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31. 发明申请

US20080283458A1 Separation column and liquid chromatography apparatus using the same 失效
标题翻译：分离柱和使用其的液相色谱仪
公开(公告)号：US20080283458A1
公开(公告)日：2008-11-20
申请号：US12081572
申请日：2008-04-17
申请人： Kimihiko Ishii , Hironori Kaji , Masahito Ito , Yoshihiro Nagaoka , Kunihiko Takao
发明人： Kimihiko Ishii , Hironori Kaji , Masahito Ito , Yoshihiro Nagaoka , Kunihiko Takao
IPC分类号： B01D15/08 , B01D15/22
CPC分类号： B01D15/22 , B01D15/206 , B01J20/3236 , B01J2220/82 , B01J2220/86 , G01N30/52 , G01N30/6017 , G01N30/603 , G01N30/6047 , G01N30/6052 , G01N2030/528
摘要： Disclosed herein is a separation column comprising a porous block covered with a coating wherein space-free adhesion is attainable therebetween by low temperature process without releasing octadecylsilyl bases and others from the porous block.A monolith rod 1 is covered with a metal or resin coating 2. Then, the monolith rod 1 covered by the coating 2 is further covered with a rod retainer 3 made of a low melting point metal (melting point 100-200 degrees C.) to form a column body 19. Since the rod retainer 3 is formed by pressure molding at low temperature (100-200 degrees C.). It is therefore possible to absorb the surface irregularities of the monolith rod 1 by the coating 2 while octadecylsilyl bases and others from are released when the retainer 3 is formed. This allows the potential separation ability of the porous block to be brought out maximally.
摘要翻译：本文公开了一种分离柱，其包括用涂层覆盖的多孔块，其中通过低温工艺在其间实现无空隙粘合，而不从多孔块中释放十八烷基甲硅烷基等。整料棒1被金属或树脂涂层2覆盖。然后，用由低熔点金属（熔点为100-200℃）制成的棒保持器3进一步覆盖由涂层2覆盖的整料棒1，以形成柱体19。由于杆保持器3通过在低温（100-200℃）下进行压力成型而形成。因此，当保持器3形成时，可以通过涂层2吸收整料棒1的表面凹凸，同时十八烷基甲硅烷基等被释放。这允许最大限度地排出多孔块的潜在分离能力。

32. 发明申请

US20070084766A1 Pump for liquid chromatograph 审中-公开
标题翻译：泵用于液相色谱
公开(公告)号：US20070084766A1
公开(公告)日：2007-04-19
申请号：US11582455
申请日：2006-10-18
申请人： Kimihiko Ishii , Kiyotoshi Mori , Masahito Ito , Hironori Kaji , Takefumi Yokokura
发明人： Kimihiko Ishii , Kiyotoshi Mori , Masahito Ito , Hironori Kaji , Takefumi Yokokura
IPC分类号： B01D35/14
CPC分类号： G01N30/32 , G01N30/34 , G01N2030/322 , G01N2030/326
摘要： A pump device is realized, which accurately detects a flow rate of a pump, performs real-time control of the flow rate, and thus can suppress a flow rate error caused by occurrence of pulsation. Control of a pump rotation speed by a pressure sensor has low responsiveness in a low pressure region, and a correlation between a pressure and a flow rate is incomplete in a high flow rate region. With this taken into consideration, a flow rate sensor 10 is disposed at an outlet port 9 of a second pump 4. A position detection sensor 14 detects a point where a first pump 3 is shifted from a suction mode to a discharge mode. Moreover, the flow rate sensor 10 detects that there is no discharge from the pump 3, and that there is discharge from the pump 4 alone. Accordingly, a controller 15 sets a rotation speed of a motor 12 to a speed double the previous speed (double the normal rotation speed). When the flow rate sensor 10 detects an increase in the flow rate at the outlet port 9 of the second pump 4, the controller 15 returns the rotation speed of the motor 12 to a normal rotation speed. The rotation speed of the motor 12 is controlled by accurate flow rate detection by the flow rate sensor 10. Thus, occurrence of pulsation can be suppressed.
摘要翻译：实现了能够精确地检测泵的流量的泵装置，实现流量的实时控制，能够抑制由脉动发生引起的流量误差。通过压力传感器控制泵的转速在低压区域的响应性低，在高流量区域中压力与流量的相关性不完全。考虑到这一点，流量传感器10设置在第二泵4的出口9处。位置检测传感器14检测第一泵3从吸入模式移动到放电模式的点。此外，流量传感器10检测到没有来自泵3的排出，并且仅从泵4排出。因此，控制器15将电动机12的转速设定为与先前速度（正常转速两倍）的速度。当流量传感器10检测到第二泵4的出口9的流量增加时，控制器15将马达12的转速恢复到正常的转速。通过流量传感器10的精确的流量检测来控制电动机12的转速。因此，可以抑制脉动的发生。

