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1. 发明申请

WO2019154081A1 PROCESS FOR PREPARING A ZEOLITIC MATERIAL COMPRISING TI AND HAVING FRAMEWORK TYPE CHA 审中-公开
公开(公告)号：WO2019154081A1
公开(公告)日：2019-08-15
申请号：PCT/CN2019/072771
申请日：2019-01-23
申请人： BASF SE , BASF (CHINA) COMPANY LIMITED
发明人： FEYEN, Mathias , MUELLER, Ulrich , BAO, Xinhe , ZHANG, Weiping , DE VOS, Dirk , GIES, Hermann , XIAO, Feng-Shou , YOKOI, Toshiyuki , KOLB, Ute , MARLER, Bernd , WANG, Yong , DE BAERDEMAEKER, Trees , SHI, Chuan , MENG, Xiangju , PAN, Xiulian
IPC分类号： C01B39/00 , C01B39/02
摘要： A process for preparing a zeolitic material comprising Ti, having framework type CHA and having a framework structure which comprises Si and O, said process comprising (i) preparing a pre-synthesis mixture comprising water, a CHA framework structure directing agent, and a zeolitic material comprising Ti, having framework type MFI and having a framework structure which comprises Si and O; (ii) removing water from the pre-synthesis mixture obtained from (i) by heating the pre-synthesis mixture to a temperature of less than 100°C at a pressure of less than 1 bar (abs); (iii) hydrothermally crystallizing the zeolitic material comprising Ti, having framework type CHA and having a framework structure which comprises Si and O.

2. 发明申请

WO2017216012A1 CATALYST COMPOSITE AND USE THEREOF IN THE SELECTIVE CATALYTIC REDUCTION OF NOx 审中-公开
标题翻译：催化剂复合材料及其在选择性催化还原NOx中的应用
公开(公告)号：WO2017216012A1
公开(公告)日：2017-12-21
申请号：PCT/EP2017/063856
申请日：2017-06-07
申请人： BASF SE
发明人： TRUKHAN, Natalia , MALTRY, Michaela , MUELLER, Ulrich , MARX, Stefan , DUMBUYA, Karifala , FEYEN, Mathias
IPC分类号： B01J29/72 , B01D53/86 , B01D53/94 , B01J29/76 , B01J37/08 , B01J37/10 , B01J37/02 , B01J35/10 , B01J35/04
摘要： The present invention relates to a process for the preparation of a catalyst for selective catalytic reduction comprising • (i) preparing a mixture comprising a metal-organic framework material comprising an ion of a metal or metalloid selected from groups 2-5, groups 7-9, and groups 11-14 of the Periodic Table of the Elements, and at least one at least monodentate organic compound, a zeolitic material containing a metal as a non-framework element, optionally a solvent system, and optionally a pasting agent, • (ii) calcining of the mixture obtained in (i); and further relates to a catalyst per se comprising a composite material containing an amorphous mesoporous metal and/or metalloid oxide and a zeolitic material, wherein the zeolitic material contains a metal as non-framework element, as well as to the use of said catalyst.
摘要翻译：本发明涉及制备用于选择性催化还原的催化剂的方法，其包括：（i）制备包含金属 - 有机骨架材料的混合物，所述金属 - 有机骨架材料包含选自以下的金属或准金属的离子：组元素周期表的第2-5族，第7-9族和第11-14族，以及至少一种至少单齿有机化合物，包含金属作为非骨架元素的沸石材料，任选的溶剂体系（ii）煅烧在（i）中获得的混合物;和（ii）煅烧在（i）中获得的混合物。并且进一步涉及催化剂本身包括含有一种无定形孔金属和/或准金属氧化物和沸石材料，其中所述沸石材料中含有金属作为非骨架元素，以及对使用所述催化剂的复合材料。

