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    • 3. 发明申请
    • METHOD FOR PREPARATION OF SUBSTRATES FOR THIN FILM SUPERCONDUCTORS AND IMPROVED DEVICES INCORPORATING SUBSTRATES
    • 薄膜超导体基板的制备方法和改良基板的装置
    • WO9850965A9
    • 1999-03-25
    • PCT/US9807579
    • 1998-04-15
    • SUPERCONDUCTOR TECH
    • EDDY MICHAEL MZUCK BETTY FFIRPO GREGORY G
    • H01L39/24
    • H01L39/2458
    • Improved reproducibility of fabrication of superconducting thin film devices on MgO substrates is accomplished through use of the inventive procedure. As a first step of the process, the surface of the MgO is removed. Preferably, the surface is removed through argon plasma bombardment, whether with low energy or high energy ions. Most preferably, ion milling is utilized, with superior results being obtained by milling at 90 DEG to the surface of the substrate. The second step of the invention is to anneal the MgO substrate. This effects recrystallization of the substrate. In the preferred embodiment, the substrate is annealed at approximately 1050 DEG C in 17 % dry oxygen, 83 % dry nitrogen for 2.5 hours. Lower temperatures, such as 950 DEG C, may be utilized, though the anneal times, e.g., three hours or greater, impacts upon the commercial viability of the process. Higher temperatures, e.g., 1150 DEG C, permit steps in the surface to become unacceptably large, and often permit second phases to migrate to the surface of the substrate. Varying other factors, such as the oxygen partial pressure, change the optimal anneal temperature. Structurally, the resultant surface manifests steps or terraces, which comprise exposed peripheral edges of atomic planes within the substrate. Optionally, additional cleanings steps are performed. Devices fabricated from filling formed with the inventive method result in higher quality and more uniform devices.
    • 通过使用本发明的方法来实现在MgO衬底上制造超导薄膜器件的改进的再现性。 作为该方法的第一步,除去MgO的表面。 优选地,无论是用低能量还是高能离子,通过氩等离子体轰击去除表面。 最优选地,使用离子研磨,通过在90°下研磨到基材的表面获得优异的结果。 本发明的第二步骤是使MgO基板退火。 这会影响底物的再结晶。 在优选的实施方案中,将基材在约1050℃下在17%干燥氧气,83%干燥氮气中退火2.5小时。 尽管退火时间(例如三小时或更长)也会影响工艺的商业可行性,但可以使用较低的温度,例如950℃。 更高的温度,例如1150℃,允许表面中的步骤变得不可接受地大,并且通常允许第二相迁移到基底的表面。 改变其他因素,如氧分压,改变最佳退火温度。 在结构上,所得到的表面表现出步骤或梯田,其包括在基底内的原子平面的暴露的外围边缘。 可选地,执行额外的清洁步骤。 由本发明方法形成的填充物制成的装置导致更高质量和更均匀的装置。
    • 6. 发明申请
    • COATED CONDUCTOR HIGH TEMPERATURE SUPERCONDUCTORS WITH INTRINSIC PINNING CENTERS
    • 涂层导体高温超导体,内置密封中心
    • WO2015054119A1
    • 2015-04-16
    • PCT/US2014/059279
    • 2014-10-06
    • SUPERCONDUCTOR TECHNOLOGIES, INC.
    • HUH, Jeong-Uk
    • H01L39/24
    • H01B12/06H01L39/126H01L39/143H01L39/2432H01L39/2458H01L39/2461
    • A coated conductor comprises a substrate supporting a ReBCO superconductor adapted to carry current in a superconducting state. The superconductor is characterized in having peaks in critical current (J c ) of at least 0.2 MA/cm 2 in a magnetic field of about 1 Tesla when the field is applied normal to the surface of the superconductor and when the field is applied parallel to the surface of the superconductor, and further characterized in that the superconductor includes horizontal defects and columnar defects in a size and an amount sufficient to result in the said critical current response. The conductor is characterized in that the ratio of the height of the peaks in the J c is in the range from 3:1 with the ratio of the field perpendicular (0 degrees) to the field parallel (+/- 90 degrees) to the range from 3:1 with the ratio of the field parallel to the field perpendicular.
    • 涂覆导体包括支撑适于承载超导状态的电流的ReBCO超导体的衬底。 超导体的特征在于当场施加到超导体的表面时以及平行于表面施加场时,在约1特斯拉的磁场中,临界电流(Jc)的峰值为至少0.2MA / cm 2 的超导体,其特征还在于,超导体包括足以导致所述临界电流响应的尺寸和量的水平缺陷和柱状缺陷。 导体的特征在于,Jc中的峰的高度的比例在3:1的范围内,场的垂直(0度)与场平行(+/- 90度)的比率与范围 从3:1,场平均与场垂直的比率。