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1. 发明授权

US4985506A Oxidatively cross-linkable, water dilutable binders, a process for their preparation and their use 失效
标题翻译：可氧化交联的水可稀释粘合剂，其制备方法及其用途
公开(公告)号：US4985506A
公开(公告)日：1991-01-15
申请号：US371262
申请日：1989-06-26
申请人： Harald Blum , Peter Hohlein , Michael Sonntag , Wolfgang Wellner
发明人： Harald Blum , Peter Hohlein , Michael Sonntag , Wolfgang Wellner
IPC分类号： C08F8/14 , C08F8/44 , C08F20/02 , C08F22/06 , C08F222/00 , C08G81/02 , C09D133/00 , C09D133/04 , C09D135/00 , C09J133/00 , C09J133/04 , C09J135/00 , C09K3/10
CPC分类号： C08F8/14 , C08F8/44 , C08F2810/20 , C08F2810/30
摘要： Oxidatively cross-linkable, water dilutable binders suitable for lacquers, coating compositions and sealing compounds are modified co-polymers of olefinically unsaturated compounds, having a molecular weight of 6000 to 160,000 and having for each 100 grams of solids content, a total of from60 to 250 milliequivalents of chemically incorporated carboxyl groups, of which from 10 to 100% are neutralized thereby rendering the product dilutable in water andfrom 15 to 50% by weight of chemically incorporated moieties corresponding to the formula--O--RwhereinR represents an olefinically monounsaturated or polyunsaturated aliphatic hydrocarbon having a molecular weight above 166 and containing from 12 to 22 carbon atoms, are prepared by:(a) preparing a co-polymer having a molecular weight from 5000 to 80,000, determined by gel permeation chromatography, and having intramolecular carboxylic acid anhydride units corresponding to the formula ##STR1## and an anhydride equivalent weight of from 240 to 1960 by a radically initiated co-polymerization of olefinically unsaturated dicarboxylic acid anhydrides with other olefinically unsaturated monomers,(b) reacting at least 50% of the acid anhydride units present in the co-polymer from (a) with an unsaturated monohydric alcohol corresponding to the formulaR--OH with anhydride ring opening ester formation, and(c) converting the free carboxyl groups in the reaction product of (b) to an extent of 10 to 100% into carboxylate groups by neutralization of the carboxys with a base.
摘要翻译：适用于漆，水溶性组合物和密封化合物的可氧化交联的水可稀释粘合剂是烯属不饱和化合物的改性共聚物，其分子量为6000至160,000，并且对于每100克固体含量，总共为60 至250毫当量的化学引入的羧基，其中10至100％被中和，使产物在水中可稀释，和15至50重量％的化学引入部分对应于式-OR，其中R表示烯属单不饱和或分子量大于166且含有12至22个碳原子的多不饱和脂族烃通过以下方法制备：（a）通过凝胶渗透色谱法测定分子量为5000至80,000，并具有分子内羧酸的共聚物对应于式“IMAGE”的酸酐单元和2当量的酸酐当量通过烯属不饱和二羧酸酐与其它烯属不饱和单体的自由引发共聚，（b）使来自（a）的共聚物中存在的至少50％的酸酐单元与不饱和一元醇对应于具有酸酐开环酯形成的式R-OH，和（c）通过用碱中和羧基将羧酸酯基团将（b）的反应产物中的游离羧基转化成羧酸酯基团。