3. 发明申请

WO2019024909A1 A ZEOLITIC MATERIAL HAVING FRAMEWORK TYPE CHA AND COMPRISING A TRANSITION METAL AND ONE OR MORE OF POTASSIUM AND CESIUM 审中-公开
公开(公告)号：WO2019024909A1
公开(公告)日：2019-02-07
申请号：PCT/CN2018/098471
申请日：2018-08-03
申请人： BASF SE , BASF (CHINA) COMPANY LIMITED
发明人： FEYEN, Mathias , MUELLER, Ulrich , BAO, Xinhe , ZHANG, Weiping , DE VOS, Dirk , GIES, Hermann , XIAO, Feng-Shou , YOKOI, Toshiyuki , KOLB, Ute , MARLER, Bernd , WANG, Tong , DE BAERDEMAEKER, Trees , SHI, Chuan , PAN, Xiulian , MENG, Xiangju
IPC分类号： B01J29/064 , B01D53/94
摘要： A zeolitic material having framework type CHA, comprising a transition metal M and an alkali metal A, and having a framework structure comprising a tetravalent element Y, a trivalent element X and O, wherein the transition metal M is a transition metal of groups 7 to 12 of the periodic table, A is one or more of K and Cs, Y is one or more of Si, Ge, Ti, Sn and Zr, and X is one or more of Al, B, Ga and In.A process for preparing such a zeolitic material. Use of such a zeolitic material.

4. 发明申请

WO2015185625A2 CHA TYPE ZEOLITIC MATERIALS AND METHODS FOR THEIR PREPARATION USING COMBINATIONS OF CYCLOALKYL- AND TETRAALKYLAMMONIUM COMPOUNDS 审中-公开
标题翻译： CHA类型的ZEOLITIC材料及其使用环己基 - 和四氨基亚甲基化合物的组合制备方法
公开(公告)号：WO2015185625A2
公开(公告)日：2015-12-10
申请号：PCT/EP2015/062377
申请日：2015-06-03
申请人： BASF SE
发明人： FEYEN, Mathias , YANG, Jeff , RUETZ, Roger , MÜLLER, Ulrich
IPC分类号： C01B39/48
CPC分类号： C01B39/48 , B01J20/18 , B01J20/3057 , B01J20/3085 , B01J29/7015 , B01J29/763 , B01J35/002 , B01J35/023 , B01J37/0018 , B01J37/0246 , B01J39/02 , B01J39/14 , B01J2229/186 , B01J2229/42
摘要： The present invention relates to a process for the preparation of a zeolitic material having a CHA-type framework structure comprising YO 2 and X 2 O 3 , wherein said process comprises the steps of: (1) providing a mixture comprising one or more sources for YO 2 , one or more sources for X 2 O 3 , one or more tetraalkylammonium cation R 1 R 2 R 3 R 4 N + -containing compounds, and one or more tetraalkylammonium cation R 5 R 6 R 7 R 8 N + -containing compounds as structure directing agent; (2) crystallizing the mixture obtained in step (1) for obtaining a zeolitic material having a CHA-type framework structure; wherein Y is a tetravalent element and X is a trivalent element, wherein R 1 , R 2 , R 3 , R 4 , R 5 , R 6 , and R 7 independently from one another stand for alkyl, and wherein R 8 stands for cycloalkyl, as well as to zeolitic materials which may be obtained according to the inventive process and to their use.
摘要翻译：本发明涉及一种制备具有包含YO 2和X 2 O 3的CHA型骨架结构的沸石材料的方法，其中所述方法包括以下步骤：（1）提供包含一种或多种YO 2，更多的X2O3，一种或多种四烷基铵阳离子R1R2R3R4N +的化合物来源，以及一种或多种四烷基铵阳离子R5R6R7R8N +化合物作为结构导向剂; （2）使步骤（1）中得到的混合物结晶得到具有CHA型骨架结构的沸石材料; 其中Y是四价元素，X是三价元素，其中R 1，R 2，R 3，R 4，R 5，R 6和R 7彼此独立地代表烷基，并且其中R8代表环烷基，以及沸石材料，可以根据本发明的方法和它们的用途获得。