33. 发明授权

US07063785B2 Pump for liquid chromatography 失效
标题翻译：泵用于液相色谱
公开(公告)号：US07063785B2
公开(公告)日：2006-06-20
申请号：US10902028
申请日：2004-07-30
申请人： Kenji Hiraku , Kunihiko Takao , Hironori Kaji , Masahito Ito
发明人： Kenji Hiraku , Kunihiko Takao , Hironori Kaji , Masahito Ito
IPC分类号： B01D15/08
CPC分类号： F04B11/0058 , B01D15/14 , F04B11/0083 , F04B13/02 , F04B53/06 , F04B2205/09 , G01N2030/326
摘要： The invention provides a pump for liquid chromatography excellent in feeding liquid stably at an extremely low flow rate with high accuracy and in discharging bubbles at startup.At startup, a first plunger feeds solvent at a large flow rate to discharge bubbles in a pump and to fill the solvent into the pump in a short time and in a normal operation, the first plunger is stopped and the second plunger is pushed into a second pressure chamber at a low speed to feed the solvent at a low flow rate. When the second plunger reaches full stroke, the second plunger is pulled back at a high speed and at the same time the first plunger is pushed into a first pressure chamber in synchronization with the pullback of the second plunger to control the flow rate passing a discharge passage to a constant value at all times by a controller. Further, while the second plunger feeds the solvent, the first plunger is slightly pushed into the first pressure chamber to keep pressure in the first pressure chamber at pressure equal to or less than pressure in the second pressure chamber.
摘要翻译：本发明提供了一种液体色谱泵，其具有以极高的精度稳定地以极低的流量供给液体并在起动时排出气泡的液体色谱。在启动时，第一柱塞以大流量供给溶剂以排出泵中的气泡并在短时间内和正常操作中将溶剂填充到泵中，使第一柱塞停止并将第二柱塞推入第二压力室以低速进料以低流量进料溶剂。当第二柱塞达到全行程时，第二柱塞被高速拉回，同时第一柱塞与第二柱塞的回退同步地被推入第一压力室，以控制通过排放的流量任何时候都由控制器传递给恒定值。此外，当第二柱塞进料溶剂时，第一柱塞稍微推入第一压力室，以将第一压力室中的压力保持在第二压力室中等于或小于压力的压力。

