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1. 发明申请

WO2018167143A1 PROCESS FOR PREPARING A CYCLIC DIESTER OR A CYCLIC DIAMIDE BY REACTING A HYDROXYCARBOXYLIC ACID OR AMIDE WITH AN ACIDIC BEA-TYPE (H-BETA POLYMORPH A) ZEOLITE 审中-公开
公开(公告)号：WO2018167143A1
公开(公告)日：2018-09-20
申请号：PCT/EP2018/056382
申请日：2018-03-14
申请人： BASF SE
发明人： GORDILLO, Alvaro , PARVULESCU, Andrei-Nicolae , SANTOS RIBEIRO, Henelyta , ROTHER, Jörg , JEVTOVIKJ, Ivana , MÜLLER, Ulrich , MAURER, Stefan
IPC分类号： C07D319/12
摘要： A process for preparing a cyclic diester or a cyclic diamide by reacting a hydroxycarboxylic acid or amide with an acidic BEA (H-beta polymorph A) type zeolite. The process is characterised in that the total amount of acid sites is in the range of from 0.25 to 1.0 mmol/g and the amount of medium acid sites is at least 40% of the total amount of acid sites. The total amount of acid sites and the amount of medium acid sites are determined by NH3-TPD (temperature-programmed desorption of ammonia). Preferably, the process refers to the preparation of lactide from lactic acid. The framework structure of the zeolitic material comprises Si, Al, O, and H.

2. 发明申请

WO2018108875A1 A PROCESS FOR THE PREPARATION OF A TITANIUM-CONTAINING ZEOLITE 审中-公开
公开(公告)号：WO2018108875A1
公开(公告)日：2018-06-21
申请号：PCT/EP2017/082366
申请日：2017-12-12
申请人： BASF SE
发明人： PARVULESCU, Andrei-Nicolae , MÜLLER, Ulrich , VOGELSANG, Regina , BRUNS, Nicole Sabine , WEIDERT, Jan-Oliver
IPC分类号： B01J29/86 , C01B37/00 , C01B39/02 , C01B39/12
摘要： A process comprising hydrothermally synthesizing a titanium-containing zeolitic material having framework type MWW in the presence of an MWW template compound, obtaining a mother liquor comprising water, a first portion of the MWW template compound and a titanium-containing zeolitic material having framework type MWW comprising a second portion of the MWW template compound, separating the first portion of the MWW template compound from the mother liquor and recycling the first portion of the MWW template compound into a hydrothermal synthesis of a titanium-containing zeolitic material having framework type MWW.