5. 发明申请

WO2015018807A2 PROCESS FOR THE OXYGEN FREE CONVERSION OF METHANE TO ETHYLENE ON ZEOLITE CATALYSTS 审中-公开
标题翻译：甲醇在乙酸乙酯中自由转化成沸石催化剂的方法
公开(公告)号：WO2015018807A2
公开(公告)日：2015-02-12
申请号：PCT/EP2014/066757
申请日：2014-08-05
申请人： BASF SE , TOKYO INSTITUTE OF TECHNOLOGY
发明人： FEYEN, Mathias , MÜLLER, Ulrich , BAO, Xinhe , ZHANG, Weiping , DE VOS, Dirk , GIES, Hermann , TATSUMI, Takashi , XIAO, Feng-Shou , GUO, Xiaoguang
IPC分类号： B01J29/04
CPC分类号： C07C2/76 , B01J29/0358 , B01J29/061 , B01J29/48 , B01J29/72 , B01J29/78 , B01J29/7815 , B01J29/80 , B01J29/85 , B01J29/90 , B01J38/10 , B01J2229/186 , C07C2529/74 , C07C2529/76 , C07C2529/78 , C07C2529/80 , Y02P20/52 , Y02P20/582 , Y02P20/584 , Y02P20/588 , C07C11/04
摘要： The present invention relates to a process for the oxygen free conversion of methane to ethylene on zeolite catalysts and catalysts comprising a zeolite, a metal and a further component.
摘要翻译：本发明涉及一种在沸石催化剂上甲烷无氧转化成乙烯的方法和包含沸石，金属和其它组分的催化剂。

6. 发明申请

WO2014154429A1 PASSIVIERUNG EINES ZEOLITH-KATALYSATORS IN EINER WIRBELSCHICHT 审中-公开
标题翻译：钝化沸石催化剂在流化床
公开(公告)号：WO2014154429A1
公开(公告)日：2014-10-02
申请号：PCT/EP2014/053702
申请日：2014-02-26
申请人： BASF SE
发明人： FEYEN, Mathias , SCHAACK, Bernd Bastian , MÜLLER, Ulrich , HEIDEMANN, Thomas , WILL, Veronika , SENK, Rainer
IPC分类号： B01J37/02 , B01J37/18 , B01J29/48 , C07C2/76 , C07C15/04
CPC分类号： C07C2/76 , B01J29/405 , B01J29/42 , B01J29/46 , B01J29/48 , B01J29/90 , B01J33/00 , B01J38/10 , B01J2229/123 , B01J2229/186 , B01J2229/32 , C07C2527/24 , C07C2529/46 , C07C2529/48 , Y02P20/52 , Y02P20/584 , C07C15/04
摘要： Verfahren zur Herstellung eines passivierten Katalysators, der einen Zeolith und mindestens ein aktives Metall enthält, dadurch gekennzeichnet, dass - der Katalysator in einer Wirbelschicht gehalten wird und - in der Wirbelschicht mit einer Siliciumverbindung passiviert wird.
摘要翻译：所述催化剂被保持在流化床和 - - 一种含有沸石和至少一种活性金属，其特征在于，一个钝化的催化剂过程在流化床与硅化合物钝化。

7. 发明申请

WO2013160133A1 CATALYTICALLY ACTIVE BODY FOR THE SYNTHESIS OF DIMETHYL ETHER FROM SYNTHESIS GAS 审中-公开
标题翻译：合成气体合成二甲醚的催化活性体
公开(公告)号：WO2013160133A1
公开(公告)日：2013-10-31
申请号：PCT/EP2013/057763
申请日：2013-04-15
申请人： BASF SE , BASF SCHWEIZ AG
发明人： SCHÄFER, Alexander , FEYEN, Mathias , PARVULESCU, Andrei-Nicolae , MüLLER, Ulrich , SCHAACK, Bernd Bastian
IPC分类号： B01J23/80 , B01J29/06 , B01J29/40 , C07C41/01
CPC分类号： B01J29/76 , B01J23/80 , B01J29/06 , B01J29/40 , B01J29/46 , C07C41/01 , C07C41/09 , C07C43/043
摘要： The invention relates to a catalytically active body for the synthesis of dimethyl ether from synthesis gas. In particular, the invention relates to an improved catalytically active body for the synthesis of dimethyl ether, whereby the components of the active body comprise a methanol active component and an acid component comprising a zeolitic material being crystallized by means of one or more alkenyltrialkylammonium cation R 1 R 2 R 3 R 4 N + -containing compounds as structure directing agent. Furthermore, the present invention concerns a method for the preparation of a catalytically active body, the use of the catalytically active body and a method for the preparation of dimethyl ether from synthesis gas.
摘要翻译：本发明涉及从合成气合成二甲醚的催化活性体。特别地，本发明涉及用于合成二甲醚的改进的催化活性体，其中活性体的组分包含甲醇活性组分和酸组分，该组分包含通过一个或多个烯基三烷基铵阳离子R1R2R3R4N +结晶的沸石材料，作为结构导向剂的化合物。此外，本发明涉及制备催化活性体的方法，催化活性体的用途以及从合成气中制备二甲醚的方法。