2. 发明授权

US4291135A Binders for coating compositions 失效
标题翻译：涂料组合物粘合剂
公开(公告)号：US4291135A
公开(公告)日：1981-09-22
申请号：US152567
申请日：1980-05-22
申请人： Peter Hohlein , Michael Sonntag
发明人： Peter Hohlein , Michael Sonntag
IPC分类号： C08L33/00 , C08G59/00 , C08G59/32 , C08G63/181 , C08G63/46 , C08G81/00 , C08G81/02 , C08L33/02 , C08L33/04 , C08L63/00 , C08L67/00 , C08L83/00 , C08L83/04 , C09D133/14 , C09D167/00 , C09D187/00 , C09D201/02 , B05D3/02 , B32B15/08 , B32B27/00
CPC分类号： C09D133/14 , C08G63/181 , C08G63/46 , C09D167/00 , C08L67/00 , C08L83/04 , Y10T428/31681 , Y10T428/31699
摘要： Reaction products of alkyd resins and/or oil-free polyesters, (meth) acrylic acid copolymers and polysiloxans are excellent binders for high quality lacquers particularly for surface lacquers used in the motor car industry.
摘要翻译：醇酸树脂和/或无油聚酯，（甲基）丙烯酸共聚物和聚硅氧烷的反应产物是用于高品质漆的优异粘合剂，特别是用于汽车工业中的表面漆。

3. 发明授权

US4639499A Cross-linkable polymer resins and use thereof as binders for coating agents 失效
标题翻译：可交联聚合物树脂及其作为涂布剂的粘合剂的用途
公开(公告)号：US4639499A
公开(公告)日：1987-01-27
申请号：US756483
申请日：1985-07-18
申请人： Peter Hohlein , Manfred Schmidt , Josef Pedain , Bernd Riberi , Michael Sonntag
发明人： Peter Hohlein , Manfred Schmidt , Josef Pedain , Bernd Riberi , Michael Sonntag
IPC分类号： C09D201/06 , C08F216/00 , C08F246/00 , C09D133/04 , C09D157/04 , C09D175/00 , C08F238/00 , C08F220/04
CPC分类号： C08F246/00 , C08F216/00 , C09D157/04
摘要： The present invention is directed to cross-linkable, hydroxyl group-containing polymer resins which are obtained by copolymerizing olefinically-unsaturated monomers and are suitable as binder components for lacquers, the polymer resins having a hydroxyl number of about 20 to 400, an average osmometrically-determined molecular weight of about 500 to 30,000 and a molecular inhomogeneity U of about 0.5 to 15, characterized in that they contain about 0.2 to 80% by weight, preferably about 10 to 70% by weight, based on the total weight of the copolymers, of incorporated monomers selected from olefinically- and acetylenically-unsaturated aliphatic diols having 4 carbon atoms, the ether group-containing alkoxylation products thereof with a hydroxyl number of about 50 to 900, the reaction products of these diols with .epsilon.-caprolactone in a mol ratio of diol:-caprolactone of about 1:0.2 to 1:10 and any mixtures of these components.The present invention is also directed to the use of the above polymer resins as binders for coating compositions.
摘要翻译：本发明涉及可交联的含羟基的聚合物树脂，其通过使烯属不饱和单体共聚合而获得，并且适合作为漆的粘合剂组分，聚合物树脂的羟值为约20至400，平均渗透压约500至30,000的测定分子量和约0.5至15的分子不均匀性U，其特征在于它们含有约0.2至80重量％，优选约10至70重量％，基于共聚物的总重量包含选自具有4个碳原子的烯属和炔属不饱和脂族二醇的单体，其含醚基的烷氧基化产物的羟值为约50至900，这些二醇与ε-己内酯的摩尔比为摩尔二醇：己内酯的比例为约1:0.2至1:10，以及这些组分的任何混合物。本发明还涉及上述聚合物树脂作为涂料组合物的粘合剂的用途。

