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1. 发明申请

WO2010034111A1 PROCESS FOR PRODUCING CHLORINE DIOXIDE USING WASTE GLYCEROL FROM A BIODIESEL PLANT 审中-公开
标题翻译：生物柴油厂使用废弃甘油的二氧化氯生产工艺
公开(公告)号：WO2010034111A1
公开(公告)日：2010-04-01
申请号：PCT/CA2009/001331
申请日：2009-09-22
申请人： FPINNOVATIONS , JEMAA, Naceur , PALEOLOGOU, Michael
发明人： JEMAA, Naceur , PALEOLOGOU, Michael
IPC分类号： C01B11/02 , C10G3/00
CPC分类号： C01B11/023 , C10G2300/1014 , C10L1/026 , Y02E50/13 , Y02P30/20
摘要： A process for chlorine dioxide production uses waste glycerol from biodiesel plants as a reducing agent. This untreated waste stream may contain other reducing agents such as sodium chloride and methanol which were found to enhance the chlorine dioxide production. Other chemicals present in this waste stream did not affect the operation of the chlorine dioxide generator. Substituting the waste glycerol for methanol or other reducing agents helps kraft pulp mills in reducing the cost of producing chlorine dioxide while providing a use for the untreated waste glycerol stream.
摘要翻译：生产二氧化氯的方法使用来自生物柴油植物的废甘油作为还原剂。这种未经处理的废物流可能含有其他还原剂，如氯化钠和甲醇，这些还原剂可以增强二氧化氯的产生。存在于该废物流中的其它化学物质不影响二氧化氯发生器的运行。将废甘油代替甲醇或其它还原剂可以帮助牛皮纸浆厂减少生产二氧化氯的成本，同时为未处理的废甘油流提供用途。

2. 发明申请

WO2009079746A1 USE OF CHEMICAL PULP MILL STEAM STRIPPER OFF GASES CONDENSATE AS REDUCING AGENT IN CHLORINE DIOXIDE PRODUCTION 审中-公开
标题翻译：使用化学粉末蒸汽分离器将气体冷凝成二氧化氯生产中的还原剂
公开(公告)号：WO2009079746A1
公开(公告)日：2009-07-02
申请号：PCT/CA2008/002010
申请日：2008-11-12
申请人： FPINNOVATIONS , JEMAA, Naceur , PALEOLOGOU, Michael , SACCIADIS, George , BERRY, Richard M.
发明人： JEMAA, Naceur , PALEOLOGOU, Michael , SACCIADIS, George , BERRY, Richard M.
IPC分类号： C01B11/02 , D21C11/06
CPC分类号： C01B11/023 , D21C9/14 , D21C11/06
摘要： Steam stripper off gas from chemical pulp mills, for example kraft or sulphite pulp mills is rich in methanol and totally reduced sulphur (TRS) compounds. This gaseous stream is usually burned to avoid further handling of this TRS-rich, odorous stream. We found that once this gaseous stream is condensed, it can be used as a reducing agent in the chlorine dioxide generator, in place of purchased methanol. Surprisingly, we found that, in addition to the methanol component, the TRS components act as reducing agents during the production of chlorine dioxide or, at the very least, do not consume chlorine dioxide. The use of this stream in the ClO 2 generator will allow pulp mills to reduce or eliminate the consumption of purchased methanol while providing a new approach to deal with TRS compounds in the chlorine dioxide generator rather than employing a dedicated TRS incinerator or any other combustion device.
摘要翻译：来自化学纸浆厂的蒸汽汽提器，例如硫酸盐或亚硫酸盐纸浆厂富含甲醇和完全还原的硫（TRS）化合物。这种气流通常被燃烧以避免进一步处理这种富含TRS的气味流。我们发现，一旦气态物流被冷凝，就可以用二氧化氯发生器中的还原剂代替购买的甲醇。令人惊讶的是，我们发现除了甲醇成分之外，TRS成分在二氧化氯生产过程中起减压剂的作用，或至少不消耗二氧化氯。在ClO2发生器中使用这种料流将允许纸浆厂减少或消除购买的甲醇的消耗，同时提供了处理二氧化氯发生器中的TRS化合物的新方法，而不是使用专用的TRS焚化炉或任何其它燃烧装置。