3. 发明申请

WO2017140774A1 A PROCESS FOR THE PREPARATION OF PROPYLENE OXIDE 审中-公开
标题翻译：一种制备环氧丙烷的方法
公开(公告)号：WO2017140774A1
公开(公告)日：2017-08-24
申请号：PCT/EP2017/053492
申请日：2017-02-16
申请人： BASF SE
发明人： RIEDEL, Dominic , TELES, Joaquim H. , SCHELLING, Heiner , WEGERLE, Ulrike , MÜLLER, Ulrich , PARVULESCU, Andrei-Nicolae , MANNWEILER, Jochen , HENN, Timo , LÜDERITZ, Thomas , WÖRZ, Nicolai Tonio , MÜLLER, Christian , WEBER, Markus , URBANCZYK, Daniel
IPC分类号： C07D301/12 , C07D301/36
CPC分类号： C07D301/12 , C07D301/36
摘要： A continuous process for the preparation of propylene oxide, comprising a start-up stage and normal run stage, wherein the normal run stage comprises (i) continuously providing a liquid feed stream comprising propene, hydrogen peroxide, acetonitrile, a formate salt, water and optionally propane, wherein in the liquid feed stream, the molar amount of the formate salt relative to the molar amount of hydrogen peroxide at a given point of time during the normal run stage is a N (Fo/H 2 O 2 ); (ii) continuously passing the liquid feed stream provided in (i) into an epoxidation zone comprising a catalyst comprising a titanium zeolite having framework type MWW, and subjecting the liquid feed stream to epoxidation reaction conditions in the epoxidation zone, obtaining a reaction mixture comprising propylene oxide, acetonitrile, water, the formate salt, optionally propene, and optionally propane; (iii) continuously removing an effluent stream from the epoxidation zone, the effluent stream comprising propylene oxide, acetonitrile, water, at least a portion of the formate salt, optionally propene, and optionally propane; wherein the normal run stage is characterized in an average rate of change of a N (Fo/H 2 O 2 ) of less than 0 h -1 .
摘要翻译：一种用于制备环氧丙烷的连续方法，其包括启动阶段和正常运行阶段，其中正常运行阶段包括（i）连续提供包含丙烯，过氧化氢，乙腈，甲酸盐，水和任选的丙烷，其中在液体进料流中，相对于在正常运行阶段期间的给定时间点的过氧化氢的摩尔量，甲酸盐的摩尔量是N （F0 / H <子> 2 0 <子> 2 ）; （ii）将（i）中提供的液体进料流连续通入包含催化剂的环氧化区中，所述催化剂包含具有骨架型MWW的钛沸石，并使液体进料流在环氧化区中经受环氧化反应条件，获得反应混合物，所述反应混合物包含环氧丙烷，乙腈，水，甲酸盐，任选的丙烯和任选的丙烷; （iii）连续地从环氧化区中除去流出物流，所述流出物流包含环氧丙烷，乙腈，水，至少一部分甲酸盐，任选的丙烯和任选的丙烷; 其中所述正常运行阶段的特征在于小于0小时的αN（Fo / H2θO 2）的平均变化率 ^-1

4. 发明申请

WO2017097835A1 A TIN-CONTAINING ZEOLITIC MATERIAL HAVING A BEA FRAMEWORK STRUCTURE 审中-公开
标题翻译：具有BEA框架结构的含锡锆钛酸盐材料
公开(公告)号：WO2017097835A1
公开(公告)日：2017-06-15
申请号：PCT/EP2016/080076
申请日：2016-12-07
申请人： BASF SE
发明人： PARVULESCU, Andrei-Nicolae , TELES, Joaquim Henrique , VAUTRAVERS, Nicolas , MÜLLER, Ulrich
IPC分类号： C01B37/02 , C01B39/08 , C01B39/12 , C01B39/48 , C07C67/00
CPC分类号： C01B39/08 , C01B37/02 , C01B39/12 , C01B39/48 , C07C51/00 , C07C67/00 , C07D313/04 , C07F5/02 , C07F7/22 , C07C59/08
摘要： A process for preparing a tin-containing zeolitic material having framework type BEA, comprising providing an aqueous synthesis mixture comprising a boron source, a silicon source, and a BEA structure directing agent; subjecting the synthesis mixture provided in to hydrothermal pre-crystallization conditions; adding the tin source to the obtained mixture; subjecting the obtained aqueous synthesis mixture to hydrothermal crystallization conditions, obtaining a tin-containing zeolitic material having framework type BEA comprised in its mother liquor.
摘要翻译：一种制备具有骨架型BEA的含锡沸石材料的方法，包括提供包含硼源，硅源和BEA结构导向剂的含水合成混合物; 对提供的合成混合物进行水热预结晶条件; 将锡源加入到所得混合物中; 将得到的含水合成混合物进行水热结晶条件，得到在其母液中含有骨架类型BEA的含锡沸石材料。