8. 发明申请

WO2019085800A1 PROCESS FOR THE PREPARATION OF ZEOLITES ENCAPSULATING TRANSITION METAL NANOPARTICLES FROM LAYERED SILICATE PRECURSORS 审中-公开
公开(公告)号：WO2019085800A1
公开(公告)日：2019-05-09
申请号：PCT/CN2018/111618
申请日：2018-10-24
申请人： BASF SE , BASF (CHINA) COMPANY LTD.
发明人： MCGUIRE, Robert , FEYEN, Mathias , MUELLER, Ulrich , ZHANG, Weiping
IPC分类号： B01J21/00 , B01J29/00
摘要： The present invention relates to a process for the production of a transition metal containing zeolite comprising expanding a layered silicate with a swelling agent and introducing the transition metal into the interlayer expanded silicate prior to calcination thereof for obtaining the transition metal containing zeolite. The present invention further relates to a zeolite containing transition metal nanoparticles as obtainable or obtained according to the inventive process, as well as to a zeolite containing nanoparticles per se. Finally the present invention relates to the use of a zeolite containing transition metal nanoparticles as obtainable or obtained according to the inventive process, as well as to the use of a zeolite containing nanoparticles per se.

9. 发明申请

WO2016128917A1 PROCESS FOR THE PREPARATION OF A DEALUMINATED ZEOLITIC MATERIAL HAVING THE BEA FRAMEWORK STRUCTURE 审中-公开
标题翻译：用于制备具有骨架结构的脱铝沸石材料的方法
公开(公告)号：WO2016128917A1
公开(公告)日：2016-08-18
申请号：PCT/IB2016/050715
申请日：2016-02-11
申请人： BASF SE , BASF (CHINA) COMPANY LIMITED , TOKYO INSTITUTE OF TECHNOLOGY
发明人： FEYEN, Mathias , MAURER, Stefan , MUELLER, Ulrich , BAO, Xinhe , ZHANG, Weiping , DE VOS, Dirk , GIES, Hermann , XIAO, Feng-Shou , TOSHIYUKI, Yokoi , YILMAZ, Bilge , OTOMO, Ryoichi
IPC分类号： C01B39/06 , B01J29/06
CPC分类号： C01B39/026 , B01J29/7007 , B01J35/002 , B01J2229/36 , B01J2229/37 , B01J2229/40 , C01B39/46 , C07C1/20 , C07C2529/70 , C07C11/02
摘要： The present invention relates to a method for the preparation of a treated zeolitic material having a BEA framework structure comprising the steps of: (i) providing a zeolitic material having a BEA framework structure, wherein the BEA framework structure comprises YO2 and X2O3, wherein Y is a tetravalent element, and X is a trivalent element, and wherein the zeolitic material having a BEA framework structure is obtainable and/or obtained from an organotemplate-free synthetic process; (ii) calcining the zeolitic material provided in step (i) at a temperature of 650°C or more; and (iii) treating the calcined zeolitic material obtained from step (ii) with an aqueous solution having a pH of 5 or less, as well as to zeolitic materials per se preferably obtainable according to the inventive method and to their use, and to a process for converting oxygenates to olefins employing the inventive zeolitic materials.
摘要翻译：本发明涉及一种制备具有BEA骨架结构的经处理的沸石材料的方法，包括以下步骤：（i）提供具有BEA骨架结构的沸石材料，其中BEA骨架结构包含YO 2和X 2 O 3，其中Y 是四价元素，X是三价元素，并且其中具有BEA骨架结构的沸石材料可以从有机无模板合成方法获得和/或获得; （ii）在650℃以上的温度下煅烧步骤（i）中提供的沸石材料; 和（iii）用pH为5以下的水溶液以及根据本发明方法可获得的沸石材料本身及其用途来处理由步骤（ii）获得的煅烧沸石材料及其用途使用本发明的沸石材料将含氧物转化为烯烃的方法。

