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1. 发明申请

WO2009129325A3 HYDROGENOLYSIS PROCESSES AND HYDROGENOLYSIS CATALYST PREPARATION METHODS 审中-公开
标题翻译：氢化方法和氢化催化剂制备方法
公开(公告)号：WO2009129325A3
公开(公告)日：2010-03-18
申请号：PCT/US2009040695
申请日：2009-04-15
申请人： BATTELLE MEMORIAL INSTITUTE , HOLLADAY JOHNATHAN E , WHITE JAMES F , PETERSON THOMAS H , FRYE JOHN G , MUZATKO DANIELLE S , BARE SIMON R , VASSILAKIS JAMES G , ROSIN RICHARD R
发明人： HOLLADAY JOHNATHAN E , WHITE JAMES F , PETERSON THOMAS H , FRYE JOHN G , MUZATKO DANIELLE S , BARE SIMON R , VASSILAKIS JAMES G , ROSIN RICHARD R
IPC分类号： B01J21/18 , B01J23/889 , B01J23/89 , B01J37/18 , C07C17/23
CPC分类号： B01J21/18 , B01J23/8896 , B01J23/8986 , B01J37/18
摘要： Hydrogenolysis processes are provided that can include providing a hydrogenolysis reactor having a catalyst therein. The catalyst can be exposed to a reducing agent in the absence of polyhydric alcohol compound while maintaining a temperature of the catalyst above 290°C. Hydrogenolysis processes can also include providing a passivated catalyst to within a reactor and exposing the catalyst to a reducing atmosphere while maintaining the catalyst at a temperature less than 210°C. Hydrogenolysis catalyst preparation methods are provided that can include exposing the catalyst to a first reducing atmosphere while maintaining the catalyst at a first temperature to reduce at least a portion of the catalyst. The method can also include passivating at least the portion of the catalyst and depassivating the portion of the catalyst in the presence of a second reducing atmosphere while maintaining the portion of the catalyst at a second temperature less than the first temperature.
摘要翻译：提供氢解方法，其可以包括提供其中具有催化剂的氢解反应器。催化剂可以在不存在多元醇化合物的情况下暴露于还原剂，同时将催化剂的温度保持在290℃以上。氢解方法还可以包括在反应器内提供钝化的催化剂，并将催化剂暴露于还原气氛，同时将催化剂保持在低于210℃的温度。提供了氢解催化剂制备方法，其可以包括将催化剂暴露于第一还原气氛，同时将催化剂保持在第一温度以减少至少一部分催化剂。该方法还可以包括钝化至少一部分催化剂，并且在第二还原气氛存在的情况下使催化剂的一部分钝化，同时保持催化剂的部分在低于第一温度的第二温度。

2. 发明申请

WO2007146836B1 HYDROXYMETHYLFURFURAL REDUCTION METHODS AND METHODS OF PRODUCING FURANDIMETHANOL 审中-公开
标题翻译：羟丙基纤维素还原方法及其制备方法
公开(公告)号：WO2007146836B1
公开(公告)日：2008-03-06
申请号：PCT/US2007070802
申请日：2007-06-08
申请人： BATTELLE MEMORIAL INSTITUTE , LILGA MICHAEL A , HALLEN RICHARD T , WERPY TODD A , WHITE JAMES F , HOLLADAY JOHNATHAN E , FRYE JOHN G , ZACHER ALAN H
发明人： LILGA MICHAEL A , HALLEN RICHARD T , WERPY TODD A , WHITE JAMES F , HOLLADAY JOHNATHAN E , FRYE JOHN G , ZACHER ALAN H
IPC分类号： C07D307/12 , C07D307/40
CPC分类号： C07D307/12 , C07D307/40
摘要： A method of reducing hydroxymethylfurfural (HMF) where a starting material containing HMF in a solvent comprising water is provided. H 2 is provided into the reactor and the starting material is contacted with a catalyst containing at least one metal selected from Ni, Co, Cu, Pd, Pt, Ru, Ir, Re and Rh, at a temperature of less than or equal to 250°C. A method of hydrogenating HMF includes providing an aqueous solution containing HMF and fructose. H 2 and a hydrogenation catalyst are provided. The HMF is selectively hydrogenated relative to the fructose at a temperature at or above 30°C. A method of producing tetrahydofuran dimethanol (THFDM) includes providing a continuous flow reactor having first and second catalysts and providing a feed comprising HMF into the reactor. The feed is contacted with the first catalyst to produce furan dimethanol (FDM) which is contacted with the second catalyst to produce THFDM.
摘要翻译：提供一种还原羟甲基糠醛（HMF）的方法，其中含有HMF的原料在包含水的溶剂中。 H 2被提供到反应器中，起始材料与含有选自Ni，Co，Cu，Pd，Pt，Ru，Ir，Re和Rh中的至少一种金属的催化剂接触，温度小于或等于250℃。氢化HMF的方法包括提供含有HMF和果糖的水溶液。 H 2 H 2和氢化催化剂。在30℃或更高的温度下，HMF相对于果糖选择性氢化。制备四氢呋喃二甲醇（THFDM）的方法包括提供具有第一和第二催化剂的连续流动反应器，并向反应器中提供包含HMF的进料。进料与第一催化剂接触以产生与第二催化剂接触以产生THFDM的呋喃二甲醇（FDM）。

