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1. 发明申请

WO2020108482A1 MECHANOCHEMICAL ACTIVATION IN SOLVENT-FREE ZEOLITE SYNTHESIS 审中-公开
公开(公告)号：WO2020108482A1
公开(公告)日：2020-06-04
申请号：PCT/CN2019/120954
申请日：2019-11-26
申请人： BASF SE , BASF (CHINA) COMPANY LIMITED
发明人： WINKELMANN, Marion , LUZ, Andreas , PARVULESCU, Andrei-Nicolae , ROMANI FERNANDEZ, Xiana , MUELLER, Ulrich , KLEINE JAEGER, Frank , MUELLER, Frank , NETSCHER, Michael , TAUBER, Ralph , STREBEL, Frank , ROLLAR, Dieter , MAURER, Stefan , DAI, Yu
IPC分类号： C01B39/04 , B01J29/06
摘要： Provided is a process for the preparation of a zeolitic material comprising YO 2 and X 2 O 3 in its framework structure, wherein Y stands for a tetravalent element and X stands for a trivalent element, wherein the process comprises:(i) preparing a mixture comprising one or more sources of YO 2 , one or more sources of X 2 O 3 , and H 2 O; (ii) grinding and/or mixing the mixture prepared in (i), wherein the energy intake of the mixture during the grinding and/or mixing procedure is in the range of from 0.3 to 200 kJ/kg of the mixture; (iii) heating the mixture obtained in (ii) at a temperature in the range of from 80 to 300 ℃ for crystallizing a zeolitic material comprising YO 2 and X 2 O 3 in its framework structure from the mixture; wherein the mixture prepared in (i) contains from 5 to 200 wt.% of H 2 O based on 100 wt.% of the one or more sources of YO 2 , calculated as YO 2 , contained in the mixture prepared in (i) and heated in (iii). Furthermore, a zeolitic material comprising YO 2 and X 2 O 3 in its framework structure as obtainable and/or obtained according to the process as well as the use of the material are provided.

2. 发明申请

WO2015185633A1 SYNTHESIS OF A BORON-CONTAINING ZEOLITE WITH AN MWW FRAMEWORK STRUCTURE 审中-公开
标题翻译：具有MWW框架结构的含硼硼沸石的合成
公开(公告)号：WO2015185633A1
公开(公告)日：2015-12-10
申请号：PCT/EP2015/062385
申请日：2015-06-03
申请人： BASF SE
发明人： MAURER, Stefan , PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , XIAO, Feng-Shou , MENG, Xiangju , WU, Yeqing
IPC分类号： C01B39/12 , C01B39/48
CPC分类号： C01B39/48 , B01D15/361 , B01D53/86 , B01D2255/50 , B01J20/18 , B01J29/86 , C01B39/12
摘要： The present invention relates to a process for the production of a boron-containing zeolitic material having an MWW framework structure comprising YO2 and B 2 O 3 , wherein Y stands for a tetravalent element, wherein said process comprises (a) providing a mixture comprising one or more sources for YO 2 , one or more sources for B 2 O 3 , one or more organotemplates, and seed crystals, (b) crystallizing the mixture obtained in (a) for obtaining a layered precursor of the boron-containing MWW-type zeolitic material, (c) calcining the layered precursor obtained in (b) for obtaining the boron-containing zeolitic material having an MWW framework structure, wherein the one or more organotemplates have the formula (I) R 1 R 2 R 3 N (I) wherein R 1 is (C 5 -C 8 ) cycloalkyl, and wherein R 2 and R 3 are independently from each other H or alkyl, as well as to a synthetic boron-containing zeolite which is obtainable and/or obtained according to the inventive process as well as to its use.
摘要翻译：本发明涉及一种生产具有包含YO 2和B 2 O 3的MWW骨架结构的含硼沸石材料的方法，其中Y代表四价元素，其中所述方法包括（a）提供包含一种或多种来源的混合物对于YO 2，一种或多种B 2 O 3，一种或多种有机模板和晶种的来源，（b）使（a）中获得的混合物结晶以获得含硼MWW型沸石材料的层状前体，（c）煅烧（b）中获得的用于获得具有MWW骨架结构的含硼沸石材料的层状前体，其中所述一种或多种有机模板具有式（I）其中R 1是（C 5 -C 8）环烷基的R 1 R 2 R 3 N（I），其中 R2和R3彼此独立地为H或烷基，以及根据本发明方法可获得和/或获得的合成含硼沸石以及其用途。