5. 发明申请

WO2016075136A1 A STORAGE VESSEL COMPRISING A ONE-PIECE SHAPED BODY OF A POROUS SOLID 审中-公开
标题翻译：包含多孔固体的单层成形体的储存容器
公开(公告)号：WO2016075136A1
公开(公告)日：2016-05-19
申请号：PCT/EP2015/076204
申请日：2015-11-10
申请人： BASF SE
发明人： WEICKERT, Mathias , MARX, Stefan , MÜLLER, Ulrich , ARNOLD, Lena , LACK, Adam , LYNCH, Joseph , DOLAN, William , SANTAMARIA, Michael
IPC分类号： F17C11/00 , B01J20/22 , B01J20/28
CPC分类号： F17C11/007 , B01J20/226 , B01J20/2803 , B01J20/28042 , B01J20/28045 , B01J20/28095 , B01J20/3007 , B01J20/3042 , F17C11/002 , F17C11/005 , F17C2201/0119 , F17C2221/011 , F17C2221/012 , F17C2221/013 , F17C2221/014 , F17C2221/017 , F17C2221/018 , F17C2221/033 , F17C2221/035 , F17C2270/0105 , F17C2270/0171 , F17C2270/0178 , F17C2270/0189 , Y02C10/08 , Y02E60/321
摘要： The invention is related to a storage vessel (1) comprising a shaped body (3) of a porous solid, wherein the storage vessel (1) comprises a wall (5) with a section (7) comprising at least one inlet (9), wherein the storage vessel (1) has a central axis (11) and the central axis (11) is a longitudinal axis of the storage vessel (1) and/or perpendicular to a cross-sectional area of the at least one inlet (9), wherein the shaped body (3) covers at least 85 % of an inner volume (13) of the storage vessel (1) and the shaped body (3) comprises an opening (19) in an axial direction (17), axial referring to the central axis (11) of the storage vessel (1), wherein the opening (19) extends from a first end (21) of the shaped body (3) to an opposing second end (23) of the shaped body (3) and wherein the storage vessel (1) comprises exactly one shaped body (3), which is formed in one piece. The invention is further related to a shaped body and use of the shaped body.
摘要翻译：本发明涉及一种包括多孔固体的成型体（3）的储存容器（1），其中所述储存容器（1）包括具有部分（7）的壁（5），所述部分（7）包括至少一个入口（9），其中所述储存容器（1）具有中心轴线（11），并且所述中心轴线（11）是所述储存容器（1）的纵向轴线和/或垂直于所述至少一个入口的横截面积（ 9），其中成形体（3）覆盖储存容器（1）的内部体积（13）的至少85％，并且成形体（3）在轴向方向（17）上包括开口（19）轴向地指存储容器（1）的中心轴线（11），其中开口（19）从成形体（3）的第一端（21）延伸到成形体的相对的第二端（23）（3），并且其中所述储存容器（1）包括一个形成为一体的正好一个成形体（3）。本发明还涉及成形体和成形体的用途。

6. 发明申请

WO2015185625A2 CHA TYPE ZEOLITIC MATERIALS AND METHODS FOR THEIR PREPARATION USING COMBINATIONS OF CYCLOALKYL- AND TETRAALKYLAMMONIUM COMPOUNDS 审中-公开
标题翻译： CHA类型的ZEOLITIC材料及其使用环己基 - 和四氨基亚甲基化合物的组合制备方法
公开(公告)号：WO2015185625A2
公开(公告)日：2015-12-10
申请号：PCT/EP2015/062377
申请日：2015-06-03
申请人： BASF SE
发明人： FEYEN, Mathias , YANG, Jeff , RUETZ, Roger , MÜLLER, Ulrich
IPC分类号： C01B39/48
CPC分类号： C01B39/48 , B01J20/18 , B01J20/3057 , B01J20/3085 , B01J29/7015 , B01J29/763 , B01J35/002 , B01J35/023 , B01J37/0018 , B01J37/0246 , B01J39/02 , B01J39/14 , B01J2229/186 , B01J2229/42
摘要： The present invention relates to a process for the preparation of a zeolitic material having a CHA-type framework structure comprising YO 2 and X 2 O 3 , wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO 2 , one or more sources for X 2 O 3 , one or more tetraalkylammonium cation R 1 R 2 R 3 R 4 N + -containing compounds, and one or more tetraalkylammonium cation R 5 R 6 R 7 R 8 N + -containing compounds as structure directing agent; (2) crystallizing the mixture obtained in step (1) for obtaining a zeolitic material having a CHA-type framework structure; wherein Y is a tetravalent element and X is a trivalent element, wherein R 1 , R 2 , R 3 , R 4 , R 5 , R 6 , and R 7 independently from one another stand for alkyl, and wherein R 8 stands for cycloalkyl, as well as to zeolitic materials which may be obtained according to the inventive process and to their use.
摘要翻译：本发明涉及一种制备具有包含YO 2和X 2 O 3的CHA型骨架结构的沸石材料的方法，其中所述方法包括以下步骤：（1）提供包含一种或多种YO 2，更多的X2O3，一种或多种四烷基铵阳离子R1R2R3R4N +的化合物来源，以及一种或多种四烷基铵阳离子R5R6R7R8N +化合物作为结构导向剂; （2）使步骤（1）中得到的混合物结晶得到具有CHA型骨架结构的沸石材料; 其中Y是四价元素，X是三价元素，其中R 1，R 2，R 3，R 4，R 5，R 6和R 7彼此独立地代表烷基，并且其中R8代表环烷基，以及沸石材料，可以根据本发明的方法和它们的用途获得。