34. 发明申请

US20060000759A1 Liquid feeding system 有权
标题翻译：送液系统
公开(公告)号：US20060000759A1
公开(公告)日：2006-01-05
申请号：US11171216
申请日：2005-07-01
申请人： Kunihiko Takao , Hironori Kaji , Masahito Ito
发明人： Kunihiko Takao , Hironori Kaji , Masahito Ito
IPC分类号： B01D15/08
CPC分类号： G01N30/32 , B01D15/14 , B01D15/166 , F04B11/0058 , F04B11/0083 , F04B13/00 , F04B13/02 , F04B53/06 , G01N2030/326
摘要： This liquid feeding system has the first and second pumps each of which is provided with a plunger. Liquid sucked through each of the pump suction ports is discharged out of the discharging port through the first pump and/or second pump. Under the starting operation mode, the second pump is stopped and only the first pump is operated. When the discharging pressure at the discharging port reaches up to a predetermined value, the starting operation mode is changed over to the normal operation mode. Under the normal operation mode, the first pump is stopped and only the second pump is operated.
摘要翻译：该液体供给系统具有第一和第二泵，每个泵设有柱塞。通过每个泵吸入口吸入的液体通过第一泵和/或第二泵排出排出口。在启动运行模式下，第二个泵停止运转，只有第一个泵运转。当排出口的排出压力达到预定值时，启动操作模式转换到正常操作模式。在正常运行模式下，第一个泵停止运转，只有第二个泵运转。

35. 发明申请

US20050095145A1 Liquid chromatograph pump and control method therefor 失效
公开(公告)号：US20050095145A1
公开(公告)日：2005-05-05
申请号：US10998937
申请日：2004-11-30
申请人： Kenji Hiraku , Kunihiko Takao , Hironori Kaji , Masahito Ito
发明人： Kenji Hiraku , Kunihiko Takao , Hironori Kaji , Masahito Ito
IPC分类号： G01N30/32 , F04B11/00 , F04B13/00 , F04B49/06 , G01N30/34 , F04B49/00 , F04B5/00
CPC分类号： F04B13/00 , F04B11/0083 , F04B49/06 , F04B2205/04 , G01N30/34 , G01N30/36
摘要： In a pump for feeding a liquid for chromatography, first and second plungers form first and second volumes respectively together with first and second chambers, the first plunger is prevented from changing the first volume sufficiently for feeding the liquid between the first and second volumes when the second plunger decreases the second volume to discharge the fluid from the second volume to an outlet path of the pump for the chromatography.

36. 发明授权

US5512170A Liquid chromatograph 失效
标题翻译：液相色谱仪
公开(公告)号：US5512170A
公开(公告)日：1996-04-30
申请号：US356751
申请日：1994-12-15
申请人： Yoshiaki Yamada , Hironori Kaji
发明人： Yoshiaki Yamada , Hironori Kaji
IPC分类号： G01N1/00 , G01N30/02 , G01N30/16 , G01N30/20 , G01N30/24 , G01N30/88 , B01D15/08
CPC分类号： G01N35/1097 , G01N30/24 , G01N2030/027 , G01N2030/8804 , G01N30/16 , G01N30/20
摘要： The volume of the sample added to the sample retainer and the capacity of the sample retainer are compared, and the less one is stored as volume of the sample injected to a sample separating column. If the volume of the sample added to the sample retainer is more than the capacity of the sample retainer, accordingly, the capacity of the sample retainer is stored.
摘要翻译：比较添加到样品保持器中的样品的体积和样品保持器的容量，并将较少的样品作为样品注入样品分离柱的体积存储。如果添加到样品保持器中的样品的体积大于样品保持器的容量，则存储样品保持器的容量。

