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    • 4. 发明授权
    • Low temperature joining of phosphate glass
    • 低温接合磷酸盐玻璃
    • US07208060B2
    • 2007-04-24
    • US10614087
    • 2003-07-08
    • Samuel David ConzoneJoseph S. HaydenAlexander J. Marker, III
    • Samuel David ConzoneJoseph S. HaydenAlexander J. Marker, III
    • B32B37/12
    • C03C3/17C03C4/0071C03C27/06G02B6/12G02B6/12002G02B6/13G02B6/30
    • A method for the low temperature joining of similar and/or different phosphate glass by mating at low temperature glass components by an aqueous solution containing phosphorus. In preferred embodiments, the phosphate glasses are polished, cleaned, and brought together with the phosphate-containing solution between the polished surfaces. Vacuum may be applied to assist in making the joint. The composite is optionally heat treated to increase strength, chemical durability, and optical performance. The bond thereby formed has low birefringence, is strong, and is virtually photonically invisible. The joints now make possible, for example, substrates for virtually no loss signal splitters and other high-end optical components at low cost. Large hybrid performs substrates composed of multiple glass components may be prepared and segmented, providing an inexpensive novel substrate for the photonics industry. Active lasing phosphate glasses may be joined by the present invention method to passive non-lasing glasses for use in laser and related applications.
    • 一种通过含磷水溶液在低温玻璃组分配合来低温接合相似和/或不同磷酸盐玻璃的方法。 在优选的实施方案中,将磷酸盐玻璃与抛光表面之间的含磷酸盐溶液进行抛光,清洁并与之一起。 可以使用真空来辅助接头。 任选地对复合材料进行热处理以提高强度,化学耐久性和光学性能。 由此形成的结合具有低双折射性,是强的,并且实际上是光学不可见的。 接头现在使得成为可能,例如,用于几乎没有损耗信号分离器和其它高端光学部件的基板以低成本。 可以制备和分段的由多个玻璃组分组成的大型混合的基片,为光子学工业提供便宜的新型基片。 主动激光磷酸盐玻璃可以通过本发明的方法连接到用于激光和相关应用的被动非激光玻璃。
    • 5. 发明授权
    • Process for the fabrication of glass ceramic structures
    • 玻璃陶瓷结构的制造工艺
    • US06699341B2
    • 2004-03-02
    • US10190724
    • 2002-07-09
    • Samuel David ConzoneAlexander J. Marker, III
    • Samuel David ConzoneAlexander J. Marker, III
    • B32B3106
    • C03C27/06C03C27/044Y10T428/21Y10T428/24273Y10T428/24322
    • A method for fabricating composite light-weighted glass ceramics, suitable for use as, e.g. mirror blanks or microlithography stages, at low temperatures is disclosed. Component pieces are polished then joined at low temperature using a silicate-containing joining liquid. Assembly is then performed in such a way that the joining liquid forms an interface between each component. After a period of low or slightly elevated temperature curing, rigid joints are formed throughout and the composite is dimensionally, vibrationally, and temperature stable and can withstand tensile stresses >4000 psi. The room-temperature cured composite can be heat treated using a slow, systematic temperature increase to dehydrate the joints. A sealing coating may optionally be provided to prevent excess dried joining liquid from flaking off the formed joint.
    • 复合轻量玻璃陶瓷的制造方法,适合用作例如玻璃陶瓷。 公开了在低温下的镜面空白或微光刻阶段。 抛光组件,然后使用含硅酸盐的接合液体在低温下接合。 然后以这样的方式进行组装,使得接合液体形成每个部件之间的界面。 经过一段时间的低温或稍微升高的温度固化后,刚性接头整体形成,复合材料的尺寸,振动和温度稳定,可承受> 4000 psi的拉伸应力。 室温固化复合材料可以通过缓慢,系统的温度升高来对接头进行脱水处理。 可以可选地提供密封涂层以防止多余的干燥的接合液体从形成的接头剥落。