7. 发明申请

WO2015083113A1 METHOD AND USE FOR THE TERTIARY MINERAL OIL PRODUCTION BY MEANS OF METAL-ORGANIC FRAMEWORK MATERIALS 审中-公开
标题翻译：方法和使用金属有机框架材料的初步矿物油生产
公开(公告)号：WO2015083113A1
公开(公告)日：2015-06-11
申请号：PCT/IB2014/066586
申请日：2014-12-04
申请人： BASF SE , BASF CHINA COMPANY LIMITED
发明人： MAURER, Stefan , KIMURA, Riichiro , PARVULESCU, Andrei-Nicolae , REINHARDT, Caroline , SIGGEL, Lorenz , MÜLLER, Ulrich
IPC分类号： C09K8/58 , C07D233/58
CPC分类号： C07D233/58 , C09K8/58
摘要： The invention relates to a method for tertiary mineral oil production, in which an aqueous suspension, comprising at least one porous metal-organic framework material,is injected through at least one injection borehole into a mineral oil deposit, and crude oil is withdrawn from the deposit through at least one production borehole. The invention further relates to the use of an aqueous suspension, comprising at least one porous metal-organic framework material. The invention further relates to the use of at least one porous metal-organic framework material or an aqueous suspension for tertiary mineral production.
摘要翻译：本发明涉及一种用于三次矿物油生产的方法，其中包含至少一种多孔金属 - 有机骨架材料的水性悬浮液通过至少一个注入孔注入矿物油沉积物中，并将原油从通过至少一个生产井眼沉积。本发明还涉及包含至少一种多孔金属 - 有机骨架材料的水性悬浮液的用途。本发明还涉及至少一种多孔金属 - 有机骨架材料或水性悬浮液用于三次矿物生产的用途。

8. 发明申请

WO2015025250A1 METHOD FOR UPTAKING A SPILLED LIQUID 审中-公开
标题翻译：一种溢出液体的方法
公开(公告)号：WO2015025250A1
公开(公告)日：2015-02-26
申请号：PCT/IB2014/063911
申请日：2014-08-14
申请人： BASF SE , BASF CHINA COMPANY LIMITED
发明人： MAURER, Stefan , KIMURA, Riichiro , PARVULESCU, Andrei-Nicolae , PETRY, Julia , SIGGEL, Lorenz , MÜLLER, Ulrich
IPC分类号： C02F1/28 , B01J20/26 , B01D15/00
CPC分类号： B01J20/28042 , B01J20/226 , C02F1/285 , C02F1/40 , C02F2101/32 , C02F2103/365
摘要： The present invention relates to a method for at least partly uptaking a spilled liquid comprising at least one liquid hydrocarbon, the method comprising the step of contacting the at least one liquid hydrocarbon with a binder agent comprising at least one porous metal-organic framework material, wherein the at least one metal-organic framework material comprises at least one organic compound coordinated to at least one metal ion, wherein the at least one organic com- pound is based on imidazole, which is unsubstituted or substituted with one or more substituents independently selected from the group consisting of C 1-6 alkyl, phenyl and benzyl. The invention further relates to the use of such a binder agent for at least partly uptaking the liquid.
摘要翻译：本发明涉及至少部分吸收包含至少一种液体烃的溢出液体的方法，该方法包括使至少一种液态烃与包含至少一种多孔金属 - 有机骨架材料的粘合剂接触的步骤，其中所述至少一种金属 - 有机骨架材料包含与至少一种金属离子配位的至少一种有机化合物，其中所述至少一种有机化合物是基于咪唑，其是未取代的或被一个或多个独立选择的取代基取代的取代基由C1-6烷基，苯基和苄基组成。本发明还涉及这种粘合剂用于至少部分吸收液体的用途。