37. 发明授权

US09410543B2 Pump for liquid chromatograph, and liquid chromatograph 有权
标题翻译：液相色谱泵，液相色谱仪
公开(公告)号：US09410543B2
公开(公告)日：2016-08-09
申请号：US13808660
申请日：2011-07-20
申请人： Kenichiro Tokuo , Kenji Hiraku , Hironori Kaji , Daisuke Akieda , Kimihiko Ishii , Naoya Yasuhara
发明人： Kenichiro Tokuo , Kenji Hiraku , Hironori Kaji , Daisuke Akieda , Kimihiko Ishii , Naoya Yasuhara
IPC分类号： F04B17/03 , F04B13/00 , F04B23/06 , F04B49/06 , G01N30/32 , G01N30/02 , F04B49/08 , G01N30/34
CPC分类号： F04B17/03 , F04B13/00 , F04B23/06 , F04B49/06 , F04B49/065 , F04B49/08 , F04B2203/0202 , F04B2205/03 , F04B2205/05 , G01N30/02 , G01N30/32 , G01N30/34 , G01N2030/326
摘要： A pump controller causes a first plunger pump and a second plunger pump connected in series or in parallel to perform intake and compression actions alternately at substantially constant cycles, sets a pressurizing chamber of one of the plunger pumps to a state of a higher pressure than the pressurizing chamber of the other plunger pump, and performs flow rate control by adjusting lift amounts of the first plunger and the second plunger. Thus, it is possible to provide a pump for liquid chromatograph, and a liquid chromatograph, which are capable of reducing pulsations even when an ejection flow rate is changed.
摘要翻译：泵控制器使得串联或并联连接的第一柱塞泵和第二柱塞泵以基本恒定的循环交替进行进入和压缩动作，将柱塞泵之一的加压室设定为比通过调节第一柱塞和第二柱塞的升程量来进行流量控制。因此，即使在喷射流量变化的情况下，也能够提供能够降低脉动的液相色谱泵和液相色谱仪。

38. 发明授权

US09018325B2 Catalyst for living radical polymerization and polymerization method 有权
标题翻译：催化剂用于活性自由基聚合和聚合方法
公开(公告)号：US09018325B2
公开(公告)日：2015-04-28
申请号：US14240607
申请日：2012-08-24
申请人： Atsushi Goto , Hironori Kaji
发明人： Atsushi Goto , Hironori Kaji
IPC分类号： C08F4/00 , C07C211/62 , C07F9/54 , C08F212/08 , C08F220/18 , C08F220/20 , C08F220/34 , C08F220/44 , C08F220/10 , C08F220/14 , C08F220/28 , C08F220/32
CPC分类号： C08F4/00 , C08F212/08 , C08F220/14 , C08F220/18 , C08F220/20 , C08F220/34 , C08F220/44 , C08F2220/1825 , C08F2220/1841 , C08F2220/1883 , C08F2220/286 , C08F2220/325 , C08F2438/00 , C08F2220/1858
摘要： A nonmetallic compound having an ionic bond with a halide ion is used as a catalyst for living radical polymerization. Even if a radical initiator is not used, a monomer can be subjected to a radical polymerization to obtain a polymer having narrow molecular weight distribution. The cost of the living radical polymerization can be remarkably reduced, and it is made possible to prevent adverse effects of using a radical initiator (such as side reactions). The present invention is significantly more environmentally friendly and economically excellent than conventional living radical polymerization methods, due to advantages such as low toxicity of the catalyst, low amount of the catalyst necessary, high solubility of the catalyst, mild reaction conditions, and no coloration/no odor, etc. The catalyst can be applied to various monomers and enables synthesis of high molecular weight polymers.
摘要翻译：使用与卤离子具有离子键的非金属化合物作为活性自由基聚合的催化剂。即使不使用自由基引发剂，也可以对单体进行自由基聚合，得到分子量分布窄的聚合物。活性自由基聚合的成本可以显着降低，并且可以防止使用自由基引发剂（例如副反应）的不利影响。本发明由于催化剂毒性低，催化剂用量少，催化剂溶解性高，反应条件温和，无着色/无色性等优点，比现有的活性自由基聚合方法显着更环保，经济，没有气味等。催化剂可以应用于各种单体，并能够合成高分子量聚合物。