4. 发明授权

US5331039A Water-based binder composition and its use for the production of coating or sealing compositions 失效
标题翻译：水性粘合剂组合物及其用于生产涂料或密封组合物的用途
公开(公告)号：US5331039A
公开(公告)日：1994-07-19
申请号：US973368
申请日：1992-11-09
申请人： Harald Blum , Werner Kubitza , Joachim Probst , Michael Sonntag , Volker Schneider
发明人： Harald Blum , Werner Kubitza , Joachim Probst , Michael Sonntag , Volker Schneider
IPC分类号： C08G18/00 , C08G18/08 , C08G18/10 , C08G18/40 , C08G18/42 , C08G18/46 , C08G18/70 , C08L75/04 , C09D175/04 , C09D175/06 , C09J175/00 , C09J175/06 , H01L23/29 , H01L23/31 , C08L67/00
CPC分类号： C09D175/06 , C08G18/0819 , C08G18/10 , C08G18/4063 , C08G18/4202 , C08G18/706 , C08G2170/80
摘要： The present invention relates to a water-based binder composition containingA) an aqueous solution or dispersion of a water-dilutable organic polyol component containing a mixture of at least 5% by weight each of at least two hydroxy-functional polymers selected fromA1) polyester resins containing hydroxyl, urethane and carboxylate groups,A2) polyester resins containing hydroxyl and carboxylate groups, but no urethane or sulfonate groups,A3) polyester resins containing hydroxyl and sulfonate groups and, optionally, carboxylate groups and/or urethane groups,A4) polyacrylate resins containing hydroxyl, carboxylate and/or sulfonate groups,A5) acrylate-grafted polyester resins containing hydroxyl, carboxylate and/or sulfonate groups, andB) a polyisocyanate component which is emulsified in the aqueous solution or dispersion A), has a viscosity at 23.degree. C. of 50 to 10,000 mPa.s and contains at least one organic polyisocyanate,wherein the NCO:OH equivalent ratio, based on the isocyanate groups of component B) and the hydroxyl groups of the polyol component present in A), is 0.2:1 to 5:1.The present invention also relates to a process for the production of a coating or sealing composition containing this aqueous binder composition.
摘要翻译：本发明涉及水性粘合剂组合物，其包含A）水可稀释有机多元醇组分的水溶液或分散体，其含有至少5重量％的至少两种羟基官能聚合物的混合物，所述羟基官能聚合物选自A1）含有羟基，氨基甲酸酯和羧酸酯基团的聚酯树脂，A2）含有羟基和羧酸酯基团但不含氨基甲酸酯基或磺酸酯基团的聚酯树脂，A3）含有羟基和磺酸酯基团以及任选的羧酸酯基团和/或氨基甲酸酯基团的聚酯树脂，A4）含有羟基，羧酸酯和/或磺酸酯基的聚丙烯酸酯树脂，A5）含有羟基，羧酸酯和/或磺酸酯基团的丙烯酸酯接枝的聚酯树脂，和B）在水溶液或分散体A）中乳化的多异氰酸酯组分具有粘度在23℃下为50至10,000mPa.s并含有至少一种有机多异氰酸酯，其中NCO:OH当量比基于异氰酸酯组分B）的组分和A）中存在的多元醇组分的羟基为0.2:1至5:1。本发明还涉及一种生产包含该含水粘合剂组合物的涂料或密封组合物的方法。

5. 发明授权

US4945137A Binder combinations and a process for the production of flat materials 失效
标题翻译：粘合剂组合和生产平板材料的工艺
公开(公告)号：US4945137A
公开(公告)日：1990-07-31
申请号：US415863
申请日：1989-10-02
申请人： Walter Schafer , Hans Rudolph , Rolf Dhein , Hanns-Peter Muller , Michael Sonntag , Christian Wamprecht , Harald Blum , Walter Krauss
发明人： Walter Schafer , Hans Rudolph , Rolf Dhein , Hanns-Peter Muller , Michael Sonntag , Christian Wamprecht , Harald Blum , Walter Krauss
IPC分类号： C08L33/06 , C03C25/10 , C08F8/32 , C08K3/28 , C08K5/17 , C08K5/353 , C08K13/02 , C08L33/04 , C08L35/00 , C08L101/00 , C08L101/08 , C09D7/12 , C09D201/08
CPC分类号： C08K5/17 , C08F8/32 , C08K3/28 , C08K5/353
摘要： A binder for a coating composition is a combination of(a) polymers containing intramolecular carboxylic anhydride groups and having an average molecular weight of from 500 to 25,000 and(b) organic compounds containing 4,5-dihydrooxazole groups in a quantity corresponding to an equivalent ratio of carboxylic anhydride groups to 4,5-dihydrooxazole groups of from 0.5:1 to 2:1, and contains from 0.005 to 5% by weight, based on the weight of components (a) and (b), of ammonia, a primary amine or secondary amine.
摘要翻译：用于涂料组合物的粘合剂是（a）含有分子内羧酸酐基团并且平均分子量为500至25,000的聚合物和（b）含有相当于当量的4,5-二氢恶唑基团的有机化合物的组合羧酸酐基团与4,5-二氢恶唑基团的比例为0.5:1至2:1，并且基于组分（a）和（b）的重量，含有0.005至5重量％的氨，伯胺或仲胺。