3. 发明申请

WO2015101930A1 BIMETAL-EXCHANGED ZEOLITE BETA FROM ORGANOTEMPLATE-FREE SYNTHESIS AND USE THEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOX 审中-公开
标题翻译：无机合成的双官能交换沸石和在选择性催化还原NOX中的用途
公开(公告)号：WO2015101930A1
公开(公告)日：2015-07-09
申请号：PCT/IB2014/067413
申请日：2014-12-30
申请人： BASF SE , TOKYO INSTITUTE OF TECHNOLOGY , BASF (CHINA) COMPANY LIMITED
发明人： FEYEN, Mathias , MAURER, Stefan , MÜLLER, Ulrich , BAO, Xinhe , ZHANG, Weiping , DE VOS, Dirk , GIES, Hermann , XIAO, Feng-Shou , TOSHIYUKI, Yokoi , YILMAZ, Bilge
IPC分类号： C01B39/00 , B01J29/00
CPC分类号： B01D53/9418 , B01D2255/20738 , B01D2255/20761 , B01D2255/502 , B01J29/7615 , B01J37/0203 , B01J37/04 , B01J37/30 , B01J2229/183 , B01J2229/186 , B01J2229/34 , C01B39/026 , C01B39/46
摘要： The present invention relates to a process for the production of a zeolitic material having a BEA-type framework structure comprising YO 2 and X2O 3 , wherein said process comprises the steps of (1)preparing a mixture comprising one or more sources for YO 2 and one or more sources for X 2 O 3 ; (2)crystallizing the mixture obtained in step (1); (3)subjecting the zeolitic material having a BEA-type framework structure obtained in step (2) to an ion-exchange procedure with Cu; and (4) subjecting the Cu ion-exchanged zeolitic material obtained in step (3) to an ion-exchange procedure with Fe; wherein Y is a tetravalent element, and X is a trivalent element, wherein the mixture provided in step (1) and crystallized in step (2) further comprises seed crystals comprising one or more zeolitic materials having a BEA-type framework structure, and wherein the mixture provided in step (1) and crystallized in step (2) does not contain an organotemplate as a structure-directing agent, as well as to the zeolitic material having a BEA framework structure per se, and to its use, in particular in a method for the treatment of NO x by selective catalytic reduction (SCR).
摘要翻译：本发明涉及生产具有包含YO 2和X 2 O 3的BEA型骨架结构的沸石材料的方法，其中所述方法包括以下步骤：（1）制备包含一种或多种YO 2和一种或多种源的混合物 X2O3的来源; （2）使步骤（1）中获得的混合物结晶; （3）将具有步骤（2）中获得的BEA型骨架结构的沸石材料与Cu进行离子交换程序; 和（4）使步骤（3）中获得的Cu离子交换的沸石材料与Fe的离子交换程序; 其中Y是四价元素，X是三价元素，其中在步骤（1）中提供并在步骤（2）中结晶的混合物还包含包含一种或多种具有BEA型骨架结构的沸石材料的晶种，其中步骤（1）中提供并在步骤（2）中结晶的混合物不含作为结构导向剂的有机模板，以及本身具有BEA骨架结构的沸石材料，特别是其用途通过选择性催化还原（SCR）处理NOx的方法。