3. 发明申请

WO2009012597A1 PROCESS FOR TREATING PULP MILL CONDENSATES USING A HOLLOW FIBER CONTACTOR 审中-公开
标题翻译：使用中空纤维接触器处理浆料冷凝液的方法
公开(公告)号：WO2009012597A1
公开(公告)日：2009-01-29
申请号：PCT/CA2008/001373
申请日：2008-07-24
申请人： FPINNOVATIONS , JEMAA, Naceur , PALEOLOGOU, Michael , O'CONNOR, Brian
发明人： JEMAA, Naceur , PALEOLOGOU, Michael , O'CONNOR, Brian
IPC分类号： C02F1/44 , B01D63/04 , C02F1/00 , C02F1/26 , D21C11/00 , B01D53/22
CPC分类号： B01D63/02 , B01D61/246 , B01D2311/13 , C02F1/20 , C02F2103/28 , C02F2301/063 , D21C11/00
摘要： A method and apparatus for the treatment of pulp mill condensates is described. A hollow fiber contactor, incorporating a hydrophobic membrane, was used to remove several undesirable compounds from pulp mill condensates. For example, TRS compounds and SO 2 were efficiently stripped from kraft and sulphite mill evaporator condensates, respectively. Methanol was also removed from kraft mill condensates but at a lower efficiency than TRS. Furthermore, other undesirable compounds found in condensates of pulp mills that contribute to the BOD and COD loading to effluent treatment systems were also removed. These contactors are cost effective since air, vacuum or a suitable solvent or scrubbing solution can be used as the stripping medium to drive off through the membrane several undesirable compounds from the feed solution. The undesirable compounds removed can thus be burned in the recovery boiler, lime kiln or a dedicated boiler.
摘要翻译：描述了用于处理纸浆厂冷凝物的方法和设备。使用掺入疏水膜的中空纤维接触器从纸浆厂冷凝物中除去若干不需要的化合物。例如，TRS化合物和SO 2分别从硫酸盐和亚硫酸盐蒸发器冷凝物中有效地脱除。甲醇也从牛皮纸浆冷凝物中除去，但效率低于TRS。此外，在纸浆厂的冷凝物中发现的有助于污水处理系统的BOD和COD负载的其他不希望的化合物也被去除。这些接触器具有成本效益，因为空气，真空或合适的溶剂或洗涤溶液可用作汽提介质以从进料溶液中排出几个不需要的化合物。因此，除去的不需要的化合物可以在回收锅炉，石灰窑或专用锅炉中燃烧。

4. 发明申请

WO2011017797A1 FRACTIONATION OF A WASTE LIQUOR STREAM FROM NANOCRYSTALLINE CELLULOSE PRODUCTION 审中-公开
标题翻译：来自纳米晶体纤维素生产的废液流的分离
公开(公告)号：WO2011017797A1
公开(公告)日：2011-02-17
申请号：PCT/CA2010/001198
申请日：2010-07-28
申请人： FPINNOVATIONS , JEMAA, Naceur , PALEOLOGOU, Michael , ZHANG, Xiao
发明人： JEMAA, Naceur , PALEOLOGOU, Michael , ZHANG, Xiao
IPC分类号： C01B17/90 , B01D61/00 , C08B1/00 , D21C11/00
CPC分类号： D21C9/00 , B01D61/027 , C01B17/902 , C08B15/08 , D21C11/0007
摘要： During nanocrystalline cellulose (NCC) production, a considerable amount of sulphuric acid is used. After the separation of the NCC, the remaining solution contains sugars and residual sulphuric acid. The sugars are in the monomeric and oligomeric forms. To reduce the cost of NCC production and to produce other added-value products, the spent acid stream can be fractionated into sugar oligomers, sugar monomers, and acid. The acid can be recycled to the NCC manufacturing process after concentration. The sugar monomers and sugar oligomers can be used for the manufacturing of other valuable chemicals. Membrane nanofiltration can be used to achieve this objective. A polymeric membrane with a molecular weight cut-off in the range of 200 Dalton was employed. Using this approach, the majority of the acid was recovered in the permeate while the sugars were concentrated in a smaller stream. The sugar level in the separated acid/permeate stream was only about 3% of the original concentration. A second membrane filtration stage can be used to separate the monomeric from the oligomeric sugars. The two sugar streams can be employed in different applications to produce value-added products.
摘要翻译：在纳米晶纤维素（NCC）生产过程中，使用了大量的硫酸。在分离NCC后，剩余的溶液含有糖和残留的硫酸。糖是单体和低聚物形式。为了降低NCC生产成本和生产其他附加值产品，废酸流可以分馏成糖低聚物，糖单体和酸。浓缩后，酸可以回收到NCC制造过程。糖单体和糖低聚物可用于制造其他有价值的化学品。膜纳米过滤可以用来达到这个目的。使用分子量截止值在200道尔顿范围内的聚合物膜。使用这种方法，大部分酸在渗透物中回收，而糖被浓缩在较小的流中。分离的酸/渗透物流中的糖含量仅为原始浓度的约3％。可以使用第二膜过滤阶段将单体与低聚糖分离。这两种糖流可用于不同的应用，以产生增值产品。

