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1. 发明申请

WO2017091815A1 FORMATION OF THREE-DIMENSIONAL MATERIALS BY COMBINING CATALYTIC AND PRECURSOR MATERIALS 审中-公开
标题翻译：催化剂和前体材料结合形成三维材料
公开(公告)号：WO2017091815A1
公开(公告)日：2017-06-01
申请号：PCT/US2016/063776
申请日：2016-11-25
申请人： WILLIAM MARSH RICE UNIVERSITY , TIANJIN UNIVERSITY
发明人： TOUR, James, M. , SHA, Junwei , ZHAO, Naiqin
IPC分类号： C01B32/15 , C01B32/162 , C01B32/184 , B01J35/02 , C23F4/04 , B82Y40/00 , B82Y30/00
CPC分类号： B82Y40/00 , B82Y30/00 , H01M4/583 , H01M4/96
摘要： Embodiments of the present disclosure pertain to methods of making three-dimensional materials by combining a catalytic material with a precursor material and forming the three- dimensional material from the precursor material in the presence of the catalytic material. The three-dimensional material may be formed on surfaces and internal cavities of the catalytic material. The formed three-dimensional material includes a plurality of connected units that are derived from the precursor materials. The methods of the present disclosure may also include steps of separating catalytic materials from the formed three-dimensional materials and incorporating the three-dimensional materials as a component of an energy storage device (e.g., as an electrode in a capacitor). Additional embodiments of the present disclosure pertain to the formed three-dimensional materials.
摘要翻译：本公开的实施例涉及通过将催化材料与前体材料组合并且在催化材料存在下由前体材料形成三维材料来制造三维材料的方法。三维材料可以形成在催化材料的表面和内腔上。所形成的三维材料包括源自前体材料的多个连接单元。本公开的方法还可以包括从形成的三维材料分离催化材料并且将三维材料结合为能量存储装置的组件（例如，作为电容器中的电极）的步骤。本公开的另外的实施方式涉及所形成的三维材料。

2. 发明申请

WO2018017369A3 THREE-DIMENSIONAL (3D) PRINTING OF GRAPHENE MATERIALS 审中-公开
公开(公告)号：WO2018017369A3
公开(公告)日：2018-01-25
申请号：PCT/US2017/041768
申请日：2017-07-12
申请人： WILLIAM MARSH RICE UNIVERSITY
发明人： TOUR, James, M. , SHA, Junwei , LI, Yilun , MILLER, Jordan , KINSTLINGER, Ian , COFER, Savannah , CHYAN, Yieu
IPC分类号： C01B32/186 , H01G11/24 , H01G11/26 , C01B32/194
摘要： Three-dimensional (3D) printing of graphene materials and methods and apparatuses for making same. In some embodiments, combined metal powder and carbon growth sources (such as powder Ni and sucrose) are utilized in the 3D printing process. In other embodiments, metal powders with binders (such as powder Ni and a polymer bases binder) are utilized in the 3D printing process. The metal in the resulting 3D printed composite material can then be etched or otherwise removed yielding the 3D printed graphene materials.

3. 发明申请

WO2017164963A9 FACILE PREPARATION OF CARBON NANOTUBE HYBRID MATERIALS BY CATALYST SOLUTIONS 审中-公开
标题翻译：碳纳米管杂化材料催化剂的简易制备
公开(公告)号：WO2017164963A9
公开(公告)日：2017-09-28
申请号：PCT/US2017/012706
申请日：2017-01-09
申请人： WILLIAM MARSH RICE UNIVERSITY
发明人： TOUR, James , SALVATIERRA, Rodrigo, Villegas , ZAKHIDOV, Dante , SHA, Junwei
IPC分类号： C01B31/04
摘要： Embodiments of the present disclosure pertain to methods of making a carbon nanotube hybrid material by depositing a catalyst solution onto a carbon-based material, and growing carbon nanotubes on the carbon-based material such that the grown carbon nanotubes become covalently linked to the carbon-based material through carbon-carbon bonds. The catalyst solution includes a metal component (e.g., iron) and a buffer component (e.g., aluminum) that may be in the form of particles. The metal component of the particle may be in the form of a metallic core or metallic oxide core while the buffer component may be on a surface of the metal component in the form of metal or metal oxides. Further embodiments of the present disclosure pertain to the catalytic particles and carbon nanotube hybrid materials. The carbon nanotube hybrid materials of the present disclosure may be incorporated as electrodes (e.g., anodes or cathodes) in energy storage devices.
摘要翻译：本公开的实施方式涉及通过将催化剂溶液沉积到碳基材料上并且在碳基材料上生长碳纳米管来制造碳纳米管混合材料的方法，使得生长的碳碳纳米管通过碳 - 碳键与碳基材料共价连接。催化剂溶液包括可以呈颗粒形式的金属组分（例如铁）和缓冲剂组分（例如铝）。颗粒的金属组分可以是金属芯或金属氧化物芯的形式，而缓冲组分可以金属或金属氧化物形式存在于金属组分的表面上。本公开的另外的实施方式涉及催化颗粒和碳纳米管混合材料。本公开的碳纳米管混合材料可以作为电极（例如，阳极或阴极）结合在能量存储装置中。