4. 发明申请

WO2012143878A1 SHAPED BODY CONTAINING POROUS AROMATIC FRAMEWORK (PAF) MATERIAL 审中-公开
标题翻译：包含多孔芳香纤维（PAF）材料的成型体
公开(公告)号：WO2012143878A1
公开(公告)日：2012-10-26
申请号：PCT/IB2012/051966
申请日：2012-04-19
申请人： BASF SE , GAAB, Manuela , MAURER, Stefan , KRAHNERT, Wolf-Rüdiger , KOSTUR, Milan , MÜLLER, Ulrich , GOKHALE, Ranjit , HINDALEKAR, Shrirang, Bhikaji , BASF (CHINA) COMPANY LIMITED
发明人： GAAB, Manuela , MAURER, Stefan , KRAHNERT, Wolf-Rüdiger , KOSTUR, Milan , MÜLLER, Ulrich , GOKHALE, Ranjit , HINDALEKAR, Shrirang, Bhikaji
IPC分类号： B01J20/26 , C08K3/22 , C08K3/34
CPC分类号： B01J20/267 , B01D53/02 , B01D53/047 , B01D2253/202 , B01D2253/34 , B01D2257/108 , B01D2257/504 , B01D2257/7025 , B01D2259/4525 , B01J20/226 , B01J20/28004 , B01J20/2803 , B01J20/28042 , B01J20/28059 , B01J20/3007 , B01J20/3042 , C01B3/0015 , C08G61/02 , C08G61/10 , C08G61/12 , C08G2261/3142 , C08G2261/3221 , C08G2261/3328 , C08G2261/3424 , C08G2261/344 , C08L65/00 , Y02C10/08 , Y02C20/20 , Y02E60/328 , Y02P20/152 , Y02P20/156 , C08L1/28
摘要： The present invention relates to shaped bodies of compositions comprising a porous aromatic covalent framework polymer, wherein the polymer comprises at least one monomer unit, the at least one monomer unit comprising at least one aromatic ring and the at least one monomer unit having at least three binding sites to adjacent monomer units in the polymer and a core, wherein the at least three binding sites are located on at least one atom of the core and wherein the at least one atom is free of covalent bonds to hydrogen; and at least one binder additive. The invention also relates to methods for the preparation of said shaped bodies and their uses.
摘要翻译：本发明涉及包含多孔芳族共价骨架聚合物的成型体组合物，其中所述聚合物包含至少一个单体单元，所述至少一个单体单元包含至少一个芳香环和至少一个单体单元，其具有至少三个与所述聚合物中的相邻单体单元的结合位点和核心，其中所述至少三个结合位点位于所述核心的至少一个原子上，并且其中所述至少一个原子与氢没有共价键; 和至少一种粘合剂添加剂。本发明还涉及制备所述成形体及其用途的方法。

5. 发明申请

WO2018167143A1 PROCESS FOR PREPARING A CYCLIC DIESTER OR A CYCLIC DIAMIDE BY REACTING A HYDROXYCARBOXYLIC ACID OR AMIDE WITH AN ACIDIC BEA-TYPE (H-BETA POLYMORPH A) ZEOLITE 审中-公开
公开(公告)号：WO2018167143A1
公开(公告)日：2018-09-20
申请号：PCT/EP2018/056382
申请日：2018-03-14
申请人： BASF SE
发明人： GORDILLO, Alvaro , PARVULESCU, Andrei-Nicolae , SANTOS RIBEIRO, Henelyta , ROTHER, Jörg , JEVTOVIKJ, Ivana , MÜLLER, Ulrich , MAURER, Stefan
IPC分类号： C07D319/12
摘要： A process for preparing a cyclic diester or a cyclic diamide by reacting a hydroxycarboxylic acid or amide with an acidic BEA (H-beta polymorph A) type zeolite. The process is characterised in that the total amount of acid sites is in the range of from 0.25 to 1.0 mmol/g and the amount of medium acid sites is at least 40% of the total amount of acid sites. The total amount of acid sites and the amount of medium acid sites are determined by NH3-TPD (temperature-programmed desorption of ammonia). Preferably, the process refers to the preparation of lactide from lactic acid. The framework structure of the zeolitic material comprises Si, Al, O, and H.

6. 发明申请

WO2015144695A1 POROUS FILMS COMPRISING METAL-ORGANIC FRAMEWORK MATERIALS 审中-公开
标题翻译：包含金属有机框架材料的多孔膜
公开(公告)号：WO2015144695A1
公开(公告)日：2015-10-01
申请号：PCT/EP2015/056242
申请日：2015-03-24
申请人： BASF SE
发明人： SCHWAB, Matthias Georg , MAURER, Stefan , BARTULI, Waldemar , MUELLER, Ulrich
IPC分类号： B01J20/26 , B01J31/16 , C08F14/18 , C08J5/18 , C08J9/00 , C08K5/56 , C08K7/02
CPC分类号： B01J20/226 , B01J20/261 , B01J20/264 , B01J20/28033 , B01J20/28057 , B01J20/28059 , B01J31/1691 , B01J2220/44
摘要： The present invention relates to porous films comprising (A) from 51 wt.-% to 99.9 wt.-% based on the total weight of the film of at least one porous metal-organic framework material, the material comprising at least one at least bidentate organic compound coordinated to at least one metal ion; (B) from 0.1 wt.-% to 49 wt.-% based on the total weight of the film of at least one fibrillated fluoropolymer; and (C) 0 wt.-% to 48.9 wt.-% based on the total weight of the film of an additive component. The invention further relates to a composition for preparing such a film and its use.
摘要翻译：本发明涉及多孔膜，其包含（A）基于至少一种多孔金属 - 有机骨架材料的膜的总重量的51重量％至99.9重量％，该材料至少包括至少一个与至少一种金属离子配位的二齿有机化合物; （B）为0.1重量％至49重量％，基于至少一个原纤化含氟聚合物的膜的总重量; 和（C）0重量％至48.9重量％，基于添加剂组分的膜的总重量。本发明还涉及一种用于制备这种膜的组合物及其用途。