39. 发明申请

US20140303334A1 CATALYST FOR LIVING RADICAL POLYMERIZATION AND POLYMERIZATION METHOD 有权
标题翻译：用于生物聚合和聚合方法的催化剂
公开(公告)号：US20140303334A1
公开(公告)日：2014-10-09
申请号：US14240607
申请日：2012-08-24
申请人： Atsushi Goto , Hironori Kaji
发明人： Atsushi Goto , Hironori Kaji
IPC分类号： C08F4/00
CPC分类号： C08F4/00 , C08F212/08 , C08F220/14 , C08F220/18 , C08F220/20 , C08F220/34 , C08F220/44 , C08F2220/1825 , C08F2220/1841 , C08F2220/1883 , C08F2220/286 , C08F2220/325 , C08F2438/00 , C08F2220/1858
摘要： A nonmetallic compound having an ionic bond with a halide ion is used as a catalyst for living radical polymerization. Even if a radical initiator is not used, a monomer can be subjected to a radical polymerization to obtain a polymer having narrow molecular weight distribution. The cost of the living radical polymerization can be remarkably reduced, and it is made possible to prevent adverse effects of using a radical initiator (such as side reactions). The present invention is significantly more environmentally friendly and economically excellent than conventional living radical polymerization methods, due to advantages such as low toxicity of the catalyst, low amount of the catalyst necessary, high solubility of the catalyst, mild reaction conditions, and no coloration/no odor, etc. The catalyst can be applied to various monomers and enables synthesis of high molecular weight polymers.
摘要翻译：使用与卤离子具有离子键的非金属化合物作为活性自由基聚合的催化剂。即使不使用自由基引发剂，也可以对单体进行自由基聚合，得到分子量分布窄的聚合物。活性自由基聚合的成本可以显着降低，并且可以防止使用自由基引发剂（例如副反应）的不利影响。本发明由于催化剂毒性低，催化剂用量低，催化剂溶解性高，反应条件温和，无着色/无色性等优点，比现有的活性自由基聚合方法显着提高环保性和经济性，没有气味等。催化剂可以应用于各种单体，并能够合成高分子量聚合物。

40. 发明授权

US08551423B2 Liquid supply device using check valve and reactive liquid chromatography system 失效
标题翻译：液体供应装置采用止回阀和反应液相色谱系统
公开(公告)号：US08551423B2
公开(公告)日：2013-10-08
申请号：US13386789
申请日：2010-05-26
申请人： Kisaburo Deguchi , Hironori Kaji , Kimihiko Ishii , Daisuke Akieda , Kunihiko Takao , Masaru Yamasaki , Kenji Hiraku , Yoshihiro Nagaoka
发明人： Kisaburo Deguchi , Hironori Kaji , Kimihiko Ishii , Daisuke Akieda , Kunihiko Takao , Masaru Yamasaki , Kenji Hiraku , Yoshihiro Nagaoka
IPC分类号： B01L3/02
CPC分类号： F04B23/06 , F04B13/00 , F04B49/08 , F04B49/22 , F04B2205/05 , F16K15/04 , F16K37/0058 , G01N30/32 , G01N30/74 , G01N2030/328 , G01N2030/8435 , Y10T137/7838
摘要： It is possible to correctly determine whether a change in the pressure or flow rate is caused by normal opening and closing operations of a check valve and to monitor in real time whether an operation of a check valve is normal or abnormal in a liquid supply device. Light is introduced in the check valve and a change in the quantity of light transmitted through or reflected by the check valve, caused by the opening and closing of the valve is detected, so that the opening and closing operations of the check valve can be directly detected. The check valve is arranged in a pipe in the liquid supply device, and a change in the pressure in the pipe is monitored on the basis of a signal from a pressure sensor and a signal which represents the opening and closing of the check valve.
摘要翻译：可以正确地确定压力或流量的变化是否由止回阀的正常的打开和关闭操作引起，并且实时监测液体供应装置中止回阀的操作是否正常或异常。在止回阀中引入光，并且检测到由阀的打开和关闭引起的止回阀透过或反射的光量的变化，使得止回阀的打开和关闭操作可以直接检测到。止回阀布置在液体供应装置中的管道中，并且基于来自压力传感器的信号和表示止回阀的打开和关闭的信号来监测管道中的压力变化。

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