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1. 发明申请

WO0183567A3 NITROAROMATIC SOLUBILIZER FOR NITROXYLS IN AROMATIC SOLVENTS 审中-公开
标题翻译：用于芳香族溶剂中硝基的硝基自由基溶解剂
公开(公告)号：WO0183567A3
公开(公告)日：2002-06-06
申请号：PCT/US0110625
申请日：2001-04-03
申请人： UNIROYAL CHEM CO INC
发明人： GEELAN BRENDAN J , BENAGE BRIGITTE , ABRUSCATO GERALD J , SCHLUP KIRK A , GREWAL RUBEN S , EISENSTEIN ANDREW J
IPC分类号： C09K3/00 , C07B63/04 , C07C291/02 , C07D211/94 , C07D295/24 , C08F2/00 , C08F4/04
CPC分类号： C07D295/24 , C07B63/04 , C07C291/02 , C07D211/94
摘要： Disclosed herein is a method for increasing the solubility of a compound having the structural formula (I), in an aromatic hydrocarbon solvent comprising adding to said solvent a nitroaromatic compound having the structure (II) wherein, in formula (II), R25, R26, R27, R28, R29 and R30 are independently selected from the group consisting of hydrogen, alkyl, aryl, cycloalkyl, heterocyclic, substituted alkyl, substituted aryl, OR11, NR11R12, SR11, NO2, NO, CN, COR11, COOR11, CONR11R12, NR11COR12, halogen, and/or any two adjacent groups can be taken together to form ring structures(s) of five to seven members, provided that at least one of R25, R26, R27, R28, R29 and R30 is NO2, and R11 and R12 are independently selected from the group consisting of hydrogen, alkyl, aryl, benzyl, cyclic, heterocyclic, and substituted alkyl or aryl where the substituents are C, O, N, S, or P, or R11 and R12 can be taken together to form a ring structure of five to seven members and, in formula (I), R1 and R4 are independently selected from the group consisting of hydrogen, alkyl, and heteroatom-substituted alkyl and R2 and R3 are independently selected from the group consisting of alkyl and heteroatom-substituted alkyl; and X1 and X2 (1) are independently selected from the group consisting of halogen, cyano, COOR7, -S-COR7, -OCOR7, (wherein R7 is alkyl or aryl), amido, -S-C6H5, carbonyl, alkenyl, or alkyl of 1 to 15 carbon atoms, or (2) taken together, form a ring structure of five to seven members with the nitrogen.
摘要翻译：本文公开了一种在芳族烃溶剂中提高具有结构式（I）的化合物的溶解度的方法，包括向所述溶剂中加入具有结构式（II）的硝基芳族化合物，其中在式（II）中，R 25，R 26 R27，R28，R29和R30独立地选自氢，烷基，芳基，环烷基，杂环，取代的烷基，取代的芳基，OR11，NR11R12，SR11，NO2，NO，CN，COR11，COOR11，CONR11R12， NR 11 COR 12，卤素和/或任何两个相邻基团可以一起形成五至七个成员的环结构，条件是R 25，R 26，R 27，R 28，R 29和R 30中的至少一个是NO 2，R 11 R 12独立地选自氢，烷基，芳基，苄基，环状，杂环和取代的烷基或芳基，其中取代基是C，O，N，S或P，或者R 11和R 12可以一起形成5至7个成员的环结构，并且在式（I）中，R 1和R 3 4独立地选自氢，烷基和杂原子取代的烷基，并且R 2和R 3独立地选自烷基和杂原子取代的烷基; 和X 1和X 2（1）独立地选自卤素，氰基，COOR 7，-S-COR 7，-OCOR 7，（其中R 7是烷基或芳基），酰氨基，-S-C 6 H 5，羰基，烯基或 1〜15个碳原子的烷基，或（2）一起，与氮形成5〜7个成员的环结构。

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