10. 发明申请

WO2015032851A2 SILICON-BRIDGED PILLARED SILICATE COMPOUNDS AND PROCESS FOR THEIR PRODUCTION 审中-公开
标题翻译：有机硅填料的硅酸盐化合物及其生产工艺
公开(公告)号：WO2015032851A2
公开(公告)日：2015-03-12
申请号：PCT/EP2014/068822
申请日：2014-09-04
申请人： BASF SE , TOKYO INSTITUTE OF TECHNOLOGY
发明人： FEYEN, Mathias , RUETZ, Roger , MÜLLER, Ulrich , GAAB, Manuela , BAO, Xinhe , ZHANG, Weiping , DE VOS, Dirk , WEISS, Ralf , GIES, Hermann , TATSUMI, Takashi , XIAO, Feng-Shou , TOSHIYUKI, Yokoi , YILMAZ, Bilge , DE BAERDEMAECKER, Trees
IPC分类号： C01B37/02
CPC分类号： B01J29/035 , B01J29/049 , B01J29/06 , B01J35/002 , B01J35/1019 , B01J2229/32 , B01J2229/37 , B01J2229/40 , B01J2229/42 , C01B33/38 , C04B35/16 , C04B2235/5409 , C07C1/20 , C07C2521/08 , C07C2529/00 , C07C11/02
摘要： The present invention relates to a process for the preparation of a pillared silicate compound comprising a layered silicate structure and bridging silicon atoms located between adjacent silicate layers of the silicate structure, wherein said bridging silicon atoms form at least one covalent bond to each of the adjacent silicate layers, said process comprising (1) providing one or more layered silicates; (2) adding said one or more layered silicates to a solvent system, wherein the resulting mixture has a pH of 5 or less; and (3) subjecting the mixture obtained in step (2) to solvothermal conditions; wherein no silicon-containing compound according to formula (I) R4-mSi[-(SiR2)n-R]m (I) is used at any point of the process up to and including step (3), wherein m is 1, 2, 3, or 4, and n is an integer greater than or equal to 0, wherein when n is equal to 0, one or more residues R are leaving groups, and wherein none of the residues R contains Si, as well as to a pillared silicate compound per se, preferably as obtained and/or obtainable according to the inventive process as well as to the use of the inventive compounds.
摘要翻译：本发明涉及一种制备柱状硅酸盐化合物的方法，其包括层状硅酸盐结构和位于硅酸盐结构的相邻硅酸盐层之间的桥接硅原子，其中所述桥连硅原子与相邻的每个相邻的硅酸盐层形成至少一个共价键硅酸盐层，所述方法包括（1）提供一层或多层分层硅酸盐; （2）将一种或多种层状硅酸盐加入到溶剂体系中，其中所得混合物的pH为5或更小; 和（3）使步骤（2）中获得的混合物经历溶剂热条件; 其中在直到并包括步骤（3）的任何处理方法中，不使用根据式（I）的含硅化合物R 4-m Si [ - （SiR 2）n R] m（I），其中m为1,2， 3或4，并且n是大于或等于0的整数，其中当n等于0时，一个或多个残基R是离去基团，并且其中残基R中没有一个包含Si，以及被支化的硅酸盐化合物本身，优选根据本发明方法获得和/或可获得，以及本发明化合物的用途。

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