7. 发明申请

WO2015083113A1 METHOD AND USE FOR THE TERTIARY MINERAL OIL PRODUCTION BY MEANS OF METAL-ORGANIC FRAMEWORK MATERIALS 审中-公开
标题翻译：方法和使用金属有机框架材料的初步矿物油生产
公开(公告)号：WO2015083113A1
公开(公告)日：2015-06-11
申请号：PCT/IB2014/066586
申请日：2014-12-04
申请人： BASF SE , BASF CHINA COMPANY LIMITED
发明人： MAURER, Stefan , KIMURA, Riichiro , PARVULESCU, Andrei-Nicolae , REINHARDT, Caroline , SIGGEL, Lorenz , MÜLLER, Ulrich
IPC分类号： C09K8/58 , C07D233/58
CPC分类号： C07D233/58 , C09K8/58
摘要： The invention relates to a method for tertiary mineral oil production, in which an aqueous suspension, comprising at least one porous metal-organic framework material,is injected through at least one injection borehole into a mineral oil deposit, and crude oil is withdrawn from the deposit through at least one production borehole. The invention further relates to the use of an aqueous suspension, comprising at least one porous metal-organic framework material. The invention further relates to the use of at least one porous metal-organic framework material or an aqueous suspension for tertiary mineral production.
摘要翻译：本发明涉及一种用于三次矿物油生产的方法，其中包含至少一种多孔金属 - 有机骨架材料的水性悬浮液通过至少一个注入孔注入矿物油沉积物中，并将原油从通过至少一个生产井眼沉积。本发明还涉及包含至少一种多孔金属 - 有机骨架材料的水性悬浮液的用途。本发明还涉及至少一种多孔金属 - 有机骨架材料或水性悬浮液用于三次矿物生产的用途。

8. 发明申请

WO2015025250A1 METHOD FOR UPTAKING A SPILLED LIQUID 审中-公开
标题翻译：一种溢出液体的方法
公开(公告)号：WO2015025250A1
公开(公告)日：2015-02-26
申请号：PCT/IB2014/063911
申请日：2014-08-14
申请人： BASF SE , BASF CHINA COMPANY LIMITED
发明人： MAURER, Stefan , KIMURA, Riichiro , PARVULESCU, Andrei-Nicolae , PETRY, Julia , SIGGEL, Lorenz , MÜLLER, Ulrich
IPC分类号： C02F1/28 , B01J20/26 , B01D15/00
CPC分类号： B01J20/28042 , B01J20/226 , C02F1/285 , C02F1/40 , C02F2101/32 , C02F2103/365
摘要： The present invention relates to a method for at least partly uptaking a spilled liquid comprising at least one liquid hydrocarbon, the method comprising the step of contacting the at least one liquid hydrocarbon with a binder agent comprising at least one porous metal-organic framework material, wherein the at least one metal-organic framework material comprises at least one organic compound coordinated to at least one metal ion, wherein the at least one organic com- pound is based on imidazole, which is unsubstituted or substituted with one or more substituents independently selected from the group consisting of C 1-6 alkyl, phenyl and benzyl. The invention further relates to the use of such a binder agent for at least partly uptaking the liquid.
摘要翻译：本发明涉及至少部分吸收包含至少一种液体烃的溢出液体的方法，该方法包括使至少一种液态烃与包含至少一种多孔金属 - 有机骨架材料的粘合剂接触的步骤，其中所述至少一种金属 - 有机骨架材料包含与至少一种金属离子配位的至少一种有机化合物，其中所述至少一种有机化合物是基于咪唑，其是未取代的或被一个或多个独立选择的取代基取代的取代基由C1-6烷基，苯基和苄基组成。本发明还涉及这种粘合剂用于至少部分吸收液体的用途。

