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    • 4. 发明授权
    • Vapor-phase fluidized-bed process and ethylene homopolymers and copolymers produced thereby
    • 气相流化床方法和由此制备的乙烯均聚物和共聚物
    • US06849699B2
    • 2005-02-01
    • US10658916
    • 2003-09-11
    • Peter BauerArmin LangeRainer KarerPhilipp RosendorferManfred HeckerGünther SchweierWolfgang MicklitzKaspar EvertzHans-Jacob Feindt
    • Peter BauerArmin LangeRainer KarerPhilipp RosendorferManfred HeckerGünther SchweierWolfgang MicklitzKaspar EvertzHans-Jacob Feindt
    • C08J5/18C08F2/34C08F4/02C08F4/24C08F4/69C08F10/02C08F210/02
    • C08F10/02C08F4/24C08F2/34
    • A continuous vapor-phase fluidized-bed process for the preparation of ethylene homopolymers and copolymers having a density of from 0.87 to 0.97 g/cm3 in which ethylene or mixtures of ethylene and C3-C8 a-monoolefins are (co)polymerized in the presence of a supported chromium catalyst in the polymerization zone of a vapor-phase fluidized-bed reactor under pressures ranging from 1 to 100 bar and at temperatures ranging from 30° to 125° C. in the vapor phase in an agitated bed of bulk material comprising particulate polymer, the resultant heat of polymerization is removed by cooling the recirculated reactor gas and the resulting (co)polymer is removed from the vapor-phase fluidized-bed reactor, wherein, for the preparation of a (co)polymer of a specific density d, the (co)polymerization is carried out at a temperature which is in a range restricted by an upper envelope defined by equation I T H = 171 + 6 ⁢   ⁢ d ′ 0.84 - d ′ ( I ) and a lower envelope defined by equation II T L = 173 + 7.3 ⁢   ⁢ d ′ 0.837 - d ′ , ( II ) in which the variables have the following meanings: TH is the highest reaction temperature in ° C.; TL is the lowest reaction temperature in ° C.; d′ is the numerical value of the density d of the (co)polymer to be synthesized.
    • 用于制备密度为0.87至0.97g / cm 3的乙烯均聚物和共聚物的连续气相流化床方法,其中乙烯或乙烯和C 3 -C 8α-单烯烃的混合物(共)聚合 在负载的铬催化剂的存在下,在气相流化床反应器的聚合区域的存在下,在压力范围为1至100巴,温度范围为30至125℃,气相在搅拌床 包含颗粒聚合物的散装材料,通过冷却再循环的反应器气体除去所得到的聚合热,并将所得(共)聚合物从气相流化床反应器中除去,其中,为制备(共)聚合物 特定密度d,(共)聚合在由等式I定义的上包络限制的范围内进行,并且由等式IIin定义的下包络,其中变量具有以下含义:T H是最高的反应温度,单位°C; TL是最低反应温度(℃); d'是待合成的(共)聚合物的密度d的数值。
    • 8. 发明授权
    • Gas phase fluidized bed method and ethylene homo- and copolymers obtained using said method
    • 气相流化床法和使用所述方法获得的乙烯均聚物和共聚物
    • US06649709B1
    • 2003-11-18
    • US09555594
    • 2000-05-31
    • Peter BauerArmin LangeRainer KarerPhilipp RosendorferManfred HeckerGünther SchweierWolfgang MicklitzKaspar EvertzHans-Jacob Feindt
    • Peter BauerArmin LangeRainer KarerPhilipp RosendorferManfred HeckerGünther SchweierWolfgang MicklitzKaspar EvertzHans-Jacob Feindt
    • C08F234
    • C08F10/02C08F4/24C08F2/34
    • A continuous vapor-phase fluidized-bed process for the preparation of ethylene homopolymers and copolymers having a density of from 0.87 to 0.97 g/cm3 in which ethylene or mixtures of ethylene and C3-C8 a-monoolefins are (co)polymerized in the presence of a supported chromium catalyst in the polymerization zone of a vapor-phase fluidized-bed reactor under pressures ranging from 1 to 100 bar and at temperatures ranging from 30° to 125° C. in the vapor phase in an agitated bed of bulk material comprising particulate polymer, the resultant heat of polymerization is removed by cooling the recirculated reactor gas and the resulting (co)polymer is removed from the vapor-phase fluidized-bed reactor, wherein, for the preparation of a (co)polymer of a specific density d, the (co)polymerization is carried out at a temperature which is in a range restricted by an upper envelope defined by equation I T H = 171 + 6 ⁢ d ′ 0.84 - d ′ ( I ) and a lower envelope defined by equation II T L = 173 + 7.3 ⁢ d ′ 0.837 - d ′ , ( II ) in which the variables have the following meanings: TH is the highest reaction temperature in ° C.; TL is the lowest reaction temperature in ° C.; d′ is the numerical value of the density d of the (co)polymer to be synthesized.
    • 用于制备密度为0.87至0.97g / cm 3的乙烯均聚物和共聚物的连续气相流化床方法,其中乙烯或乙烯和C 3 -C 8α-单烯烃的混合物(共)聚合 在负载的铬催化剂的存在下,在气相流化床反应器的聚合区域的存在下,在压力范围为1至100巴,温度范围为30至125℃,气相在搅拌床 包含颗粒聚合物的散装材料,通过冷却再循环的反应器气体除去所得到的聚合热,并将所得(共)聚合物从气相流化床反应器中除去,其中,为制备(共)聚合物 特定密度d,(共)聚合在由等式I定义的上包络限制的范围内进行,并且由等式IIin定义的下包络,其中变量具有以下含义:T H是最高的反应温度,单位°C; TL是最低反应温度(℃); d'是待合成的(共)聚合物的密度d的数值。