3. 发明申请

WO2011106048A3 PROCESSES AND SYSTEMS FOR THE PRODUCTION OF PROPYLENE GLYCOL FROM GLYCEROL 审中-公开
标题翻译：用于从甘油生产丙二醇的方法和系统
公开(公告)号：WO2011106048A3
公开(公告)日：2011-10-27
申请号：PCT/US2010057651
申请日：2010-11-22
申请人： BATTELLE MEMORIAL INSTITUTE , FRYE JOHN G , OBERG AARON A , ZACHER ALAN H
发明人： FRYE JOHN G , OBERG AARON A , ZACHER ALAN H
IPC分类号： C07C29/60 , C07C29/128 , C07C31/20
CPC分类号： C07C29/60 , C07C31/205
摘要： Processes and systems for converting glycerol to propylene glycol are disclosed. The glycerol feed is diluted with propylene glycol as the primary solvent, rather than water which is typically used. The diluted glycerol feed is sent to a reactor where the glycerol is converted to propylene glycol (as well as other byproducts) in the presence of a catalyst. The propylene glycol-containing product from the reactor is recycled as a solvent for the glycerol feed.
摘要翻译：公开了用于将甘油转化为丙二醇的方法和系统。用丙二醇作为主要溶剂稀释甘油进料，而不是通常使用的水。将稀释的甘油进料送入反应器，在该反应器中甘油在催化剂存在下转化为丙二醇（以及其它副产物）。来自反应器的含丙二醇的产物再循环作为甘油进料的溶剂。

4. 发明申请

WO2005105945A3 DEICING/ANTI-ICING FLUIDS 审中-公开
标题翻译：检测/防止流体
公开(公告)号：WO2005105945A3
公开(公告)日：2005-12-15
申请号：PCT/US2005014520
申请日：2005-04-28
申请人： BATTELLE MEMORIAL INSTITUTE , SAMUELS WILLIAM D , CONKLE NICHOLAS H , MONZYK BRUCE F , SIMMONS KEVIN L , FRYE JOHN G , WERPY TODD A , KUCZEK SARA F , CHAUHAN SATYA P
发明人： SAMUELS WILLIAM D , CONKLE NICHOLAS H , MONZYK BRUCE F , SIMMONS KEVIN L , FRYE JOHN G , WERPY TODD A , KUCZEK SARA F , CHAUHAN SATYA P
IPC分类号： C09K3/18
CPC分类号： C09K3/18 , C09K3/185
摘要： A nontoxic deicing/anti-icing fluid includes a freezing point depressant selected from short chain polyols having 3 to 5 carbons atoms, and mixtures thereof, a wetting agent, an antioxidant/preservative, and water. The fluid has an LD50 greater than about 10,000 mg/L. Another deicing/anti-icing fluid includes the freezing point depressant, a vinylpyrrolidone polymer having a molecular weight between about 10,000 and about 700,000, and water. A runway deicing fluid includes glycerol, a buffer, an antioxidant/preservative, and water. Another deicing/anti-icing fluid includes a freezing point depressant having hydrophobic character, a wetting agent comprising an organophosphorus compound capable of producing an organic wettable surface, and water.
摘要翻译：无毒除冰/防冰液体包括选自具有3至5个碳原子的短链多元醇及其混合物，润湿剂，抗氧化剂/防腐剂和水的凝固点抑制剂。流体的LD50大于约10,000 mg / L。另一种除冰/防冰液体包括冰点抑制剂，分子量介于约10,000至约700,000之间的乙烯基吡咯烷酮聚合物和水。跑道除冰液包括甘油，缓冲剂，抗氧化剂/防腐剂和水。另一种除冰/防冰流体包括具有疏水性的凝固点抑制剂，包含能够产生有机可湿性表面的有机磷化合物的润湿剂和水。

5. 发明申请

WO2004039910A3 BIOBASED DEICING/ANTI-ICING FLUIDS 审中-公开
标题翻译：生物检测/抗流感液体
公开(公告)号：WO2004039910A3
公开(公告)日：2004-10-21
申请号：PCT/US0334181
申请日：2003-10-28
申请人： BATTELLE MEMORIAL INSTITUTE
发明人： SIMMONS KEVIN L , FRYE JOHN G , WERPY TODD A , SAMUELS WILLIAM D , CONKLE H NICHOLAS , KUCZEK SARA F
IPC分类号： C09K3/18
CPC分类号： C09K3/185 , C09K3/18
摘要： A nontoxic deicing/anti-icing fluid includes a biobased freezing point depressant, a surfactant, an antioxidant, and water. The fluid has an LD50 greater than about 10,000 mg/L. Another deicing/anti-icing fluid includes a biobased freezing point depressant, a vinylpyrrolidone polymer having a molecular weight between about 10,000 and about 700,000, and water. Another deicing/anti-icing fluid includes a biobased freezing point depressant, a nonionic surfactant selected from the polyoxyalkylene ethers, an antioxidant, and water. Another deicing/anti-icing fluid includes a biobased freezing point depressant, a surfactant, a food grade material that functions as an antioxidant, and water. A further deicing/anti-icing fluid includes a biobased freezing point depressant, a material that functions as both a buffer and a freezing point depressant, and water.
摘要翻译：无毒除冰/防冰液体包括生物基冰点抑制剂，表面活性剂，抗氧化剂和水。流体的LD50大于约10,000 mg / L。另一种除冰/防冰液体包括生物基冰点抑制剂，分子量约为10,000至约700,000的乙烯基吡咯烷酮聚合物和水。另一种除冰/防冰液体包括生物基冰点抑制剂，选自聚氧化烯醚，抗氧化剂和水的非离子表面活性剂。另一种除冰/防冰液体包括生物基冰点抑制剂，表面活性剂，起抗氧化剂作用的食品级材料和水。另外的除冰/防冰液体包括生物基凝固点抑制剂，作为缓冲剂和凝固点抑制剂两者的材料以及水。

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