6. 发明授权

US5412056A Surface coatings and a process for their production 失效
标题翻译：表面涂层及其生产工艺
公开(公告)号：US5412056A
公开(公告)日：1995-05-02
申请号：US286612
申请日：1994-08-05
申请人： Christian Zwiener , Michael Sonntag , Dieter Margotte , Pedain , Harald Blum , Volker Schneider
发明人： Christian Zwiener , Michael Sonntag , Dieter Margotte , Pedain , Harald Blum , Volker Schneider
IPC分类号： C07D263/04 , C07D269/02 , C08G18/28 , C08G18/30 , C08G18/32 , C08G18/38 , C08G18/65 , C09D175/00 , C09D175/04 , C09D175/12 , C08G18/34
CPC分类号： C08G18/6535 , C08G18/3253 , C08G18/3262 , C08G18/3296 , C08G18/3821 , C09D175/12
摘要： A coating composition in which the binding agent is a two-component system containing a) a polyisocyanate component and b) an isocyanate-reactive component and contains b1) specific ester group-containing secondary polyamines, b2) specific moisture-activatable blocked polyamines and b3) optionally other known compounds containing isocyanate-reactive groups, and a process for preparing coated substrates from this coating composition.
摘要翻译：一种涂料组合物，其中所述粘合剂是包含a）多异氰酸酯组分和b）异氰酸酯反应性组分的双组分体系，并且包含b1）具体的含酯基的仲多胺，b2）特定的可湿气活化的封端多胺和b3 ）任选地其它含有异氰酸酯反应性基团的已知化合物，以及由该涂料组合物制备涂覆的基材的方法。

7. 发明授权

US5089565A Process for the preparation of curable binder combinations, the combinations obtainable by this process and the use thereof 失效
标题翻译：制备可固化粘合剂组合的方法，本方法可获得的组合及其用途
公开(公告)号：US5089565A
公开(公告)日：1992-02-18
申请号：US358448
申请日：1989-05-30
申请人： Harald Blum , Christian Wamprecht , Josef Pedain , Michael Sonntag
发明人： Harald Blum , Christian Wamprecht , Josef Pedain , Michael Sonntag
IPC分类号： C08L35/00 , C08F20/02 , C08F22/06 , C08K5/35 , C09D133/02 , C09D135/00
CPC分类号： C09D135/00 , C08K5/35
摘要： A moisture-curing binder composition useful in paints and other coating compositions is prepared by mixing or mixing with spontaneous reaction in the absence of moistureA) 30 to 99 parts by weight of at least one compound containing at least two intramolecular carboxylic anhydride groups andB) 1 to 70 parts by weight of organic compounds having blocked amino groups, wherein B)comprises organic compounds containing hydrogen atoms which are reactive to acid anhydride groups and containing bicyclic amide acetal or bicyclic amide groups or both, wherein the ratios of the amounts of the individual components are chosen such that, by taking into account the addition reaction which occurs spontaneously between components A) and B) in the absence of moisture, in the resulting mixture 0.25 to 50 anhydride groups are present per bicyclic amide acetal and bicyclic amide aminal group.
摘要翻译：用于油漆和其他涂料组合物的湿固化粘合剂组合物通过在不存在水分的情况下与自发反应混合或混合制备A）30至99重量份的至少一种含有至少两个分子内羧酸酐基团的化合物和B ）1至70重量份具有封闭氨基的有机化合物，其中B）包含含有与酸酐基团反应并含有双环酰胺缩醛或双环酰胺基团或两者的氢原子的有机化合物，其中，选择各个组分使得通过考虑到在不存在水分的情况下在组分A）和B）之间自发发生的加成反应，在所得混合物中，每双酰胺缩醛和双环酰胺缩醛存在0.25至50个酸酐基团组。