9. 发明申请

WO2014060259A1 POST-TREATMENT OF DEBORONATED ZEOLITE BETA 审中-公开
标题翻译：脱硼沸石BET的后处理
公开(公告)号：WO2014060259A1
公开(公告)日：2014-04-24
申请号：PCT/EP2013/071040
申请日：2013-10-09
申请人： BASF SE
发明人： PARVULESCU, Andrei-Nicolae , YANG, Jeff , MAURER, Stefan , GAAB, Manuela , SEIDEL, Karsten , GERLACH, Olga , MÜLLER, Ulrich
IPC分类号： C01B39/02 , B01J21/00
CPC分类号： C01B39/026 , B01J29/7007 , B01J35/1014 , B01J2229/38 , C01B39/46
摘要： A process for the post-treatment of a zeolitic material having a BEA framework structure, the process comprising (i) providing a zeolitic material having a BEA framework structure, wherein the framework structure of the zeolitic material comprises X 2 O 3 and YO 2 , wherein Y is a tetravalent element and X is a trivalent element and wherein the molar ratio X 2 O 3 : YO 2 is greater than 0.02 : 1; (ii) treating the zeolitic material provided in (i) with a liquid solvent system thereby obtaining a zeolitic material having a molar ratio X 2 O 3 : YO 2 of at most 0.02 : 1, and at least partially separating the zeolitic material from the liquid solvent system; (iii) treating the zeolitic material obtained from (ii) with a liquid aqueous system having a pH in the range of 5.5 to 8 and a temperature of at least 75 °C.
摘要翻译：一种用于后处理具有BEA骨架结构的沸石材料的方法，该方法包括（i）提供具有BEA骨架结构的沸石材料，其中沸石材料的骨架结构包含X 2 O 3和YO 2，其中Y是四价元素，X是三价元素，其中X 2 O 3 :YO 2的摩尔比大于0.02:1; （ii）用液体溶剂系统处理（i）中提供的沸石材料，从而获得摩尔比X2O3：YO2至多0.02:1的沸石材料，并至少部分地将沸石材料与液体溶剂系统分离; （iii）用pH为5.5〜8，温度为至少75℃的液态水系统处理由（ⅱ）得到的沸石材料。

10. 发明申请

WO2013118064A1 PROCESS AND APPARATUS FOR TREATMENT OF GAS STREAMS CONTAINING NITROGEN OXIDES 审中-公开
标题翻译：用于处理含有氮氧化物的气体流的方法和装置
公开(公告)号：WO2013118064A1
公开(公告)日：2013-08-15
申请号：PCT/IB2013/050985
申请日：2013-02-06
申请人： BASF SE , BASF (CHINA) COMPANY LIMITED , BASF SCHWEIZ AG
发明人： DEUERLEIN, Stephan , MAURER, Stefan
IPC分类号： C01B39/06 , B01J29/06
CPC分类号： B01D53/9413 , B01D53/8628 , B01D53/9418 , B01D53/9427 , B01D2251/202 , B01D2251/204 , B01D2251/208 , B01D2255/502 , B01D2257/402 , B01D2257/404 , B01D2258/0283 , B01J29/7007 , B01J29/7615 , B01J35/002 , B01J37/06 , C01B39/46 , Y02C20/10 , Y02P20/153
摘要： The present invention relates to a process for the treatment of a gas stream containing nitrogen oxides comprising the steps of: (1) providing a gas stream containing one or more nitrogen oxides; (2) contacting the gas stream provided in step (1) with a transition metal containing zeolitic material having a BEA-type framework structure for reacting one or more of the nitrogen oxides; wherein the zeolitic material is obtainable from an organotemplate-free synthetic process, as well as to an apparatus for the treatment of a gas stream comprising containing nitrogen oxides.
摘要翻译：本发明涉及一种处理含有氮氧化物的气流的方法，包括以下步骤：（1）提供含有一种或多种氮氧化物的气流; （2）使步骤（1）中提供的气流与含有BEA型骨架结构的含过渡金属的沸石材料接触，使一种或多种氮氧化物反应; 其中所述沸石材料可从无有机模板的合成方法获得，以及用于处理包含氮氧化物的气流的装置。

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