4. 发明申请

WO2018017369A2 THREE-DIMENSIONAL (3D) PRINTING OF GRAPHENE MATERIALS 审中-公开
标题翻译：石墨材料的三维（3D）印刷
公开(公告)号：WO2018017369A2
公开(公告)日：2018-01-25
申请号：PCT/US2017/041768
申请日：2017-07-12
申请人： WILLIAM MARSH RICE UNIVERSITY
发明人： TOUR, James, M. , SHA, Junwei , LI, Yilun , MILLER, Jordan , KINSTLINGER, Ian , COFER, Savannah , CHYAN, Yieu
IPC分类号： C01B32/186 , H01G11/24 , H01G11/26 , C01B32/194
摘要： Three-dimensional (3D) printing of graphene materials and methods and apparatuses for making same. In some embodiments, combined metal powder and carbon growth sources (such as powder Ni and sucrose) are utilized in the 3D printing process. In other embodiments, metal powders with binders (such as powder Ni and a polymer bases binder) are utilized in the 3D printing process. The metal in the resulting 3D printed composite material can then be etched or otherwise removed yielding the 3D printed graphene materials.
摘要翻译：石墨烯材料的三维（3D）印刷以及用于制造石墨烯材料的方法和设备。在一些实施例中，在3D打印过程中使用组合金属粉末和碳生长源（例如粉末Ni和蔗糖）。在其他实施例中，在3D打印过程中使用具有粘合剂（例如粉末Ni和聚合物基料粘合剂）的金属粉末。然后可以蚀刻或除去所得到的3D印刷复合材料中的金属，得到3D印刷的石墨烯材料。

5. 发明申请

WO2017164963A3 FACILE PREPARATION OF CARBON NANOTUBE HYBRID MATERIALS BY CATALYST SOLUTIONS 审中-公开
公开(公告)号：WO2017164963A3
公开(公告)日：2017-09-28
申请号：PCT/US2017/012706
申请日：2017-01-09
申请人： WILLIAM MARSH RICE UNIVERSITY
发明人： TOUR, James , SALVATIERRA, Rodrigo, Villegas , ZAKHIDOV, Dante , SHA, Junwei
IPC分类号： C01B31/04
摘要： Embodiments of the present disclosure pertain to methods of making a carbon nanotube hybrid material by depositing a catalyst solution onto a carbon-based material, and growing carbon nanotubes on the carbon-based material such that the grown carbon nanotubes become covalently linked to the carbon-based material through carbon-carbon bonds. The catalyst solution includes a metal component (e.g., iron) and a buffer component (e.g., aluminum) that may be in the form of particles. The metal component of the particle may be in the form of a metallic core or metallic oxide core while the buffer component may be on a surface of the metal component in the form of metal or metal oxides. Further embodiments of the present disclosure pertain to the catalytic particles and carbon nanotube hybrid materials. The carbon nanotube hybrid materials of the present disclosure may be incorporated as electrodes (e.g., anodes or cathodes) in energy storage devices.

6. 发明申请

WO2017164963A2 FACILE PREPARATION OF CARBON NANOTUBE HYBRID MATERIALS BY CATALYST SOLUTIONS 审中-公开
公开(公告)号：WO2017164963A2
公开(公告)日：2017-09-28
申请号：PCT/US2017/012706
申请日：2017-01-09
申请人： WILLIAM MARSH RICE UNIVERSITY
发明人： TOUR, James , SALVATIERRA, Rodrigo, Villegas , ZAKHIDOV, Dante , SHA, Junwei
IPC分类号： C01B31/04
CPC分类号： C01B32/162 , B01J21/04 , B01J23/72 , B01J23/745 , B82Y30/00 , B82Y40/00 , C01B32/16 , C01B2202/22 , C01B2202/32 , C01P2006/12 , H01G11/36 , H01M4/0428 , H01M4/13 , H01M4/139 , H01M4/362 , H01M4/583 , H01M4/587 , H01M4/663 , H01M4/9083 , H01M4/96 , H01M2004/021 , H01M2004/027 , Y10S977/742 , Y10S977/843 , Y10S977/948
摘要： Embodiments of the present disclosure pertain to methods of making a carbon nanotube hybrid material by depositing a catalyst solution onto a carbon-based material, and growing carbon nanotubes on the carbon-based material such that the grown carbon nanotubes become covalently linked to the carbon-based material through carbon-carbon bonds. The catalyst solution includes a metal component (e.g., iron) and a buffer component (e.g., aluminum) that may be in the form of particles. The metal component of the particle may be in the form of a metallic core or metallic oxide core while the buffer component may be on a surface of the metal component in the form of metal or metal oxides. Further embodiments of the present disclosure pertain to the catalytic particles and carbon nanotube hybrid materials. The carbon nanotube hybrid materials of the present disclosure may be incorporated as electrodes (e.g., anodes or cathodes) in energy storage devices.

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