8. 发明授权

US4975493A Process for the production of moisture-hardening binder compositions and their use 失效
标题翻译：湿固化粘合剂组合物的生产方法及其用途
公开(公告)号：US4975493A
公开(公告)日：1990-12-04
申请号：US223803
申请日：1988-07-25
申请人： Harald Blum , Josef Pedain , Christian Wamprecht , Michael Sonntag
发明人： Harald Blum , Josef Pedain , Christian Wamprecht , Michael Sonntag
IPC分类号： C08L23/00 , C08F8/32 , C08K5/35 , C09D133/04 , C09D135/00
CPC分类号： C08K5/35 , C08F8/32 , C09D135/00 , C08F2800/20
摘要： A moisture-hardening binder composition for lacquer of coating compositions is prepared by mixing(A) 50 to 97 parts by weight of copolymers of maleic anhydride with olefinically unsaturated monomers, said copolymers containing succinic anhydride units and having molecular weights Mw of 1,500 to 75,000 with(B) 3 to 50 parts by weight oxazolanes having a molecular weight Mw of 87 to 10,000,the quantitative ratios of (A) to (B) being such that the composition contains 0.25 to 10 anhydride groups for every oxazolane group,wherein component (A) consists essentially of copolymers of(a) 4.5 to 45 parts by weight of maleic anhydride,(b) 5 to 80 parts by weight of monomers of the formulae ##STR1## or both, and (c) 15 to 92 parts by weight of monomers of the formula ##STR2## wherein, R.sub.1 and R.sub.4 is each, independent of the other, an aliphatic or cycloaliphatic C.sub.1 -C.sub.12 hydrocarbon radical with or without oxygen, sulfur or nitrogen as a heteratom, R.sub.2 is hydrogen, methyl, ethyl, chlorine or fluorine,R.sub.3 is a C.sub.2 -C.sub.15 aliphatic hydrocarbon radical, a C.sub.5 -C.sub.10 cycloaliphatic hydrocarbon radical, a C.sub.7 -C.sub.18 araliphatic hydrocarbon radical, a C.sub.6 -C.sub.12 aromatic hydrocarbon radical, chlorine, fluorine, nitrile or a C.sub.2 -C.sub.18 hydrocarbon radical containing one or more heteroatoms selected from the group consisting of oxygen, sulfur and nitrogen in the form of ether, ester, amide, urethane, urea, thioester, oxirane, ketone, lactam or lactone groups.
摘要翻译：通过混合（A）50至97重量份的马来酸酐与烯属不饱和单体的共聚物，所述共聚物含有琥珀酸酐单元并具有1500至75,000的分子量Mw，制备用于涂料组合物漆的湿润硬化粘合剂组合物，（B）3〜50重量份的分子量Mw为87〜10,000的恶唑烷，（A）〜（B）的定量比为每个恶唑烷基组成含有0.25〜10个酸酐基，其中组分（ A）基本上由（a）4.5至45重量份马来酸酐的共聚物组成，（b）5-80重量份式（IMAGE）或两者的单体，和（c）15至92重量份具有下式的单体：其中，R 1和R 4各自独立地为具有或不具有氧，硫或氮作为杂原子的脂族或脂环族C 1 -C 12烃基，R 2为氢，甲基，乙基，氯或氟 ne，R 3是C 2 -C 15脂族烃基，C 5 -C 10脂环族烃基，C 7 -C 18芳脂族烃基，C 6 -C 12芳烃基，氯，氟，腈或含有一个的C 2 -C 18烃基或更多选自醚，酯，酰胺，氨基甲酸酯，脲，硫酯，环氧乙烷，酮，内酰胺或内酯基团的氧，硫和氮的杂原子。