5. 发明申请

WO2019153085A1 MELTABLE LIGNIN COMPOSITIONS, METHOD FOR PRODUCING THEM AND THEIR USES 审中-公开
公开(公告)号：WO2019153085A1
公开(公告)日：2019-08-15
申请号：PCT/CA2019/050161
申请日：2019-02-07
申请人： FPINNOVATIONS
发明人： LALEG, Makhlouf , JEMAA, Naceur , WAFA AL DAJANI, Waleed , ZHANG, Yaolin , PALEOLOGOU, Michael
IPC分类号： C08J3/12 , B29B7/00 , C08L97/00 , D21C11/00
摘要： Novel meltable lignin compositions having tailored compatibilities, moisture/water-resistant adhesion characteristics, and low to medium glass transition temperatures (30 to 120 o C) desirable for applications in the manufacturing of various products and the integration in the formulations of adhesives, coatings, plastics, composites and masterbatches, are obtained by blending at low temperatures (0-120 o C) dry lignins (0 to 10% moisture), in their hydrogen or protonated forms - hereby referred to as H-forms (pH = 2.3-6.5 for a 10% aqueous suspension), with a reactive and/or interactive molecule or combination of molecules.

6. 发明申请

WO2017181280A1 LIGNIN RECOVERY AND FURFURAL PRODUCTION FROM BIOMASS PREHYDROLYSATE STREAMS 审中-公开
标题翻译：生物质解氢化物流的木质素回收和糠醛生产
公开(公告)号：WO2017181280A1
公开(公告)日：2017-10-26
申请号：PCT/CA2017/050486
申请日：2017-04-20
申请人： FPINNOVATIONS
发明人： JEMAA, Naceur , MAZAR, Adil , WAFA AL DAJANI, Waleed , PALEOLOGOU, Michael
IPC分类号： C07D307/50
摘要： The present invention relates to a method of producing furfural and extracting lignin from a hemi-cellulosic biomass solution comprising a total quantity of C5 sugars, comprising the steps of heating the hemi-cellulosic biomass solution to a temperature of at least about 200°C; acidifying the hemi-cellulosic biomass solution with acid to produce the furfural in vapor phase; and condensing the furfural to recover furfural in solution, wherein the furfural is produced at a total molar yield of at least 70% of moles of furfural produced/the total moles C5 sugars present in the initial hemi-cellulosic biomass solution. Low molecular weight lignin can also be recovered from the hemi-cellulosic biomass solution prior to furfural production by membrane concentration, acidification, coagulation and filtration.
摘要翻译：本发明涉及从包含总量的C5糖的半纤维素生物质溶液中生产糠醛和提取木质素的方法，该方法包括以下步骤：将半纤维素生物质溶液加热至温度至少约200℃; 用酸酸化半纤维素生物质溶液以产生气相糠醛; 和冷凝糠醛以在溶液中回收糠醛，其中糠醛以至少70％产生的糠醛的摩尔数/最初半纤维素生物质溶液中存在的总C5摩尔糖的总摩尔产率产生。在通过膜浓缩，酸化，凝结和过滤来生产糠醛之前，还可以从半纤维素生物质溶液中回收低分子量木质素。

7. 发明申请

WO2018161164A1 PROCESS FOR PRODUCING CATIONIC LIGNIN COPOLYMER UNDER AQUEOUS ACID CONDITIONS 审中-公开
公开(公告)号：WO2018161164A1
公开(公告)日：2018-09-13
申请号：PCT/CA2018/050269
申请日：2018-03-07
申请人： FPINNOVATIONS , LAKEHEAD UNIVERSITY
发明人： FATEHI, Pedram , WANG, Shoujuan , PRICE, Jacquelyn , JEMAA, Naceur , MAHMOOD, Talat , PALEOLOGOU, Michael
IPC分类号： C08H7/00 , C02F1/56 , C02F11/14
摘要： A water-based process was developed for the synthesis of aminated lignin copolymers with high MW, thermal stability and solubility in water over a wide range of p H values. The cationic lignin copolymer described herein comprises: a grafting ratio of (weight of cationic amine compound) / (weight of lignin) of 70 to 200% and a charge density of +1.4-3.0 meq/g. This cationic lignin copolymer can be used as a flocculant in numerous wastewater streams including municipal and industrial systems and sludge dewatering in the pulp & paper, mining and oil industries.

