning,R.sup.3 represents hydrogen, halogen, hydroxyl, mercapto, amino or an optionally substituted radical from the group consisting of alkyl, cycloalkyl, aralkyl, aryl alkoxy, alkenyloxy, alkinyloxy, alkylthio, alkylsulphinyl, alkylsulphonyl, alkenylthio, alkinylthio, aralkoxy, aralkylthio, alkylamino and dialkylamino,R.sup.4 represents hydrogen, halogen, hydroxyl, amino or an optionally substituted radical from the group consisting of alkyl, alkoxy, alkylthio, alkylsulphinyl, alkylsulphonyl, alkylamino and dialkylamino,X represents nitrogen or a CH group,Y represents nitrogen or a CR.sup.5 group whereR.sup.5 represents hydrogen, halogen, cyano, alkyl, formyl, alkylcarbonyl or alkoxycarbonyl, andZ represents nitrogen or a CR.sup.6 group whereR.sup.6 represents hydrogen, halogen, hydroxyl, amino or an optionally substituted radical from the group consisting of alkyl, alkoxy, alkylthio, alkylsulphinyl, alkylsulphonyl, alkylamino and dialkylamino,and salts thereof. Intermediates of the formulas ##STR2## are also new.

9. 发明授权

US4988381A Herbicidal substituted 4-sulphonylamino-2-azinyl-1,2,4-triazol-3-ones 失效
标题翻译：除草取代的4-磺酰基氨基-2-氮杂基-1,2,4-三唑-3-酮
公开(公告)号：US4988381A
公开(公告)日：1991-01-29
申请号：US382163
申请日：1989-07-19
申请人： Klaus-Helmut Muller , Rolf Kirsten , Joachim Kluth , Klaus Konig , Hans-Jochem Riebel , Peter Babczinski , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang
发明人： Klaus-Helmut Muller , Rolf Kirsten , Joachim Kluth , Klaus Konig , Hans-Jochem Riebel , Peter Babczinski , Hans-Joachim Santel , Robert R. Schmidt , Harry Strang
IPC分类号： A01N43/64 , A01N43/653 , A01N43/66 , A01N43/707 , A01N43/713 , C07D401/14 , C07D403/00 , C07D403/04 , C07D403/14 , C07D405/14 , C07D409/14 , C07D417/14
CPC分类号： C07D401/14 , A01N43/653 , A01N43/66 , C07D403/04 , C07D403/14 , C07D409/14 , C07D417/14
摘要： Herbicidal substituted sulphonylaminotriazolinones of the formula ##STR1## in which R.sup.1 represents an optionally substituted radical from the group consisting of alkyl, aralkyl, aryl and heteroaryl,R.sup.2 represents hydrogen or the group --SO.sub.2 --R.sup.1 where R.sup.1 has the abovementioned meaning,R.sup.3 represents hydrogen, halogen, hydroxyl, mercapto, amino or an optionally substituted radical from the group consisting of alkyl, cycloalkyl, aralkyl, aryl, alkoxy, alkenyloxy, alkinyloxy, alkylthio, alkylsulphinyl, alkylsulphonyl, alkenylthio, alkinylthio, aralkoxy, aralkylthio, alkylamino and dialkylamino,R.sup.4 represents hydrogen, halogen, hydroxyl, amino or an optionally substituted radical from the group consisting of alkyl, alkoxy, alkylthio, alkylsulphinyl, alkylsulphonyl, alkylamino and dialkylamino,X represents nitrogen or a CH group,Y represents nitrogen or a CR.sup.5 group whereR.sup.5 represents hydrogen, halogen, cyano, alkyl, formyl, alkylcarbonyl or alkoxycarbonyl, andZ represents nitrogen or a CR.sup.6 group whereR.sup.6 represents hydrogen, halogen, hydroxyl, amino or an optionally substituted radical from the group consisting of alkyl, alkoxy, alkylthio, alkylsulphinyl, alkylsulphonyl, alkylamino and dialkylamino,and salts thereof. Intermediates of the formulas ##STR2## are also new.
摘要翻译：式（I）的除草取代的磺酰基氨基三唑啉酮，其中R 1表示由烷基，芳烷基，芳基和杂芳基组成的组中的任选取代的基团，R 2表示氢或基团-SO 2 -R 1，其中R 1具有上述含义， R 3表示氢，卤素，羟基，巯基，氨基或任选取代的基团，其由烷基，环烷基，芳烷基，芳基，烷氧基，烯氧基，烷氧基，烷硫基，烷基亚磺酰基，烷基磺酰基，链烯硫基，炔基硫基，芳烷氧基，芳烷硫基，和二烷基氨基，R 4表示氢，卤素，羟基，氨基或任选取代的基团，其由烷基，烷氧基，烷硫基，烷基亚磺酰基，烷基磺酰基，烷基氨基和二烷基氨基，X表示氮或CH基，Y表示氮或CR 5 基团，其中R 5表示氢，卤素，氰基，烷基，甲酰基，烷基羰基或烷氧基羰基，Z表示氮或C R 6基团，其中R 6表示氢，卤素，羟基，氨基或任选取代的由烷基，烷氧基，烷硫基，烷基亚磺酰基，烷基磺酰基，烷基氨基和二烷基氨基组成的组的基团及其盐。式（II）和（IMA）（IV）的中间体也是新的。

10. 发明授权

US4843107A Process for the preparation of polyamines and their use for the preparation of polyurethanes 失效
标题翻译：制备多胺的方法及其用于制备聚氨酯的用途
公开(公告)号：US4843107A
公开(公告)日：1989-06-27
申请号：US173204
申请日：1988-03-24
申请人： Andreas Ruckes , Werner Rasshofer , Klaus Konig , Richard Kopp
发明人： Andreas Ruckes , Werner Rasshofer , Klaus Konig , Richard Kopp
IPC分类号： C08G18/64 , C08G18/10 , C08G18/50 , C08G73/02
CPC分类号： C08G18/5048 , C08G18/10
摘要： Polyamines containing primary amino groups are made by a one-shot process for the hydrolysis of prepolymers containing isocyanate end groups and having an isocyanate content of from 0.5 to 40 weight % with 0.75 to 40 mol of water per equivalent of isocyanate groups in the presence of very small quantities of sodium hydroxide in certain organic, polar solvents. The compounds containing isocyanate groups used for this process are isocyanate prepolymers (preferably containing urethane groups). Hydrolysis according to this process leads directly to the polyamines with elimination of carbon dioxide. These polyamines may be isolated by the usual methods and the removal of the small quantities of catalyst may advantageously be omitted. These polyamines are useful for the preparation of polyurethane(urea)s.
摘要翻译：含有伯氨基的多胺通过一步法制备，用于水解包含异氰酸酯端基并且异氰酸酯含量为0.5至40重量％的预聚物，每当异氰酸酯基为0.75至40摩尔水时，某些有机极性溶剂中极少量的氢氧化钠。用于该方法的含有异氰酸酯基团的化合物是异氰酸酯预聚物（优选含有氨基甲酸酯基团）。根据该方法的水解直接导致多胺消除二氧化碳。这些多胺可以通过常规方法分离，并且可以有利地省略少量催化剂的去除。这些多胺可用于制备聚氨酯（尿素）。

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