9. 发明授权

US06423816B1 Polyester polyols and their use as a binder component in two-component polyurethane coating compositions 失效
标题翻译：聚酯多元醇及其在双组分聚氨酯涂料组合物中作为粘合剂组分的用途
公开(公告)号：US06423816B1
公开(公告)日：2002-07-23
申请号：US08583167
申请日：1996-01-04
申请人： Christian Wamprecht , Michael Sonntag
发明人： Christian Wamprecht , Michael Sonntag
IPC分类号： C08G6312
CPC分类号： C09D175/14 , C08G18/68 , C08G63/52 , C09D167/06 , C08L2666/36
摘要： The present invention relates to polyester polyols having a hydroxyl number of 60 to 400, which are esterification products of a) an alcohol component containing one or more aliphatic or cycloaliphatic alcohols having at least 3 hydroxyl groups and 3 to 8 carbon atoms with b) a carboxylic acid component containing itaconic acid, maleic acid, their anhydrides and/or fumaric acid, provided that at least 10 mole % of either component a) or component b) is an aliphatic or cycloaliphatic, saturated or unsaturated monoalcohol or monocarboxylic acid having 1 to 18 carbon atoms. The present invention also relates to two-component polyurethane coating compositions containing these polyester polyols and lacquer polyisocyanates as the binder and to their use for coating substrates, in particular automotive substrates.
摘要翻译：本发明涉及羟基数为60〜400的聚酯多元醇，它们是a）含有一个或多个具有至少3个羟基和3至8个碳原子的脂族或脂环族醇的醇组分与b）羧酸的酯化产物含有衣康酸的组分，马来酸，它们的酸酐和/或富马酸，条件是至少10摩尔％的组分a）或组分b）是具有1至18个碳原子的脂族或脂环族饱和或不饱和的一元醇或一元羧酸原子本发明还涉及含有这些聚酯多元醇和漆多异氰酸酯作为粘合剂的双组分聚氨酯涂料组合物，以及它们用于涂覆基材，特别是汽车基材的用途。

10. 发明授权

US4727128A Diisocyanates containing urethane groups, a process for their preparation and their use as binders or binder component in polyurethane lacquers 失效
标题翻译：含有氨基甲酸酯基团的二异氰酸酯，其制备方法以及它们在聚氨酯漆中作为粘合剂或粘合剂组分的用途
公开(公告)号：US4727128A
公开(公告)日：1988-02-23
申请号：US820057
申请日：1986-01-21
申请人： Josef Pedain , Bernd Riberi , Michael Sonntag , Klaus Konig , Jurg Frohlich
发明人： Josef Pedain , Bernd Riberi , Michael Sonntag , Klaus Konig , Jurg Frohlich
IPC分类号： C08G18/00 , C07C67/00 , C07C239/00 , C07C269/02 , C07C271/06 , C07C271/20 , C08G18/10 , C08G18/32 , C08G18/73 , C08G18/80 , C09D175/00 , C09D175/04 , C07C125/07 , C08G18/78
CPC分类号： C08G18/8009
摘要： The present invention is directed to a process for the preparation of a diisocyanate by reacting a diisocyanate with 2,2,4-trimethyl-pentanediol-(1,3) or reaction products of this diol which contain either ether or ester groups and optionally other diols or triols. The present invention is additionally directed to the diisocyanates produced by this process and to their use in one-component and two-component coating compositions.
摘要翻译：本发明涉及通过使二异氰酸酯与2,2,4-三甲基戊二醇 - （1,3）或该二醇的含有醚基或酯基的任意其它的二醇的反应产物进行反应来制备二异氰酸酯的方法二醇或三醇。本发明另外涉及通过该方法制备的二异氰酸酯及其在单组分和双组分涂料组合物中的用途。

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