8. 发明申请

WO2016168924A1 METHOD FOR RECOVERING AN ACID FROM ACID/SUGAR SOLUTIONS 审中-公开
标题翻译：从酸/糖解决方案中回收酸的方法
公开(公告)号：WO2016168924A1
公开(公告)日：2016-10-27
申请号：PCT/CA2016/050449
申请日：2016-04-20
申请人： FPINNOVATIONS
发明人： JEMAA, Naceur , PALEOLOGOU, Michael , MAHMOOD, Talat
IPC分类号： C13K1/04 , C01B17/90 , C01B25/234 , C01B7/07 , C07C51/47 , D21C11/00
CPC分类号： C13B20/146 , B01J41/04 , B01J41/13 , C01B17/905 , C07C51/47 , C13K1/02 , C13K13/002 , C07C55/10 , C07C53/02 , C07C59/08
摘要： Acid hydrolysis of biomass is an important step for releasing the component sugars before converting them to fuels and/or biochemicals. During such a process, a significant amount of mineral acid, such as sulfuric acid, is used. In most cases, the residual acid is neutralized with lime before the sugar conversion step. By doing so, a waste calcium sulphate stream is generated and sent to disposal. The efficient separation of acid from the sugars would allow the recycle of the acid and make the entire process more economically viable. We found that a resin bed packed with an acid retardation resin can be used to achieve an efficient separation (i.e. 98.5% recovery of the acid) of the sulfuric acid from the sugars. The resin bed can be simply regenerated with water.
摘要翻译：生物质的酸水解是将组分糖转化为燃料和/或生物化学物质之前释放组分糖的重要步骤。在这样的过程中，使用大量的无机酸，例如硫酸。在大多数情况下，在糖转化步骤之前，用石灰中和残留的酸。通过这样做，产生废硫酸钙流并将其送到处理中。酸与糖的有效分离将允许酸的再循环并使整个过程更经济地可行。我们发现可以使用填充有酸性延迟树脂的树脂床来实现糖的有效分离（即酸的98.5％回收）。树脂床可以简单地用水再生。

9. 发明申请

WO2014201555A1 METHOD FOR PRODUCING BIO-METHANOL AT PULP MILLS 审中-公开
标题翻译：用于生产PULP MILLS的生物甲醇的方法
公开(公告)号：WO2014201555A1
公开(公告)日：2014-12-24
申请号：PCT/CA2014/050559
申请日：2014-06-16
申请人： FPINNOVATIONS
发明人： JEMAA, Naceur , PALEOLOGOU, Michael
IPC分类号： C07C29/74 , C07C29/80 , D21C11/02 , C07C31/04 , C12P7/04
CPC分类号： C07C29/76 , B01D3/002 , B01D3/145 , B01D3/148 , B01D15/08 , B01D61/025 , B01D2311/2626 , B01D2311/2646 , B01D2311/2669 , B01D2311/2673 , C07C29/80 , D21C11/02 , C07C31/04
摘要： The present invention describes a process and system of producing methanol from methanol condensates. In a preferred embodiment the condensates are biomethanol condensates from chemical pulp mills and various waste sources used to produce a purified biomethanol. Pulp condensates are rich in methanol and contain many other contaminants. Presently, most chemical pulp mills, such as Kraft pulp mills use steam stripping to remove and concentrate the methanol and burn the methanol onsite along with the contaminants. A combination of treatments that include air stripping, steam stripping, distillation and reverse osmosis is described to obtain purified biomethanol suitable for sale or use on site.
摘要翻译：本发明描述了由甲醇缩合物生产甲醇的方法和系统。在优选的实施方案中，冷凝物是来自化学纸浆厂的生物甲醇缩合物和用于生产纯化的生物甲醇的各种废物来源。纸浆冷凝物富含甲醇并含有许多其他污染物。目前，大多数化学纸浆厂，如牛皮纸浆厂使用蒸汽汽提，去除和浓缩甲醇，并与污染物一起燃烧甲醇。描述了包括气提，汽提，蒸馏和反渗透的处理的组合，以获得适合在现场出售或使用的纯化生物甲醇。

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