9. 发明申请

WO2015018807A2 PROCESS FOR THE OXYGEN FREE CONVERSION OF METHANE TO ETHYLENE ON ZEOLITE CATALYSTS 审中-公开
标题翻译：甲醇在乙酸乙酯中自由转化成沸石催化剂的方法
公开(公告)号：WO2015018807A2
公开(公告)日：2015-02-12
申请号：PCT/EP2014/066757
申请日：2014-08-05
申请人： BASF SE , TOKYO INSTITUTE OF TECHNOLOGY
发明人： FEYEN, Mathias , MÜLLER, Ulrich , BAO, Xinhe , ZHANG, Weiping , DE VOS, Dirk , GIES, Hermann , TATSUMI, Takashi , XIAO, Feng-Shou , GUO, Xiaoguang
IPC分类号： B01J29/04
CPC分类号： C07C2/76 , B01J29/0358 , B01J29/061 , B01J29/48 , B01J29/72 , B01J29/78 , B01J29/7815 , B01J29/80 , B01J29/85 , B01J29/90 , B01J38/10 , B01J2229/186 , C07C2529/74 , C07C2529/76 , C07C2529/78 , C07C2529/80 , Y02P20/52 , Y02P20/582 , Y02P20/584 , Y02P20/588 , C07C11/04
摘要： The present invention relates to a process for the oxygen free conversion of methane to ethylene on zeolite catalysts and catalysts comprising a zeolite, a metal and a further component.
摘要翻译：本发明涉及一种在沸石催化剂上甲烷无氧转化成乙烯的方法和包含沸石，金属和其它组分的催化剂。

10. 发明申请

WO2014154429A1 PASSIVIERUNG EINES ZEOLITH-KATALYSATORS IN EINER WIRBELSCHICHT 审中-公开
标题翻译：钝化沸石催化剂在流化床
公开(公告)号：WO2014154429A1
公开(公告)日：2014-10-02
申请号：PCT/EP2014/053702
申请日：2014-02-26
申请人： BASF SE
发明人： FEYEN, Mathias , SCHAACK, Bernd Bastian , MÜLLER, Ulrich , HEIDEMANN, Thomas , WILL, Veronika , SENK, Rainer
IPC分类号： B01J37/02 , B01J37/18 , B01J29/48 , C07C2/76 , C07C15/04
CPC分类号： C07C2/76 , B01J29/405 , B01J29/42 , B01J29/46 , B01J29/48 , B01J29/90 , B01J33/00 , B01J38/10 , B01J2229/123 , B01J2229/186 , B01J2229/32 , C07C2527/24 , C07C2529/46 , C07C2529/48 , Y02P20/52 , Y02P20/584 , C07C15/04
摘要： Verfahren zur Herstellung eines passivierten Katalysators, der einen Zeolith und mindestens ein aktives Metall enthält, dadurch gekennzeichnet, dass - der Katalysator in einer Wirbelschicht gehalten wird und - in der Wirbelschicht mit einer Siliciumverbindung passiviert wird.
摘要翻译：所述催化剂被保持在流化床和 - - 一种含有沸石和至少一种活性金属，其特征在于，一个钝化的催化剂过程在流化床与硅化合物钝化。

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